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1. 发明授权

US07601378B2 Polymeric antioxidants 失效
标题翻译：聚合物抗氧化剂
公开(公告)号：US07601378B2
公开(公告)日：2009-10-13
申请号：US11235633
申请日：2005-09-26
申请人： Ashok L. Cholli , Vijayendra Kumar , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
发明人： Ashok L. Cholli , Vijayendra Kumar , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
IPC分类号： A23D7/00
CPC分类号： C08G65/44 , A23L3/349 , C08G61/10 , C08G2261/43 , C09K15/08 , C09K15/10 , C09K15/12 , C09K15/18 , C09K15/20 , C10M2207/026 , C10M2209/10 , Y10T428/1303 , Y10T428/1321 , Y10T428/1352 , Y10T428/31504 , Y10T428/31993
摘要： The following is an examiner's statement of reasons for allowance: an antioxidant polymer and method of preparing, the antioxidant comprising repeat units that include one or both of Structural Formulas (I) and (II) wherein R is —H or a substituted or unsubstituted alkyl, acyl or aryl group; Ring A is substituted with at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Ring B is substituted with at least one —H and at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group is not taught nor fairly suggested by the prior art or any combination thereof.
摘要翻译：以下是审查员关于津贴原因的说明：抗氧化聚合物和制备方法，所述抗氧化剂包含重复单元，其包含结构式（I）和（II）中的一个或两个，其中R是-H或取代或未取代的烷基，酰基或芳基; 环A被至少一个叔丁基或取代或未取代的正烷氧基羰基取代; 环B被至少一个-H取代，至少一个叔丁基或取代或未取代的正烷氧基羰基不是由现有技术或其任何组合教导或公认的。

2. 发明授权

US07507454B2 Polymeric antioxidants 失效
标题翻译：聚合物抗氧化剂
公开(公告)号：US07507454B2
公开(公告)日：2009-03-24
申请号：US11711434
申请日：2007-02-27
申请人： Ashok L. Cholli , Vijayendra Kumar , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
发明人： Ashok L. Cholli , Vijayendra Kumar , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
IPC分类号： B32B1/08
CPC分类号： C08G65/44 , A23L3/349 , C08G61/10 , C08G2261/43 , C09K15/08 , C09K15/10 , C09K15/12 , C09K15/18 , C09K15/20 , C10M2207/026 , C10M2209/10 , Y10T428/1303 , Y10T428/1321 , Y10T428/1352 , Y10T428/31504 , Y10T428/31993
摘要： Antioxidant polymers of the present invention comprise repeat units that include one or both of Structural Formulas (I) and (II): wherein: R is —H or a substituted or unsubstituted alkyl, acyl or aryl group; Ring A is substituted with at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Ring B is substituted with at least one —H and at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Rings A and B are each optionally substituted with one or more groups selected from the group consisting of —OH, —NH, —SH, a substituted or unsubstituted alkyl or aryl group, and a substituted or unsubstituted alkoxycarbonyl group; n is an integer equal to or greater than 2; and p is an integer equal to or greater than 0. The invention also includes methods of using and preparing these polymers.
摘要翻译：本发明的抗氧化聚合物包含重复单元，其包括结构式（I）和（II）中的一个或两个：其中：R是-H或取代或未取代的烷基，酰基或芳基; 环A被至少一个叔丁基或取代或未取代的正烷氧基羰基取代; 环B被至少一个-H和至少一个叔丁基或取代或未取代的正烷氧基羰基取代; 环A和环B各自任选被一个或多个选自-OH，-NH，-SH，取代或未取代的烷基或芳基和取代或未取代的烷氧基羰基的基团取代; n是等于或大于2的整数; 并且p是等于或大于0的整数。本发明还包括使用和制备这些聚合物的方法。

3. 发明授权

US07223432B2 Polymeric antioxidants 失效
公开(公告)号：US07223432B2
公开(公告)日：2007-05-29
申请号：US10408679
申请日：2003-04-04
申请人： Ashok L. Cholli , Vijayendra Kumar , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
发明人： Ashok L. Cholli , Vijayendra Kumar , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
IPC分类号： A23D7/00
CPC分类号： C08G65/44 , A23L3/349 , C08G61/10 , C08G2261/43 , C09K15/08 , C09K15/10 , C09K15/12 , C09K15/18 , C09K15/20 , C10M2207/026 , C10M2209/10 , Y10T428/1303 , Y10T428/1321 , Y10T428/1352 , Y10T428/31504 , Y10T428/31993
摘要： Antioxidant polymers of the present invention comprise repeat units that include one or both of Structural Formulas (I) and (II): wherein: R is —H or a substituted or unsubstituted alkyl, acyl or aryl group; Ring A is substituted with at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Ring B is substituted with at least one —H and at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Rings A and B are each optionally substituted with one or more groups selected from the group consisting of —OH, —NH, —SH, a substituted or unsubstituted alkyl or aryl group, and a substituted or unsubstituted alkoxycarbonyl group; n is an integer equal to or greater than 2; and p is an integer equal to or greater than 0. The invention also includes methods of using and preparing these polymers.

4. 发明授权

US07595074B2 Polymeric antioxidants 失效
标题翻译：聚合物抗氧化剂
公开(公告)号：US07595074B2
公开(公告)日：2009-09-29
申请号：US10761933
申请日：2004-01-21
申请人： Ashok L. Cholli , Vijayendra Kumar , Ashish Dhawan , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
发明人： Ashok L. Cholli , Vijayendra Kumar , Ashish Dhawan , Jayant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
IPC分类号： A23D7/00
CPC分类号： A23G3/36 , A23G4/06 , A23L3/3463 , A23L3/349 , A23L13/42 , C09K15/08 , C09K15/10 , C09K15/12 , C09K15/18 , C09K15/20 , C10M2207/026 , C10M2209/10 , C11B5/0035
摘要： A method of preparing a phenolic polymer comprising: a) protecting at least one hydroxyl group of a substituted or unsubstituted phenol represented by Structural Formula (XXIX), wherein: R11, R12, R13, R14 and R15 are independently —H, —OH, —NH, —SH, a substituted or unsubstituted alkyl or aryl group, a substituted or unsubstituted alkoxycarbonyl or aryloxycarbonyl group, a substituted or unsubstituted alkoxy group or a saturated or unsaturated carboxylic acid group; or R11, R12, R13, R14 or R15, in conjunction with an adjacent R11, R12, R13, R14 or R15, forms a substituted or unsubstituted alkylene dioxy group; provided that at least one of R11, R12, R13, R14 or R15 is a tert-butyl group 1-ethenyl-2-carboxylic acid or ester thereof, a substituted or unsubstituted alkylene dioxy group or a substituted or unsubstituted n-alkoxycarbonyl group, at least one of R11, R12, R13, R14 or R15 is a hydroxyl group, and at least one of R11, R12, R13, R14 and R15 is —H; with a protecting group, wherein thereby obtaining one or more protected hydroxyl groups; and b) polymerizing the substituted or unsubstituted phenol, thereby obtaining the phenolic polymer.
摘要翻译：一种制备酚醛聚合物的方法，包括：a）保护由结构式（XXIX）表示的取代或未取代的酚的至少一个羟基，其中：R 11，R 12，R 13，R 14和R 15独立地为-H，-OH， -NH，-SH，取代或未取代的烷基或芳基，取代或未取代的烷氧基羰基或芳氧基羰基，取代或未取代的烷氧基或饱和或不饱和羧酸基团; 或R11，R12，R13，R14或R15与相邻的R11，R12，R13，R14或R15结合形成取代或未取代的亚烷基二氧基; 条件是R11，R12，R13，R14或R15中的至少一个是叔丁基1-乙烯基-2-羧酸或其酯，取代或未取代的亚烷基二氧基或取代或未取代的正烷氧基羰基， R 11，R 12，R 13，R 14或R 15中的至少一个为羟基，R 11，R 12，R 13，R 14和R 15中的至少一个为-H; 与保护基，其中由此获得一个或多个被保护的羟基; 和b）使取代或未取代的苯酚聚合，由此得到酚类聚合物。

5. 发明授权

US07754267B2 Polymeric antioxidants 失效
公开(公告)号：US07754267B2
公开(公告)日：2010-07-13
申请号：US11711395
申请日：2007-02-27
申请人： Ashok L. Cholli , Vijayendra Kumar , Javant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
发明人： Ashok L. Cholli , Vijayendra Kumar , Javant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
IPC分类号： A23D7/00 , C09K15/04
CPC分类号： C08G65/44 , A23L3/349 , C08G61/10 , C08G2261/43 , C09K15/08 , C09K15/10 , C09K15/12 , C09K15/18 , C09K15/20 , C10M2207/026 , C10M2209/10 , Y10T428/1303 , Y10T428/1321 , Y10T428/1352 , Y10T428/31504 , Y10T428/31993
摘要： Antioxidant polymers of the present invention comprise repeat units that include one or both of Structural Formulas (I) and (II): wherein: R is —H or a substituted or unsubstituted alkyl, acyl or aryl group; Ring A is substituted with at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Ring B is substituted with at least one —H and at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Rings A and B are each optionally substituted with one or more groups selected from the group consisting of —OH, —NH, —SH, a substituted or unsubstituted alkyl or aryl group, and a substituted or unsubstituted alkoxycarbonyl group; n is an integer equal to or greater than 2; and p is an integer equal to or greater than 0. The invention also includes methods of using and preparing these polymers.

6. 发明授权

US07727571B2 Polymeric antioxidants 失效
标题翻译：聚合物抗氧化剂
公开(公告)号：US07727571B2
公开(公告)日：2010-06-01
申请号：US11711211
申请日：2007-02-27
申请人： Ashok L. Cholli , Vijayendra Kumar , Javant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
发明人： Ashok L. Cholli , Vijayendra Kumar , Javant Kumar , Virinder Singh Parmar , Lynne Ann Samuelson , Ferdinando F. Bruno
IPC分类号： A23D7/00
CPC分类号： C08G65/44 , A23L3/349 , C08G61/10 , C08G2261/43 , C09K15/08 , C09K15/10 , C09K15/12 , C09K15/18 , C09K15/20 , C10M2207/026 , C10M2209/10 , Y10T428/1303 , Y10T428/1321 , Y10T428/1352 , Y10T428/31504 , Y10T428/31993
摘要： Antioxidant polymers of the present invention comprise repeat units that include one or both of Structural Formulas (I) and (II): wherein: R is —H or a substituted or unsubstituted alkyl, acyl or aryl group; Ring A is substituted with at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Ring B is substituted with at least one —H and at least one tert-butyl group or substituted or unsubstituted n-alkoxycarbonyl group; Rings A and B are each optionally substituted with one or more groups selected from the group consisting of —OH, —NH, —SH, a substituted or unsubstituted alkyl or aryl group, and a substituted or unsubstituted alkoxycarbonyl group; n is an integer equal to or greater than 2; and p is an integer equal to or greater than 0. The invention also includes methods of using and preparing these polymers.
摘要翻译：本发明的抗氧化聚合物包含重复单元，其包括结构式（I）和（II）中的一个或两个：其中：R是-H或取代或未取代的烷基，酰基或芳基; 环A被至少一个叔丁基或取代或未取代的正烷氧基羰基取代; 环B被至少一个-H和至少一个叔丁基或取代或未取代的正烷氧基羰基取代; 环A和环B各自任选被一个或多个选自-OH，-NH，-SH，取代或未取代的烷基或芳基和取代或未取代的烷氧基羰基的基团取代; n是等于或大于2的整数; 并且p是等于或大于0的整数。本发明还包括使用和制备这些聚合物的方法。

7. 发明授权

US08143308B2 Synthesis of oligo/poly(catechins) and methods of use 有权
标题翻译：寡聚/聚（儿茶素类）的合成和使用方法
公开(公告)号：US08143308B2
公开(公告)日：2012-03-27
申请号：US11978540
申请日：2007-10-29
申请人： Ferdinando F. Bruno , Jayant Kumar , Subhalakshmi Nagarajan , Susan J. Braunhut , Ramaswamy Nagarajan , Lynne A. Samuelson , Donna McIntosh , Klaudia Foley
发明人： Ferdinando F. Bruno , Jayant Kumar , Subhalakshmi Nagarajan , Susan J. Braunhut , Ramaswamy Nagarajan , Lynne A. Samuelson , Donna McIntosh , Klaudia Foley
IPC分类号： A61K31/352 , A61P35/00 , C07D407/02 , C12P17/16
CPC分类号： A61K36/82 , A61K31/353 , C08G83/00 , C08H6/00
摘要： A method for synthesizing a biocompatible, water-soluble oligo/polyflavanoid, includes polymerizing an optionally substituted flavanoid with a polymerization agent in the presence of a biocompatible polymerization solubilizer, thereby producing the biocompatible, soluble oligo/polyflavanoid. Also included is a biocompatible, soluble, oligo/polyflavanoid or a pharmaceutically acceptable salt, solvate, or complex thereof. Also included are methods of treating a subject for cancer, cardiac damage, viral infection, and obesity.
摘要翻译：用于合成生物相容性的水溶性寡聚/类黄酮的方法包括在生物相容性聚合增溶剂的存在下用聚合剂聚合任选取代的黄酮类化合物，从而产生生物相容性的可溶性寡聚/多形黄烷。还包括生物相容性，可溶性，寡聚/多形黄烷或其药学上可接受的盐，溶剂合物或复合物。还包括治疗受试者癌症，心脏损伤，病毒感染和肥胖症的方法。

8. 发明申请

US20090170928A1 Synthesis of oligo/poly(catechins) and methods of use 有权
标题翻译：寡聚/聚（儿茶素类）的合成和使用方法
公开(公告)号：US20090170928A1
公开(公告)日：2009-07-02
申请号：US11978540
申请日：2007-10-29
申请人： Ferdinando F. Bruno , Jayant Kumar , Subhalakshmi Nagarajan , Susan J. Braunhut , Ramaswamy Nagarajan , Lynne A. Samuelson , Donna McIntosh , Klaudia Foley
发明人： Ferdinando F. Bruno , Jayant Kumar , Subhalakshmi Nagarajan , Susan J. Braunhut , Ramaswamy Nagarajan , Lynne A. Samuelson , Donna McIntosh , Klaudia Foley
IPC分类号： A61K31/352 , C07D407/02 , C12P17/16 , A61P35/00
CPC分类号： A61K36/82 , A61K31/353 , C08G83/00 , C08H6/00
摘要： A method for synthesizing a biocompatible, water-soluble oligo/polyflavanoid, includes polymerizing an optionally substituted flavanoid with a polymerization agent in the presence of a biocompatible polymerization solubilizer, thereby producing the biocompatible, soluble oligo/polyflavanoid. Also included is a biocompatible, soluble, oligo/polyflavanoid or a pharmaceutically acceptable salt, solvate, or complex thereof. Also included are methods of treating a subject for cancer, cardiac damage, viral infection, and obesity.
摘要翻译：用于合成生物相容性的水溶性寡聚/类黄酮的方法包括在生物相容性聚合增溶剂的存在下用聚合剂聚合任选取代的黄酮类化合物，从而产生生物相容性的可溶性寡聚/多形黄烷。还包括生物相容性，可溶性，寡聚/多形黄烷或其药学上可接受的盐，溶剂合物或复合物。还包括治疗受试者癌症，心脏损伤，病毒感染和肥胖症的方法。

9. 发明授权

US06210936B1 Enzyme-catalyzed modifications of macromolecules in organic solvents 失效
标题翻译：大分子在有机溶剂中的酶催化修饰
公开(公告)号：US06210936B1
公开(公告)日：2001-04-03
申请号：US09165043
申请日：1998-10-01
申请人： Joseph A. Akkara , Ferdinando F. Bruno
发明人： Joseph A. Akkara , Ferdinando F. Bruno
IPC分类号： C12P762
CPC分类号： C12P7/625
摘要： Protease enzyme from Bacillus subtilis and Bacillus sp. Catalyzes the acylation of organic solvent-insoluble macromolecules in isooctane solution containing vinyl esters of fatty acids, lactones or lactides as acyl donors. The reaction occurs only when the enzyme is solubilized via ion-pairing with the anionic surfactant dioctylsulfosuccinate, sodium salt (AOT). Enzyme based acylation was demonstrated in macromolecules such as silk proteins. These macromolecules are reactive either as cryogenically milled powder suspended in the organic solvent or as a thin film deposited onto ZnSe slides. This selective acylation approach represents the first attempt at using enzymes to modify organic-insoluble macromolecules in nonaqueous media.
摘要翻译：来自枯草芽孢杆菌和芽孢杆菌的蛋白酶催化有机溶剂不溶性大分子在含有脂肪酸，内酯或丙交酯的乙烯基酯作为酰基供体的异辛烷溶液中的酰化反应。仅当酶通过与阴离子表面活性剂二辛基磺基琥珀酸盐钠盐（AOT）的离子配对溶解时才发生反应。在大分子如丝蛋白中证明了酶的酰化作用。这些大分子作为悬浮在有机溶剂中的低温研磨粉末或沉积在ZnSe载片上的薄膜是反应性的。这种选择性酰化方法代表了在非水介质中使用酶来修饰有机不溶性大分子的第一次尝试。

10. 发明授权

US08932468B2 Separation of enzymatically synthesized polyepicatechin via high performance liquid chromatography 有权
标题翻译：通过高效液相色谱法分离酶合成的多表儿茶素
公开(公告)号：US08932468B2
公开(公告)日：2015-01-13
申请号：US12635729
申请日：2010-01-12
申请人： Nicole Favreau , Ferdinando F. Bruno
发明人： Nicole Favreau , Ferdinando F. Bruno
IPC分类号： B01D15/16
CPC分类号： B01D15/166
摘要： Disclosed is a process for the separation of one or more fractions from a resulting reaction mixture of an enzymatically catalyzed polymerization of flavonoid using HPLC with a varying concentration of organic solvent in the mobile phase. The isolated fractions can be used in numerous applications including as an antioxidant.
摘要翻译：公开了一种从所得反应混合物中分离出一种或多种级分的方法，所述反应混合物中的黄酮类化合物使用HPLC和流动相中不同浓度的有机溶剂进行酶促催化聚合。分离的级分可用于许多应用，包括作为抗氧化剂。

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