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1. 发明授权

US5401434A Cis-1,4-substituted 2-butene derivative 失效
标题翻译：顺式-1,4-取代的2-丁烯衍生物
公开(公告)号：US5401434A
公开(公告)日：1995-03-28
申请号：US41198
申请日：1993-04-01
申请人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
发明人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
IPC分类号： C07C13/28 , C07C22/08 , C07C25/24 , C07C43/225 , C07C255/50 , C09K19/30 , C09K19/42 , C07C255/00 , C09K19/12 , C09K19/54
CPC分类号： C07C22/08 , C07C13/28 , C07C25/24 , C07C255/50 , C07C43/225 , C09K19/3001 , C09K19/3048 , C07C2101/14
摘要： A novel liquid crystal compound having an intermediate group of a cis-1,4-substituted 2-butenyl group, low viscosity and a broad mesomorphic temperature range is provided, which compound is expressed by the following formula: ##STR1## wherein R.sup.1 represents an alkyl group of 1 to 10 carbon atoms, n represents 1 or 2, X represents a hydrogen atom, an alkyl group, a halogen atom, a cyano group, an alkoxy group, a methyl group substituted by 1 to 3 halogen atom(s) or a trihaloalkoxy group, and Y and Y' each independently represents a hydrogen atom, or a halogen atom.
摘要翻译：提供了具有顺式-1,4-取代的2-丁烯基的中间基团，低粘度和宽的介晶温度范围的新型液晶化合物，该化合物由下式表示：其中 R1表示1〜10个碳原子的烷基，n表示1或2，X表示氢原子，烷基，卤素原子，氰基，烷氧基，被1〜3个卤素原子取代的甲基或三卤代烷氧基，Y和Y'各自独立地表示氢原子或卤素原子。

2. 发明授权

US5662830A Diene derivative 失效
公开(公告)号：US5662830A
公开(公告)日：1997-09-02
申请号：US678098
申请日：1996-07-11
申请人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
发明人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
IPC分类号： C07C13/28 , C07C22/08 , C07C25/24 , C07C43/188 , C07C43/225 , C07C255/50 , C09K19/02 , C09K19/04 , C09K19/30 , C09K19/42 , C07C13/615
CPC分类号： C09K19/3003 , C07C13/28 , C07C22/08 , C07C25/24 , C07C255/50 , C07C43/188 , C07C43/225 , C09K19/0208 , C09K19/0403 , C07C2101/14 , C09K2019/0407 , C09K2019/0444 , C09K2019/3021
摘要： A novel liquid crystal material having a carbon chain containing a conjugated diene as a terminal substituent of the molecule and exhibiting superior characteristics is provided, which is a diene derivative expressed by the formula (I) ##STR1## wherein R and R' each independently represent 1-5C alkyl; A and B each independently represent 1,4-cyclohexylene or 1,4-phenylene; n is 0 or 1; m is an integer of 0 to 2; X and X' each independently represent H atom or F atom when A is 1,4-phenylene or represent H atom when A is 1,4-cyclohexylene; Y is alkyl, halogen or CN, alkoxy, methyl group substituted by 1-3 halogen atoms or trihaloalkoxy when A is 1,4-phenylene, or represent alkyl, alkoxy, methyl group substituted by 1-3 halogen atoms or trihaloalkoxy when A is 1,4-cyclohexylene; and R and R' are not simultaneously alkyl chain of 4 or more carbon atoms.The compound of the present invention has a generally usable viscosity and a high NI point and a high elastic constant ratio; hence the liquid crystal composition, particularly the liquid crystal composition for STN, containing the compound of the present invention exhibits improved characteristics as compared with the conventional ones.

3. 发明授权

US5609791A Diene derivative 失效
标题翻译：二烯衍生物
公开(公告)号：US5609791A
公开(公告)日：1997-03-11
申请号：US450805
申请日：1995-05-25
申请人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
发明人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
IPC分类号： C07C13/28 , C07C22/08 , C07C25/24 , C07C43/188 , C07C43/225 , C07C255/50 , C09K19/02 , C09K19/04 , C09K19/30 , C09K19/42
CPC分类号： C09K19/3003 , C07C13/28 , C07C22/08 , C07C25/24 , C07C255/50 , C07C43/188 , C07C43/225 , C09K19/0208 , C09K19/0403 , C07C2101/14 , C09K2019/0407 , C09K2019/0444 , C09K2019/3021
摘要： A novel liquid crystal material having a carbon chain containing a conjugated diene as a terminal substituent of the molecule and exhibiting superior characteristics is provided, which is a diene derivative expressed by the formula (I) ##STR1## wherein R and R' each independently represent 1-5C alkyl; A and B each independently represent 1,4-cyclohexylene or 1,4-phenylene; n is 0 or 1; m is an integer of 0 to 2; X and X' each independently represent H atom or F atom when A is 1,4-phenylene or represent H atom when A is 1,4-cyclohexylene; Y is alkyl, halogen or CN, alkoxy, methyl group substituted by 1-3 halogen atoms or trihaloalkoxy when A is 1,4-phenylene, or represent alkyl, alkoxy, methyl group substituted by 1-3 halogen atoms or trihaloalkoxy when A is 1,4-cyclohexylene; and R and R' are not simultaneously alkyl chain of 4 or more carbon atoms.The compound of the present invention has a generally usable viscosity and a high NI point and a high elastic constant ratio; hence the liquid crystal composition, particularly the liquid crystal composition for STN, containing the compound of the present invention exhibits improved characteristics as compared with the conventional ones.
摘要翻译：提供了具有含有共轭二烯作为分子的末端取代基并表现出优异特性的碳链的新型液晶材料，其为由式（I）表示的二烯衍生物，其中R和R' 各自独立地表示1-5C烷基; A和B各自独立地表示1,4-亚环己基或1,4-亚苯基; n为0或1; m为0〜2的整数; 当A为1,4-亚苯基时，X和X'各自独立地表示H原子或F原子，或当A为1,4-亚环己基时，表示H原子; 当A为1,4-亚苯基时，Y为烷基，卤素或CN，烷氧基，被1-3个卤素原子或三卤代烷氧基取代的甲基，或代表烷基，烷氧基，被1-3个卤素原子取代的甲基或三卤代烷氧基，当A为 1,4-亚环己基; 并且R和R'不是同时为4个或更多个碳原子的烷基链。本发明的化合物具有通常可用的粘度和高的NI点和高弹性常数比; 因此，与现有技术相比，含有本发明化合物的液晶组合物，特别是STN用液晶组合物显示出改善的特性。

4. 发明授权

US5449810A Diene derivative 失效
标题翻译：二烯衍生物
公开(公告)号：US5449810A
公开(公告)日：1995-09-12
申请号：US41184
申请日：1993-04-01
申请人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
发明人： Atsuko Fujita , Shuichi Matsui , Yuichi Onji , Makoto Ushioda , Yasuyuki Goto
IPC分类号： C07C13/28 , C07C22/08 , C07C25/24 , C07C43/188 , C07C43/225 , C07C255/50 , C09K19/02 , C09K19/04 , C09K19/30 , C09K19/42
CPC分类号： C09K19/3003 , C07C13/28 , C07C22/08 , C07C25/24 , C07C255/50 , C07C43/188 , C07C43/225 , C09K19/0208 , C09K19/0403 , C07C2101/14 , C09K2019/0407 , C09K2019/0444 , C09K2019/3021
摘要： A novel liquid crystal material having a carbon chain containing a conjugated diene as a terminal substituent of the molecule and exhibiting superior characteristics is provided, which is a diene derivative expressed by the formula (I) ##STR1## wherein R and R' each independently represent 1-5C alkyl; A and B each independently represent 1,4-cyclohexylene or 1,4-phenylene; n is 0 or 1; m is an integer of 0 to 2; X and X' each independently represent H atom or F atom when A is 1,4-phenylene or represent H atom when A is 1,4-cyclohexylene; Y is alkyl, halogen or CN, alkoxy, methyl group substituted by 1-3 halogen atoms or trihaloalkoxy when A is 1,4-phenylene, or represent alkyl, alkoxy, methyl group substituted by 1-3 halogen atoms or trihaloalkoxy when A is 1,4-cyclohexylene; and R and R' are not simultaneously alkyl chain of 4 or more carbon atoms.The compound of the present invention has a generally usable viscosity and a high NI point and a high elastic constant ratio; hence the liquid crystal composition, particularly the liquid crystal composition for STN, containing the compound of the present invention exhibits improved characteristics as compared with the conventional ones.
摘要翻译：提供了具有含有共轭二烯作为分子的末端取代基并表现出优异特性的碳链的新型液晶材料，其为由式（I）表示的二烯衍生物，其中R和R' 各自独立地表示1-5C烷基; A和B各自独立地表示1,4-亚环己基或1,4-亚苯基; n为0或1; m为0〜2的整数; 当A为1,4-亚苯基时，X和X'各自独立地表示H原子或F原子，或当A为1,4-亚环己基时，表示H原子; 当A为1,4-亚苯基时，Y为烷基，卤素或CN，烷氧基，被1-3个卤素原子或三卤代烷氧基取代的甲基，或代表烷基，烷氧基，被1-3个卤素原子取代的甲基或三卤代烷氧基，当A为 1,4-亚环己基; 并且R和R'不是同时为4个或更多个碳原子的烷基链。本发明的化合物具有通常可用的粘度和高的NI点和高弹性常数比; 因此，与现有技术相比，含有本发明化合物的液晶组合物，特别是STN用液晶组合物显示出改善的特性。

5. 发明授权

US5382379A Cyclohexane derivative 失效
标题翻译：环己烷衍生物
公开(公告)号：US5382379A
公开(公告)日：1995-01-17
申请号：US132917
申请日：1993-10-07
申请人： Yuichi Onji , Makoto Ushioda , Shuichi Matsui , Tomoyuki Kondo , Yasuyuki Goto
发明人： Yuichi Onji , Makoto Ushioda , Shuichi Matsui , Tomoyuki Kondo , Yasuyuki Goto
IPC分类号： C07C17/23 , C07C17/26 , C07C25/24 , C07C43/225 , C07C45/51 , C07C45/59 , C07C45/62 , C07C45/68 , C07C47/24 , C07C47/457 , C07C49/697 , C09K19/30 , C07C19/08
CPC分类号： C07C17/23 , C07C17/263 , C07C17/2635 , C07C25/24 , C07C43/225 , C07C45/513 , C07C45/59 , C07C45/62 , C07C45/68 , C07C47/24 , C07C47/457 , C07C49/697 , C09K19/3001 , C09K19/3003 , C09K2019/0444
摘要： A novel liquid crystal material having an alkenyl group at the end of the molecule, and having a low viscosity is provided. When the compound is added to a display element it is able to reduce the threshold voltage of the resulting display element. The compound is expressed by the formula (I), ##STR1## wherein X is a F atom, a trifluoromethyl group, a trifluoromethoxy group or a difluoromethoxy group, --A-- is 1,4-cyclohexylene or 1,4-phenylene, --B-- is 1,4-cyclohexylene, l is 0, 1 or 2, m is 0, 1 or 2, l+m.gtoreq.1, Z is --CH.sub.2 CH.sub.2 -- or single bond, n is an integer of 0 to 4, R is a H atom or a linear or branched alkyl group of 1-7C, and when R is an alkyl group, the double bond has a trans-configuration. The compounds of the present invention are suitable as liquid crystal material for STN display element, and further are chemically stable; hence it is possible to prepare a composition having a superior multiplex characteristic and capable of effecting a low voltage drive.
摘要翻译：提供了一种在分子末端具有烯基并具有低粘度的新型液晶材料。当将化合物添加到显示元件时，能够降低所得到的显示元件的阈值电压。该化合物由式（I），其中X是F原子，三氟甲基，三氟甲氧基或二氟甲氧基的式（I）表示，-A-是1,4-亚环己基或1,4-亚环己基，亚苯基，-B-是1,4-亚环己基，l是0,1或2，m是0,1或2,1 + m> = 1，Z是-CH 2 CH 2 - 或单键，n是 0〜4，R为H原子或1-7C的直链或支链烷基，当R为烷基时，双键具有反式构型。本发明的化合物适用于STN显示元件的液晶材料，并且化学稳定; 因此可以制备具有优异的多重特性并能够进行低电压驱动的组合物。

6. 发明授权

US5213708A Liquid crystalline compound having negative dielectric anisotropy value 失效
标题翻译：具有负介电各向异性值的液晶化合物
公开(公告)号：US5213708A
公开(公告)日：1993-05-25
申请号：US794622
申请日：1991-11-18
申请人： Yasuyuki Goto , Makoto Ushioda
发明人： Yasuyuki Goto , Makoto Ushioda
IPC分类号： C07D237/08 , C07D237/14 , C09K19/34
CPC分类号： C07D237/08 , C07D237/14 , C09K19/3455
摘要： The present invention provides a liquid crystalline compound having a large negative dielectric anisotropy value, a low viscosity and a large birefringence value and a liquid crystal composition suitable as an element constituting light switching elements. The liquid crystalline compound is expressed by the formula ##STR1## wherein R.sup.1 and R.sup.2 each independently represent an alkyl group or an alkoxy group each of 1 to 15 carbon atoms and Y.sub.1 and Y.sup.2 each independently represent H or F.
摘要翻译：本发明提供具有大的负介电各向异性值，低粘度和大双折射值的液晶化合物和适合作为构成光开关元件的元件的液晶组合物。液晶化合物由下式表示，其中R 1和R 2各自独立地表示具有1至15个碳原子的烷基或烷氧基，并且Y 1和Y 2各自独立地表示H或F.

7. 发明授权

US5180519A Alkenyl ether derivative and liquid crystal composition containing the same 失效
标题翻译：烯基醚衍生物和含有它们的液晶组合物
公开(公告)号：US5180519A
公开(公告)日：1993-01-19
申请号：US680042
申请日：1991-03-29
申请人： Manabu Uchida , Makoto Ushioda , Yasuyuki Goto
发明人： Manabu Uchida , Makoto Ushioda , Yasuyuki Goto
IPC分类号： C07C43/162 , C07C43/168 , C07C43/215 , C09K19/12 , C09K19/30
CPC分类号： C07C43/215 , C07C43/162 , C07C43/168 , C09K19/12 , C09K19/3003 , C07C2101/14
摘要： An alkenyl ether derivative having a low viscosity, a good compatibility with other liquid crystalline compounds and being capable of use in preparing a liquid crystal display element having a high response rate are provided, which derivative is expressed by the formulaR.sub.1 --CH.sub.2 --O--(CH.sub.2)n--A.sub.1 --A.sub.2 A.sub.3 --R.sub.2[1]wherein R.sub.1 is a 2-7C alkenyl group having a double bond at its terminal or a double bond of a trans configuration at a position other than its terminal, R.sub.2 is 1-10C alkyl group or alkoxy group, A.sub.1 and A.sub.2 each independently are a 1,4-phenylene or a trans-1,4-cyclohexylene, A.sub.3 represents a 1,4-phenylene, a trans-1,4-cyclohexylene or a single bond and n is 1 or 2.
摘要翻译：提供具有低粘度，与其它液晶化合物的良好相容性并且能够用于制备具有高响应速率的液晶显示元件的烯基醚衍生物，该衍生物由式R 1 -CH 2 -O- （CH2）n-A1-A2A3-R2 [1]其中R1是其末端具有双键的2-7C烯基或反式构型在其末端以外的位置的双键，R2为1-10C 烷基或烷氧基，A1和A2各自独立地为1,4-亚苯基或反式-1,4-亚环己基，A3表示1,4-亚苯基，反-1,4-亚环己基或单键， n为1或2。

8. 发明授权

US5167858A Pyrimidine derivative and liquid crystal composition contain the same 失效
标题翻译：嘧啶衍生物和液晶组合物含有
公开(公告)号：US5167858A
公开(公告)日：1992-12-01
申请号：US648009
申请日：1991-01-31
申请人： Yasuyuki Goto , Makoto Ushioda
发明人： Yasuyuki Goto , Makoto Ushioda
IPC分类号： G02F1/13 , C07C55/08 , C07C257/18 , C07D239/26 , C09K19/34
CPC分类号： C09K19/3469
摘要： The present invention provides a novel pyrimidine derivative having a large .DELTA..epsilon. value and a low viscosity, and affording a liquid crystal composition having a high clearing point and a low threshold voltage value without raising its viscosity when the derivative is mixed with other liquid crystal compositions or liquid crystal compound. The pyrimidine derivative is a 5-[2'-(trans-4"-alkylcyclohexyl)ethyl]-2-(3,4-difluorophenyl)pyrimidine expressed by the formula ##STR1## wherein R represents a linear alkyl group having 1 to 10 carbon atoms.
摘要翻译：本发明提供了一种具有较高DELTAε值和低粘度的新型嘧啶衍生物，并且当衍生物与其它液晶组合物混合时，提供具有高透明度和低阈值电压值的液晶组合物，而不增加其粘度或液晶化合物。嘧啶衍生物是由式“IMAGE”表示的5- [2' - （反式-4“ - 烷基环己基）乙基] -2-（3,4-二氟苯基）嘧啶，其中R表示具有1〜 10个碳原子。

9. 发明授权

US4900472A 2,5-diphenyl pyrimidine compounds and liquid crystal compositions 失效
标题翻译： 2,5-二苯基嘧啶化合物和液晶组合物
公开(公告)号：US4900472A
公开(公告)日：1990-02-13
申请号：US260519
申请日：1988-10-20
申请人： Kazutoshi Miyazawa , Makoto Ushioda , Hiromichi Inoue , Shinichi Saito , Kouji Ohno
发明人： Kazutoshi Miyazawa , Makoto Ushioda , Hiromichi Inoue , Shinichi Saito , Kouji Ohno
IPC分类号： C07D239/26 , C09K19/34
CPC分类号： C07D239/26 , C09K19/3463
摘要： The present invention provides optically active compounds represented by the following general formula: ##STR1## liquid crystal compositions containing the compounds, and electro optical elements using the above compositions.The compounds of the present invention are optically active compounds having characteristics suited for a ferroelectric liquid crystal composition, especially having enough spontaneous polarization to realize quick response.

10. 发明授权

US5183587A Liquid crystalline compound 失效
标题翻译：液晶化合物
公开(公告)号：US5183587A
公开(公告)日：1993-02-02
申请号：US454988
申请日：1989-12-22
申请人： Kisei Kitano , Makoto Ushioda , Manabu Uchida , Toshiharu Suzuki
发明人： Kisei Kitano , Makoto Ushioda , Manabu Uchida , Toshiharu Suzuki
IPC分类号： C07C43/188 , C07C17/00 , C07C22/00 , C07C22/08 , C07C25/24 , C07C43/215 , C07C255/46 , C07C255/50 , C07C255/54 , C07C255/56 , C09K19/12 , C09K19/14 , C09K19/20 , C09K19/30 , C09K19/44
CPC分类号： C07C255/56 , C07C22/00 , C07C22/08 , C07C255/50 , C09K19/14 , C09K19/20 , C09K19/3003 , C09K19/3028 , C09K19/3066
摘要： A liquid crystal compound having a relatively low viscosity, a superior compatibility with other liquid crystalline compounds and suitable for preparing a liquid crystal device having a high response rate, and a superior liquid crystal composition containing the compound are provided, which compound is expressed by the formula ##STR1## wherein R.sup.1 is H, F, Cl, CN or 1-20C alkyl or alkenyl in which alkenyl one --CH.sub.2 -- group or two not adjacent --CH.sub.2 -- groups may be replaced by --O-- and in which alkenyl the position and number of the double bond may be optionally chosen; A.sup.1, A.sup.2 and A.sup.3 are ##STR2## the H atom(s) of which ##STR3## may be replaced by F, Cl or methyl; B.sup.1 and B.sup.2 are --CH.sub.2 CH.sub.2 --, --CH.sub.2 O--, --OCH.sub.2 -- or single bond; n is 0 or 1; and m is 0 to 20.

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