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1. 发明授权

US5320796A Method for the preparation of powder mixtures 失效
标题翻译：粉末混合物的制备方法
公开(公告)号：US5320796A
公开(公告)日：1994-06-14
申请号：US55483
申请日：1993-04-29
申请人： Asao Harashima , Kaoru Kunimatsu , Atsushi Sasaki , Ryuji Tachibana
发明人： Asao Harashima , Kaoru Kunimatsu , Atsushi Sasaki , Ryuji Tachibana
IPC分类号： B01F3/18 , B01F7/10 , B29B7/42
CPC分类号： B29B7/421 , B01F7/10 , B29B7/402 , B29B7/428 , B29C47/385 , B29C47/666 , B01F3/18
摘要： A method for producing powder mixtures capable of inducing an even more intimate, microhomogeneous intermixing in a heterogeneous powder composed of at least two types of powders. The method is effective even for the mixing of an aggregable powder and a nonaggregable powder. According to the method, a heterogeneous powder composed of at least two type of powders that have been preliminarily mixed by stirring is introduced into an inlet while a rotating axle is turning and is axially transported within a cylinder by a screw. As the heterogeneous powder passes between rotating disks and fixed disks, it is subjected to a highly efficient mixing by compression and shear forces due to a sliding-shear action exerted between depressions and elevations installed on the opposing surfaces of the rotating disks and fixed disks. The mixture passes in sequence through multiple stages of the rotating and fixed disks. A powder mixture, which has been microhomogeneously interdispersed, is discharged from the outlet.
摘要翻译：一种生产粉末混合物的方法，所述粉末混合物能够在由至少两种类型的粉末组成的非均质粉末中引起更加紧密，微均匀的混合。该方法即使对于可聚集粉末和不可聚集粉末的混合也是有效的。根据该方法，通过搅拌预先混合的至少两种粉末组成的非均相粉末在旋转轴转动的同时被引入入口，并通过螺杆在气缸内轴向传送。当异质粉末通过旋转盘和固定盘之间时，由于在安装在旋转盘和固定盘的相对表面上的凹陷和高度之间施加的滑动剪切作用，它受到压缩和剪切力的高效混合。混合物依次通过旋转和固定盘的多个阶段。已经微分散分散的粉末混合物从出口排出。

2. 发明授权

US5837793A Silicone rubber powder and method for the preparation thereof 失效
标题翻译：硅橡胶粉及其制备方法
公开(公告)号：US5837793A
公开(公告)日：1998-11-17
申请号：US819244
申请日：1997-03-17
申请人： Asao Harashima , Yoshitsugu Morita , Ryuji Tachibana
发明人： Asao Harashima , Yoshitsugu Morita , Ryuji Tachibana
IPC分类号： C08J3/12 , C08G77/08 , C08G77/14
CPC分类号： C08J3/12 , C08J3/122 , C08J2383/12
摘要： There is disclosed a silicone rubber powder prepared from a curable silicone composition, said powder comprising a polyorganosiloxane drain having at least one silicon-bonded polyoxyalkylene group of the formula --R.sup.1 (OR.sup.2).sub.m OR.sup.3 wherein R.sup.1 is an alkylene radical, R.sup.2 is an alkylene radical, R.sup.3 is selected from the group consisting of hydrogen and alkyl radicals and m is an integer having a value of 2 to 100. The rubber powder is preferably prepared by curing the above silicone composition to form a cured silicone rubber and then pulverizing the silicone rubber.
摘要翻译：公开了由可固化有机硅组合物制备的硅橡胶粉末，所述粉末包含具有至少一个式-R 1（OR 2）mOR 3的与硅键合的聚氧化烯基团的聚有机硅氧烷漏斗，其中R1是亚烷基，R2是亚烷基， R3选自氢和烷基，m是2〜100的整数。橡胶粉末优选通过固化上述有机硅组合物来制备固化的硅橡胶，然后粉碎硅橡胶。

3. 发明授权

US5628989A Antiperspirant and deodorant 失效
标题翻译：止汗剂和除臭剂
公开(公告)号：US5628989A
公开(公告)日：1997-05-13
申请号：US489474
申请日：1995-06-12
申请人： Asao Harashima , Yoshitsugu Morita , Ryuji Tachibana
发明人： Asao Harashima , Yoshitsugu Morita , Ryuji Tachibana
IPC分类号： A61K8/00 , A61K8/02 , A61K8/89 , A61K8/891 , A61Q15/00 , C08L83/04 , A61K7/32 , A61K7/34 , A61K7/38
CPC分类号： A61Q15/00 , A61K8/02 , A61K8/891 , A61K2800/412 , Y10S424/05
摘要： Antiperspirant/deodorants contain 5-90 wt % of spheroid silicone rubber powders with average particle sizes of 0.1-200 .mu.m and JIS A hardness of the silicone rubber forming said powder is 35-80. They spread well, are smooth, and have a dry feel when used.
摘要翻译：防汗剂/除臭剂含有5-90重量％的平均粒径为0.1-200μm的球状硅橡胶粉末，形成所述粉末的硅橡胶的JIS A硬度为35-80。它们传播良好，光滑，使用时感觉干燥。

4. 发明授权

US5929163A Silicone gel composition 失效
标题翻译：硅胶组合物
公开(公告)号：US5929163A
公开(公告)日：1999-07-27
申请号：US54998
申请日：1993-04-29
申请人： Asao Harashima
发明人： Asao Harashima
IPC分类号： A61K8/72 , A61K8/02 , A61K8/31 , A61K8/89 , A61K8/891 , A61K8/894 , A61Q1/00 , A61Q1/12 , A61Q5/00 , A61Q15/00 , A61Q17/04 , A61Q19/00 , C08G77/04 , C08J3/18 , C08L83/04 , C08L83/12 , C11D3/37
CPC分类号： A61K8/894 , A61K8/042 , A61K8/31 , A61Q19/00 , C08L83/04 , C08L83/12 , A61Q1/02 , A61Q15/00 , A61Q17/04 , A61Q5/06 , C08G77/045 , C08G77/46 , C08G77/70
摘要： A silicone gel composition that contains(a) a silicone oil,(b) a polyoxyalkylene group-containing organopolysiloxane with the formula ##STR1## wherein R is the methyl or phenyl group; A is the methyl group, phenyl group, or polyoxyalkylene groups with the formula--C.sub.3 H.sub.6 O(C.sub.2 H.sub.4 O).sub.a (C.sub.3 H.sub.6 O).sub.b R'wherein R' is the hydrogen atom, an acyl group, or alkyl groups having 1 to 4 carbon atoms, a is an integer with a value of 5 to 50, and b is an integer with a value of 5 to 50;m is an integer with a value of 50 to 1,000; andn is an integer with a value of 1 to 40,and (c) water.
摘要翻译：一种硅氧烷凝胶组合物，其包含（a）硅油，（b）具有下式的聚氧化烯基的有机聚硅氧烷：其中R是甲基或苯基; A是具有式-C 3 H 6 O（C 2 H 4 O）a（C 3 H 6 O）b R'的甲基，苯基或聚氧化烯基，其中R'是氢原子，酰基或具有1至4个碳原子的烷基，a是值为5〜50的整数，b为5〜50的整数， m是值为50〜1000的整数; n为1〜40的整数，（c）为水。

5. 发明申请

US20110257274A1 Method For Producing Emulsion 有权
标题翻译：生产乳液的方法
公开(公告)号：US20110257274A1
公开(公告)日：2011-10-20
申请号：US13140858
申请日：2009-12-21
申请人： Kazuhiko Kojima , Tsutomu Naganawa , Asao Harashima
发明人： Kazuhiko Kojima , Tsutomu Naganawa , Asao Harashima
IPC分类号： B01F17/00
CPC分类号： C08J3/03 , C08G77/46 , C08J2383/04
摘要： The present invention has an objective to easily obtain an emulsion exhibiting superior storage stability, and in particular, an emulsion of a polyorganosiloxane. The present invention provides a method for producing an emulsion characterized by obtaining an emulsion by emulsifying a mixture of an oil and a surfactant, obtained by synthesizing the surfactant in the oil. In particular, the method is suitably used for the preparation of an emulsion of an organopolysiloxane (A) which is usually difficult to be stably emulsified. A silicone-based surfactant (B), and in particular, a silicone-based surfactant having a small degree of polymerization of a siloxane chain such as a trisiloxane is synthesized in an oil. Thereby, an emulsion exhibiting superior storage stability can be produced.
摘要翻译：本发明的目的是容易地获得表现出优异的储存稳定性的乳液，特别是聚有机硅氧烷的乳液。本发明提供了一种乳液的制造方法，其特征在于，通过将表面活性剂在油中合成而得到的油和表面活性剂的混合物乳化得到乳液。特别地，该方法适合用于制备通常难以稳定乳化的有机聚硅氧烷（A）的乳液。在油中合成有机硅系表面活性剂（B），特别是硅氧烷链聚合度低的硅氧烷系表面活性剂，例如三硅氧烷。由此，可以制造出具有优异的储存稳定性的乳液。

6. 发明授权

US5328683A Water repellent and method of preparation 失效
标题翻译：防水剂及其制备方法
公开(公告)号：US5328683A
公开(公告)日：1994-07-12
申请号：US85809
申请日：1993-07-06
申请人： Asao Harashima
发明人： Asao Harashima
IPC分类号： A61K8/18 , A61K8/11 , A61K8/26 , A61K8/58 , A61Q1/00 , A61Q1/02 , A61Q1/12 , C08K9/06 , C08L83/04 , C09C1/36 , C09C3/12 , C09D7/12 , C09D11/02 , C09D11/03 , C09D183/00 , C09D183/02 , C09K3/18 , A61K7/021
CPC分类号： B82Y30/00 , A61K8/0241 , A61K8/585 , A61Q1/02 , A61Q1/12 , C09C1/3684 , C09C3/12 , A61K2800/412 , A61K2800/621 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2004/80 , C01P2004/84 , C01P2006/20 , C01P2006/90
摘要： A water repellent powdered material and a method of making the powder in which the powdered material is mixed with an organic solvent solution of a triorganosiloxysilicic acid having the formula (R.sub.3 SiO.sub.1/2).sub.2 nSiO.sub.2 in which R is a monovalent hydrocarbon radical such as alkyl, aryl, and alkenyl; and n is an integer having a value of one to five; with the acid being present in an amount of from 0.1 to 20 parts by weight per one hundred parts by weight of the powdered material. The powder can be used to formulate cosmetic foundations.
摘要翻译：一种防水粉末材料及其制造方法，其中粉末材料与具有式（R3SiO1 / 2）2nSiO2的三有机硅氧硅酸的有机溶剂溶液混合，其中R是一价烃基，例如烷基，芳基和烯基; n为1〜5的整数，酸的存在量为每100重量份粉末材料0.1至20重量份。该粉末可用于配制化妆品基础。

7. 发明授权

US5045584A Polish containing silicone elastomer particles 失效
标题翻译：波兰含有硅氧烷弹性体颗粒
公开(公告)号：US5045584A
公开(公告)日：1991-09-03
申请号：US431123
申请日：1989-11-03
申请人： Atushi Sasaki , Asao Harashima , Keiji Yoshida
发明人： Atushi Sasaki , Asao Harashima , Keiji Yoshida
IPC分类号： C09G1/00 , C09G1/12
CPC分类号： C09G1/12
摘要： A polish including a film forming wax material and an organopolysiloxane elastomer. The elastomer is in the form of particles mixed with the film forming wax. The particles are spherical and have an average diameter of from about 0.3 um to about 30 um. The polish contains at least one additive selected from the group consisting of organic solvents, silicone oils, and surfactants. The film forming wax material may be one of carnauba wax, montan wax, candelilla wax, ceresin wax, paraffin waxes, and beeswax.
摘要翻译：包括成膜蜡材料和有机聚硅氧烷弹性体的抛光剂。弹性体是与成膜蜡混合的颗粒的形式。颗粒是球形的并且具有约0.3μm至约30μm的平均直径。抛光剂含有至少一种选自有机溶剂，硅油和表面活性剂的添加剂。成膜蜡材料可以是巴西棕榈蜡，褐煤蜡，小烛树蜡，纯地蜡，石蜡和蜂蜡中的一种。

8. 发明授权

US08835555B2 Method for producing emulsion 有权
标题翻译：生产乳液的方法
公开(公告)号：US08835555B2
公开(公告)日：2014-09-16
申请号：US13140858
申请日：2009-12-21
申请人： Kazuhiko Kojima , Tsutomu Naganawa , Asao Harashima
发明人： Kazuhiko Kojima , Tsutomu Naganawa , Asao Harashima
IPC分类号： C08J3/03 , C08G77/46
CPC分类号： C08J3/03 , C08G77/46 , C08J2383/04
摘要： The present invention has an objective to easily obtain an emulsion exhibiting superior storage stability, and in particular, an emulsion of a polyorganosiloxane. The present invention provides a method for producing an emulsion characterized by obtaining an emulsion by emulsifying a mixture of an oil and a surfactant, obtained by synthesizing the surfactant in the oil. In particular, the method is suitably used for the preparation of an emulsion of an organopolysiloxane (A) which is usually difficult to be stably emulsified. A silicone-based surfactant (B), and in particular, a silicone-based surfactant having a small degree of polymerization of a siloxane chain such as a trisiloxane is synthesized in an oil. Thereby, an emulsion exhibiting superior storage stability can be produced.
摘要翻译：本发明的目的是容易地获得表现出优异的储存稳定性的乳液，特别是聚有机硅氧烷的乳液。本发明提供了一种乳液的制造方法，其特征在于，通过将表面活性剂在油中合成而得到的油和表面活性剂的混合物乳化得到乳液。特别地，该方法适合用于制备通常难以稳定乳化的有机聚硅氧烷（A）的乳液。在油中合成有机硅系表面活性剂（B），特别是硅氧烷链聚合度低的硅氧烷系表面活性剂，例如三硅氧烷。由此，可以制造出具有优异的储存稳定性的乳液。

9. 发明授权

US5696192A Organopolysiloxane bearing polyoxyalkylene bonded to silicon across alkylene and method of preparation 失效
标题翻译：带有聚亚烷基氧基的聚氧化硅与亚烷基结合，制备方法
公开(公告)号：US5696192A
公开(公告)日：1997-12-09
申请号：US749451
申请日：1996-11-15
申请人： Asao Harashima
发明人： Asao Harashima
IPC分类号： C08K5/00 , C08G65/32 , C08G77/34 , C08G77/46 , C08K3/32 , C08K3/38 , C08K5/098 , C08K5/15 , C08L71/00 , C08L71/02 , C08L83/04 , C08L83/05 , C08L83/07 , C08L83/12 , C08K5/06
CPC分类号： C08K3/38 , C08G77/46 , C08K3/32 , C08K5/098
摘要： A polyoxyalkylene-modified organopolysiloxane that generates almost no odor with the passage of time, and a method for preparation of the polyoxyalkylene-modified organopolysiloxane. This organopolysiloxane bears polyoxyalkylene bonded to silicon across alkylene, and contains 5-1,000 ppm by weight of an antioxidant. It also has a peroxide value not exceeding 5 meq/kg, and a total content of aldehyde plus ketone not exceeding 100 ppm.
摘要翻译：随着时间的推移几乎不产生气味的聚氧化烯改性的有机聚硅氧烷，以及聚氧化烯改性的有机聚硅氧烷的制备方法。该有机聚硅氧烷在与亚烷基结合的硅上承载聚氧化烯，含有5-1000重量ppm的抗氧化剂。其过氧化值不超过5meq / kg，醛加酮的总含量不超过100ppm。

10. 发明授权

US4980167A Silicone cosmetic composition 失效
标题翻译：硅胶化妆品组合物
公开(公告)号：US4980167A
公开(公告)日：1990-12-25
申请号：US469859
申请日：1990-01-24
申请人： Asao Harashima , Keiji Yoshida
发明人： Asao Harashima , Keiji Yoshida
IPC分类号： A61K8/55 , A61K8/58 , A61K8/72 , A61K8/89 , A61K8/891 , A61Q1/00 , A61Q1/02 , A61Q1/04 , A61Q1/06 , A61Q1/12 , A61Q19/00 , C08L83/04
CPC分类号： A61Q19/00 , A61K8/891 , A61Q1/02 , A61Q1/06 , Y10S514/845 , Y10S514/847
摘要： The cosmetic composition of the present invention exhibits excellent lubricancy since it contains silicone rubber powder containing 0.50-80 wt % of silicone oil. When it is coated on the skin, no foreign sensations or irritations are reported. A smooth and moist texture is obtained.

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