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1. 发明申请

WO03078310A8 METHOD FOR THE PRODUCTION OF A CATALYST CONTAINING VANADIUM, PHOSPHORUS, AND OXYGEN 审中-公开
标题翻译：用于生产钒，磷和氧的含催化剂
公开(公告)号：WO03078310A8
公开(公告)日：2004-11-11
申请号：PCT/EP0302502
申请日：2003-03-12
申请人： BASF AG , WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
发明人： WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/08 , B01J37/14 , B01J37/18 , C07C51/215 , C07C51/25 , C07C57/145
CPC分类号： B01J8/10 , B01J8/067 , B01J19/22 , B01J27/198 , B01J35/023 , B01J35/026 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/08 , B01J37/14 , B01J37/18 , B01J2208/00849 , B01J2208/00876 , B01J2219/182 , C07C51/215 , C07C51/252 , C07C57/145
摘要： Disclosed is a method for producing a catalyst containing vanadium, phosphorus, and oxygen, which is used for oxidizing the gas phase of a hydrocarbon having at least four carbon atoms to maleic anhydride. According to the inventive method, a corresponding catalyst precursor which contains vanadium, phosphorus, and oxygen and is provided with particles having an average diameter of at least 2 mm is converted into a catalytically active form by means of calcination, and a flow of the catalyst precursor is transported on a conveyor belt across at least one calcination area over a distance ln at an essentially steady speed in order to be calcinated. The variation over time of the gas temperature in relation to the set point value amounts to
摘要翻译：一种用于生产一种适用于具有至少四个碳原子的烃的非均相催化气相氧化马来酸酐，含有钒，磷和氧的催化剂，其中含有相应的钒，磷，和具有氧的催化剂前体的方法，其中具有至少2mm的平均直径的颗粒，换算通过煅烧成催化活性形式，其中通过至少一个煅烧区，长度LN N，进行在传送带上以基本上恒定的速度进行煅烧的催化剂前体的电流，其中在该范围内的任何点与设定值的气体温度的时间变化催化剂前体的煅烧区的LN / 2在每种情况下的长度的一半后的流<= 5℃，并在气体温度的任何点之间在催化剂前体的流的区域中的局部差异 s为煅烧LN / 2的每个<= 5°C后一半的长度。

2. 发明申请

WO2004014833A2 METHOD FOR PRODUCING MALEIC ANHYDRIDE 审中-公开
标题翻译：制备马来酸酐的方法
公开(公告)号：WO2004014833A2
公开(公告)日：2004-02-19
申请号：PCT/EP0307982
申请日：2003-07-22
申请人： BASF AG , WEIGUNY JENS , RUPPEL WILHELM , DUDA MARK
发明人： WEIGUNY JENS , RUPPEL WILHELM , DUDA MARK
IPC分类号： C07B61/00 , C07D307/60 , C07C51/00
CPC分类号： C07D307/60
摘要： The invention relates to a method for producing maleic anhydride by the heterogeneous catalytic gas phase oxidation of hydrocarbons comprising at least four carbon atoms with gases containing oxygen, in the presence of a volatile phosphorus compound, on a catalyst containing vanadium, phosphor and oxygen in a multitube flow reactor unit with at least one reaction zone that is cooled by a heat-transfer medium, at a temperature ranging between 350 and 500 °C. In the first reaction zone, in relation to the educt supply, the supply temperature and/or the supply quantity is set in such a way that the average temperature of the heat transfer medium in the first reaction zone TSB(1st zone), said temperature being produced by the average value formation of the supply temperature and the drainage temperature of the heat-transfer medium, fulfils the formulas (I) and (II): (I) TSB(1st zone)
摘要翻译：一种用于通过具有在挥发性含磷化合物的催化剂在具有钒，磷和氧在管束反应器单元的至少一个的温度在所述范围由载热介质的反应区中冷却的存在下与含氧气体的至少四个碳原子的烃的非均相催化气相氧化制备马来酸酐的方法从350至500℃，其中，在其中进料的温度和/或载热介质的供给量相对于被调节到反应物供应，在第一反应区，使得在第一反应区TSB载热介质的平均温度（第一区），其通过平均入口温度和载热介质的流动温度，式（I）和（II）得到的：TSB（第一区）<= TD（1个区） - TSafety（1个区）（I）... ; TSB，λ最大（1个区） - TA <= TSB（第一区）<= TSB，λ最大+ TB（II）被满足，其中TD（1（1区）（1个区）（1个区）。。。。用于第一反应区的通过温度; TSafety（第一区）代表第一反应区的安全温度，为1°C; （1个区）TSB，λ最大是在第一反应区中的载热介质，其中，在TSB（第一区）的范围内的平均温度<= TD最大产率在马来酸酐实现。（1个区）; TA（第一区）为20°C; 和TB（第一区）是10℃

3. 发明申请

WO03078310A2 METHOD FOR THE PRODUCTION OF A CATALYST CONTAINING VANADIUM, PHOSPHORUS, AND OXYGEN 审中-公开
标题翻译：用于生产钒，磷和氧的含催化剂
公开(公告)号：WO03078310A2
公开(公告)日：2003-09-25
申请号：PCT/EP0302502
申请日：2003-03-12
申请人： BASF AG , WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
发明人： WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/08 , B01J37/14 , B01J37/18 , C07C51/215 , C07C51/25 , C01B3/38
CPC分类号： B01J8/10 , B01J8/067 , B01J19/22 , B01J27/198 , B01J35/023 , B01J35/026 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/08 , B01J37/14 , B01J37/18 , B01J2208/00849 , B01J2208/00876 , B01J2219/182 , C07C51/215 , C07C51/252 , C07C57/145
摘要： Disclosed is a method for producing a catalyst containing vanadium, phosphorus, and oxygen, which is used for oxidizing the gas phase of a hydrocarbon having at least four carbon atoms to maleic anhydride. According to the inventive method, a corresponding catalyst precursor which contains vanadium, phosphorus, and oxygen and is provided with particles having an average diameter of at least 2 mm is converted into a catalytically active form by means of calcination, and a flow of the catalyst precursor is transported on a conveyor belt across at least one calcination area over a distance ln at an essentially steady speed in order to be calcinated. The variation over time of the gas temperature in relation to the set point value amounts to
摘要翻译：一种用于生产一种适用于具有至少四个碳原子的烃的非均相催化气相氧化马来酸酐，含有钒，磷和氧的催化剂，其中含有相应的钒，磷，和具有氧的催化剂前体的方法，其中具有至少2mm的平均直径的颗粒，换算通过煅烧成催化活性形式，其中通过至少一个煅烧区，长度LN N，进行在传送带上以基本上恒定的速度进行煅烧的催化剂前体的电流，其中在该范围内的任何点与设定值的气体温度的时间变化催化剂前体的煅烧区的LN / 2在每种情况下的长度的一半后的流<= 5℃，并在气体温度的任何点之间在催化剂前体的流的区域中的局部差异 s为煅烧LN / 2的每个<= 5°C后一半的长度。

4. 发明申请

WO0234387A8 CATALYST AND METHOD FOR PRODUCING MALEIC ANHYDRIDE 审中-公开
标题翻译：催化剂及其生产顺酐
公开(公告)号：WO0234387A8
公开(公告)日：2002-05-23
申请号：PCT/EP0112445
申请日：2001-10-26
申请人： BASF AG , STORCK SEBASTIAN , WEIGUNY JENS , DUDA MARK , COX GERHARD
发明人： STORCK SEBASTIAN , WEIGUNY JENS , DUDA MARK , COX GERHARD
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J37/08 , C07B61/00 , C07C51/215 , C07C51/225 , C07C57/145
CPC分类号： B01J37/08 , B01J27/198 , B01J35/026 , C07C51/215 , C07C57/145
摘要： The invention relates to a vanadium-, phosphorus- and oxygen-containing catalyst that is used for producing maleic anhydride by heterogeneous catalytic gas phase oxidation of a hydrocarbon carrying at least four carbon atoms in which the ratio of phosphorus/vanadium is 0.9 to 1.5. Said catalyst comprises particles with an average diameter of at least 2 mm and the composition has a x-ray powder diffraction pattern, obtained by irradiation with CuK alpha radiation ( lambda = 1.54 10 m), that produces in the 2 theta range of 10 DEG to 70 DEG a signal/noise ratio of
摘要翻译： Vnadium，磷和催化剂用于通过具有至少四个碳原子的烃，其中所述磷/钒比为0.9〜1.5的非均相催化气相氧化制备马来酸酐，具有含氧，其具有至少2mm的平均直径的颗粒且其中使用CuKα辐射的组合物（拉姆达= 1.54。10- <10>米）的粉末XRöntgenbeugungsdiagram结果的θ2在10°〜70°时，信号/背景比将含有钒和磷相位所有衍射线可以归因，包括

5. 发明专利

BRPI0517615A 未知
公开(公告)号：BRPI0517615A
公开(公告)日：2008-10-14
申请号：BRPI0517615
申请日：2005-11-11
申请人： BASF AG
发明人： CRONE SVEN , KLANNER CATHARINA , SCHINDLER GOETZ-PETER , DUDA MARK , BORGMEIER FRIEDER
IPC分类号： C07C5/333 , C07C11/167
摘要： Processes for producing butadiene from n-butane comprising: (a) providing a feed gas stream comprising n-butane; (b) non-oxidatively dehydrogenating the feed gas stream in the presence of a catalyst in a first dehydrogenation zone to form a first intermediate gas stream comprising n-butane, 1-butene, 2-butene, butadiene and hydrogen; (c) oxidatively dehydrogenating the first intermediate gas stream in the presence of an oxygenous gas having an oxygen content of at least 75% by volume in a second dehydrogenation zone to form a second intermediate gas stream comprising n-butane, butadiene, hydrogen, carbon dioxide and steam; (d) compressing and cooling the second intermediate gas to form a first condensate stream comprising water and a third intermediate gas stream comprising n-butane, butadiene, hydrogen, carbon dioxide and steam; (e) compressing and cooling the third intermediate gas to form a second condensate stream comprising n-butane, butadiene and water and a fourth intermediate gas stream comprising n-butane, butadiene, hydrogen and carbon dioxide; (1) cooling the fourth intermediate gas stream to form a third condensate stream comprising n-butane and butadiene, and an offgas stream comprising carbon dioxide and hydrogen; (g) removing water from the second condensate stream and combining the second condensate stream and third condensate stream to form a C 4 hydrocarbon stream comprising n-butane and butadiene; and (h) separating the C 4 hydrocarbon stream to form a recylce stream comprising n-butane and a product stream comprising butadiene; wherein at least a portion of the recycle stream is fed to the first dehydrogenation zone.

6. 发明专利

DE102005035978A1 未知
公开(公告)号：DE102005035978A1
公开(公告)日：2007-02-01
申请号：DE102005035978
申请日：2005-07-28
申请人： BASF AG
发明人： DOBNER CORNELIA , DUDA MARK , RAICHLE ANDREAS , WILMER HAGEN , ROSOWSKI FRANK , HOELZLE MARKUS
IPC分类号： B01J27/185 , B01J23/847 , B01J37/03 , C07D307/60
摘要： Catalysts comprising a catalytically active composition, the catalytically active composition comprising vanadium, phosphorus, iron and oxygen, wherein the catalytically active composition has an iron:vanadium atomic ratio of 0.005 to

7. 发明专利

BRPI0412985A 未知
公开(公告)号：BRPI0412985A
公开(公告)日：2006-10-03
申请号：BRPI0412985
申请日：2004-07-06
申请人： BASF AG
发明人： DUDA MARK , MACHHAMMER OTTO , WECK ALEXANDER
IPC分类号： C07C51/215
摘要： Maleic anhydride production by gas-phase oxidation of n-butane with oxygen-containing gases on a heterogeneous vanadium-, phosphorus- and oxygen-containing (VPO) catalyst at 350-500[deg]C with recycling of unconverted n-butane is such that (a) the stream entering the reactor has n-butane and O 2 concentrations of 0.5-1.5 and 5-21 volume % respectively; (b) pressure at the inlet is 0.4-2 MPa abs.; and (c) 40-100% of the n-butane is converted. Maleic anhydride (MA) production by gas- phase oxidation of n-butane with oxygen-containing gases on a heterogeneous vanadium-, phosphorus- and oxygen-containing (VPO) catalyst at 350-500[deg]C with MA separation by forming a gas stream containing unconverted n-butane and water and recycling part of the n-butane to the reactor unit is such that (a) the stream entering the reactor has n-butane and oxygen concentrations of 0.5-1.5 and 5-21 volume % respectively; (b) the pressure at the inlet is 0.4-2 MPa abs.; and (c) 40-100% of the n-butane is converted.

8. 发明专利

CA2533025A1 METHOD FOR THE PRODUCTION OF MALEIC ANHYDRIDE 未知
公开(公告)号：CA2533025A1
公开(公告)日：2005-03-03
申请号：CA2533025
申请日：2004-07-06
申请人： BASF AG
发明人： DUDA MARK , WECK ALEXANDER , MACHHAMMER OTTO
IPC分类号： C07C51/215
摘要： Disclosed is a method for producing maleic anhydride by means of heterogeneo us catalytic gas phase oxidation of n-butane with gases containing oxygen on a catalyst comprising vanadium, phosphorus, and oxygen in a reactor unit at a temperature ranging between 350 and 500 ~C, whereupon the obtained maleic anhydride is isolated while a gas flow is formed that contains unreacted n- butane and water, and at least some of the unreacted n-butane is recirculate d to the reactor unit. According to the inventive method, an input flow having an n-butane concentration of 0.5 to 1.5 percent by volume and an oxygen concentration of 5 to 21 percent by volume is fed to the reactor unit while a pressure of 0.4 to 2 MPa abs is adjusted at the inlet of the reactor unit an d 40 to 100 percent of the n-butane from the input flow are reacted per reacto r cycle.

9. 发明专利

DE10235355A1 Production of maleic anhydride, useful for the production of gamma-butyrolactone, by heterogeneous catalytic gas phase oxidation of hydrocarbons with oxygen-containing gas in a reaction zone cooled by a heat exchange medium 未知
公开(公告)号：DE10235355A1
公开(公告)日：2004-02-19
申请号：DE10235355
申请日：2002-08-02
申请人： BASF AG
发明人： WEIGUNY JENS , RUPPEL WILHELM , DUDA MARK
IPC分类号： C07B61/00 , C07D307/60 , B01J27/198
摘要： A process for the production of maleic acid anhydride by heterogeneous catalytic gas phase oxidation of hydrocarbons having at least four carbon atoms with oxygen-containing gas in the presence of a volatile phosphorus compound at a vanadium, phosphorus and oxygen-containing catalyst in a tubular reactor unit having at least one reaction zone cooled by a heat exchange medium at 350-500 degreesC. A process for the production of maleic acid anhydride by heterogeneous catalytic gas phase oxidation of hydrocarbons having at least four carbon atoms with oxygen-containing gas in the presence of a volatile phosphorus compound at a vanadium, phosphorus and oxygen-containing catalyst in a tubular reactor unit having at least one reaction zone cooled by a heat exchange medium at 350-500 degreesC. With respect to the addition of reactants to the first reaction zone, the addition temperature and/or addition amount of the heat exchange medium are such that the average temperature of the heat exchange medium in the first reaction zone (TSB(1. zone)) is described by formula (1) and (2). TSB(1.zone) at most TD(1.zone)-TSafety(1.zone) (1) TSB,Amax(1.zone)-TA(1.zone) at most TSB(1.zone) at most TSB,Amax(1.zone)+TB(1.zone) (2) TD(1.zone) = through temperature in the first reaction zone corresponding to the average temperature of the heat exchange medium at which a 1 degreesC increase in the average temperature of the heat exchange medium results in a 5 degreesC increase of the hot spot temperature of the first reaction zone THS(1.zone); TSB(1.zone) = average temperature of the heat exchange medium; TSafety(1.zone) = safety temperature of the first reaction zone and is 1 degreesC; TSB,Amax(1.zone) = average temperature of the heat exchange medium in the first reaction zone in the region TSB(1.zone) of no greater than T (1.zone) corresponding to the maximum yield of maleic acid anhydride; T (1.zone) = 20 degreesC; T (1.zone) = 10 degreesC

10. 发明专利

AU2176802A Catalyst and method for producing maleic anhydride 未知
公开(公告)号：AU2176802A
公开(公告)日：2002-05-06
申请号：AU2176802
申请日：2001-10-26
申请人： BASF AG
发明人： STORCK SEBASTIAN , WEIGUNY JENS , DUDA MARK , COX GERHARD
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J37/08 , C07B61/00 , C07C51/215
摘要： A vanadium-, phosphorus- and oxygen-containing catalyst for the preparation of maleic anhydride by heterogeneously catalyzed gas-phase oxidation of a hydrocarbon of at least four carbon atoms has a phosphorus/vanadium ratio of from 0.9 to 1.5, comprises particles having a mean diameter of at least 2 mm and has a composition which, using CuKalpha radiation (lambda=1.54.10- m), gives a powder X-ray diffraction pattern which, in the 2theta range from 10° to 70°, has a signal/background ratio of

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