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1. 发明授权

US06359128B1 Free-flowing flakes of vinyl caprolactam monomer and process for making same 失效
标题翻译：乙烯基己内酰胺单体的自由流动薄片及其制备方法
公开(公告)号：US06359128B1
公开(公告)日：2002-03-19
申请号：US09618395
申请日：2000-07-18
申请人： Arvind M. Mathur , James A. Dougherty , Philip F. Wolf
发明人： Arvind M. Mathur , James A. Dougherty , Philip F. Wolf
IPC分类号： C07D22310
CPC分类号： C07D223/10
摘要： Free-flowing flakes of vinyl caprolactam monomer usable below its melting point of 34° C. without developing coloration.
摘要翻译：乙烯基己内酰胺单体的自由流动薄片可以在其熔点为34℃以下使用，而不会显色

2. 发明授权

US5468820A Reactive diluent for radiation curing of film-forming polymers 失效
标题翻译：用于成膜聚合物辐射固化的活性稀释剂
公开(公告)号：US5468820A
公开(公告)日：1995-11-21
申请号：US182870
申请日：1994-01-14
申请人： James A. Dougherty , Philip F. Wolf
发明人： James A. Dougherty , Philip F. Wolf
IPC分类号： C08F2/46 , A61C13/00 , A61C13/07 , C08F2/54 , C08F26/00 , C08F220/10 , C08F220/12 , C08F226/02 , C08F226/06 , C08F290/00 , C08F290/02 , C09D4/00 , C09D4/02
CPC分类号： C08F220/12 , A61C13/0024 , A61C13/0025 , C08F226/02 , C08F226/06
摘要： This invention relates to a reactive diluent mixture employed in a free radical polymerization of film-forming monomers which comprises between about 25 and about 90 wt. % N-vinyl lactam containing 6 to 9 carbon atoms and between about 10 and about 75 wt. % of a non-cyclic vinyl amide having from 3 to 7 carbon atoms which is employed in a concentration of between about 10 and about 50 wt. % based on total film forming monomers.
摘要翻译：本发明涉及用于成膜单体的自由基聚合的反应性稀释剂混合物，其包含约25至约90wt。含有6至9个碳原子的N-乙烯基内酰胺和约10至约75重量％％的具有3至7个碳原子的非环状乙烯基酰胺，其浓度为约10至约50重量％。基于总成膜单体的％。

3. 发明授权

US6011160A Crosslinked polyvinylpyrrolidone (PVPP) copolymer of vinyl pyrrolidone (VP) and monomer derived from 1-vinyl-3-(E)-ethylidene pyrrolidone (EVP) 失效
公开(公告)号：US6011160A
公开(公告)日：2000-01-04
申请号：US932893
申请日：1997-09-18
申请人： Edward G. Malawer , Victor Kabanov , Kolazi S. Narayanan , Michael A. Tallon , Susan Y. Tseng , Philip F. Wolf
发明人： Edward G. Malawer , Victor Kabanov , Kolazi S. Narayanan , Michael A. Tallon , Susan Y. Tseng , Philip F. Wolf
IPC分类号： C07D207/26 , C08F26/06 , G07D13/00 , G07D207/09 , G07D207/12
CPC分类号： C07D207/26 , C08F26/06
摘要： What is described herein is a crosslinked polyvinylpyrrolidone (PVPP) copolymer of vinyl pyrrolidone (VP) and monomer derived from 1-vinyl-3-(E)-ethylidene pyrrolidone (EVP).

4. 发明授权

US5654385A One-step process for making lightly-crosslinked polyvinylpyrrolidone hydrogel 失效
标题翻译：制备轻度交联的聚乙烯吡咯烷酮水凝胶的一步法
公开(公告)号：US5654385A
公开(公告)日：1997-08-05
申请号：US648789
申请日：1996-05-16
申请人： Susan Y. Tseng , Philip F. Wolf , Thomas E. Royster
发明人： Susan Y. Tseng , Philip F. Wolf , Thomas E. Royster
IPC分类号： C08F2/00 , C08F226/10
CPC分类号： C08F226/10
摘要： A one-step for making a lightly-crosslinked polyvinylpyrrolidone hydrogel by polymerizing vinyl pyrrolidone in water in the presence of a suitable crosslinker such as 1-vinyl-3(E)-ethylidene pyrrolidone and a free radical initiator under initial agitation conditions sufficient to overcome the inertia of the polymer when formed.
摘要翻译：在适当的交联剂例如1-乙烯基-3（E） - 亚乙基吡咯烷酮和自由基引发剂的存在下，在足够克服的初始搅拌条件下，通过在水中聚合乙烯基吡咯烷酮在水中制备轻度交联的聚乙烯吡咯烷酮水凝胶的一个步骤聚合物形成时的惯性。

5. 发明授权

US5604275A Color stabilized aqueous n-vinyl heterocyclic copolymer solutions 失效
标题翻译：颜色稳定的N-乙烯基杂环共聚物水溶液
公开(公告)号：US5604275A
公开(公告)日：1997-02-18
申请号：US534753
申请日：1995-09-27
申请人： Yuanzhen Zhong , Philip F. Wolf
发明人： Yuanzhen Zhong , Philip F. Wolf
IPC分类号： C08F226/06 , C08K5/00 , C08K5/35
CPC分类号： C08F226/06 , C08K5/0091
摘要： This invention relates to an N-vinyl heterocyclic copolymer in substantially pure deionized water or in aqueous alcoholic solution which exhibits significantly reduced color and odor and which is obtained by contacting an alcohol-copolymer mixture with water and a nitrogen containing, trivalent boron complex compound selected from the group of borane-ammonia, borane-lower alkylamine, tetra-lower alkyl ammonium octahydrotriborate, morpholine-borane, lower alkyl morpholine-borane, silylamino borane and mixtures thereof and stripping alcohol from the resulting mixture under vacuum at between about 100 and about 740 mm Hg below absolute whereby an aqueous, 10-70 wt. % solids solution of the copolymer is obtained having a water white color stability of more than a year.
摘要翻译：本发明涉及基本上纯的去离子水或含水醇溶液中的N-乙烯基杂环共聚物，其表现出显着降低的颜色和气味，并且是通过使醇共聚物混合物与水和含氮的三价硼配位化合物接触而获得的从硼烷 - 氨，硼烷 - 低级烷基胺，四氢低级烷基铵八氢五氟硼酸盐，吗啉 - 硼烷，低级烷基吗啉 - 硼烷，甲硅烷基氨基硼烷及其混合物组合，并在真空下从约100至约低于绝对值740毫米汞柱，由此得到10-70重量％得到具有大于一年的水白色稳定性的共聚物的固体％固体溶液。

6. 发明授权

US5912312A Homogeneous copolymers containing vinyl pyrrolidone and 2-methylene-1,3-dioxepane and process for making same 失效
标题翻译：含有乙烯基吡咯烷酮和2-亚甲基-1,3-二氧杂环庚烷的均相共聚物及其制备方法
公开(公告)号：US5912312A
公开(公告)日：1999-06-15
申请号：US71841
申请日：1998-05-01
申请人： Yuanzhen Zhong , Philip F. Wolf , Edward G. Malawer , Kolazi S. Narayanan
发明人： Yuanzhen Zhong , Philip F. Wolf , Edward G. Malawer , Kolazi S. Narayanan
IPC分类号： C08F226/10 , C08F26/08
CPC分类号： C08F226/10
摘要： Homogeneous copolymers of 60-99 mole % of vinyl pyrrolidone (VP) and 1-40 mole % 2-methylene-1,3-dioxepane (MDO), preferably 85-95 mole % VP and 5-10 mole % MDO, having a K-value of about 30-50, and a Tg of about 124-138.degree. C., are described herein. The copolymers are hydrolytically degradable in aqueous acid or basic solutions and biodegradable.
摘要翻译： 60-99摩尔％乙烯基吡咯烷酮（VP）和1-40摩尔％2-亚甲基-1,3-二氧杂环庚烷（MDO），优选85-95摩尔％VP和5-10摩尔％MDO的均相共聚物具有 K值约30-50，Tg约124-138℃。共聚物在酸性或碱性溶液中可水解降解，可生物降解。

7. 发明授权

US5663258A Strongly swellable, moderately crosslinked copolymers of vinylpyrrolidone and vinyl acetate 失效
标题翻译：乙烯基吡咯烷酮和乙酸乙烯酯的强溶胀中等交联共聚物
公开(公告)号：US5663258A
公开(公告)日：1997-09-02
申请号：US603668
申请日：1996-02-20
申请人： Yuanzhen Zhong , Philip F. Wolf
发明人： Yuanzhen Zhong , Philip F. Wolf
IPC分类号： C08F226/10 , C08F218/08
CPC分类号： C08F226/10
摘要： Strongly swellable, moderately crosslinked poly(vinyl pyrrolidone/vinyl acetate) copolymer (XL-PVP/VA) in the form of fine, white powders characterized by (a) an aqueous gel volume of about 15 to 150 ml/g of polymer, (b) a Brookfield viscosity in 5% aqueous solution of at least about 10,000 cps, and (c) being prepared directly by precipitation polymerization of VP and VA monomers in the presence of a crosslinking agent in the amount of about 0.1 to about 2% by weight of VP and VA.
摘要翻译：强溶胀性，中等交联的聚（乙烯基吡咯烷酮/乙酸乙烯酯）共聚物（XL-PVP / VA），其为细的白色粉末，其特征在于（a）约15至150ml / g聚合物的水凝胶体积， b）至少约10,000cps的5％水溶液中的布鲁克菲尔德粘度，和（c）直接通过在约0.1至约2％量的交联剂存在下VP和VA单体的沉淀聚合制备， VP和VA的重量。

8. 发明授权

US5614583A Homogenized flowable hydrogel of crosslinked N-vinyl lactam polymer 失效
标题翻译：交联的N-乙烯基内酰胺聚合物的均匀流动性水凝胶
公开(公告)号：US5614583A
公开(公告)日：1997-03-25
申请号：US528383
申请日：1995-09-13
申请人： Susan Y. Tseng , Jui-Chang Chuang , Philip F. Wolf
发明人： Susan Y. Tseng , Jui-Chang Chuang , Philip F. Wolf
IPC分类号： A61K8/04 , A61K8/365 , A61K8/368 , A61K8/81 , A61K9/16 , A61K9/70 , A61K31/19 , A61K31/194 , A61K31/20 , A61K31/60 , A61K47/32 , A61Q5/00 , A61Q5/08 , A61Q19/00 , A61Q19/02 , C08J3/075 , A61K9/14 , C08L39/06
CPC分类号： A61Q19/00 , A61K31/19 , A61K31/194 , A61K31/20 , A61K31/60 , A61K8/0204 , A61K8/042 , A61K8/365 , A61K8/368 , A61K8/8176 , A61K8/8182 , A61K2800/75 , A61Q19/02 , A61Q5/08
摘要： This invention relates to a crosslinked N-vinyl lactam polymer in the form of a stable, homogenized flowable hydrogel having microparticles which can be passed through a screen of between about 40 and about 350 mesh size. The invention also concerns the process for the preparation of the homogenized gel and to its use as a hair and skin conditioner or as a carrier for a cosmetically or pharmaceutically active substance.
摘要翻译：本发明涉及一种具有稳定，均质的可流动水凝胶形式的交联的N-乙烯基内酰胺聚合物，其具有可以通过约40至约350目尺寸的筛网的微粒。本发明还涉及制备均质化凝胶的方法及其用作头发和皮肤调理剂或作为化妆品或药学活性物质的载体的用途。

9. 发明授权

US5360883A Process for obtaining a polymerizable reaction solution 失效
标题翻译：获得可聚合反应溶液的方法
公开(公告)号：US5360883A
公开(公告)日：1994-11-01
申请号：US40400
申请日：1993-03-30
申请人： Susan Y. Tseng , Philip F. Wolf
发明人： Susan Y. Tseng , Philip F. Wolf
IPC分类号： C07D207/38 , C08F226/06 , C08F226/10
CPC分类号： C08F226/06 , C07D207/38
摘要： What is provided herein is a process for obtaining a polymerizable reaction solution which includes 5-30% by weight of a crosslinker which is the isomeric compound 1-vinyl-3(E)-ethylidene pyrrolidone and 50-80% by weight of a monomer which is vinylpyrrolidone. The polymerizable solution can be used to make crosslinked polyvinylpyrrolidone rapidly upon heating the solution at about 80.degree.-120.degree. C. in the absence of base.
摘要翻译：本文提供的是一种获得可聚合反应溶液的方法，其包含5-30重量％的交联剂，其为异构化合物1-乙烯基-3（E） - 亚乙基吡咯烷酮和50-80重量％的单体它是乙烯基吡咯烷酮。在不存在碱的情况下，在约80-120℃下加热溶液，可聚合溶液可用于快速制备交联聚乙烯吡咯烷酮。

10. 发明授权

US4524224A Hydrolysis of alkylene carbonates to aklylene glycols 失效
标题翻译：将碳酸亚烷基酯水解成亚磷酰二醇
公开(公告)号：US4524224A
公开(公告)日：1985-06-18
申请号：US495462
申请日：1983-05-20
申请人： Glenn A. Taylor , Philip F. Wolf
发明人： Glenn A. Taylor , Philip F. Wolf
IPC分类号： C07C29/12 , B01J27/00 , B01J27/232 , C07C27/00 , C07C29/09 , C07C31/20 , C07C67/00 , C07C31/12
CPC分类号： C07C29/095 , Y02P20/52
摘要： This invention is concerned with producing glycols of the formulaHOCHRCH.sub.2 OHfrom hydrolysis, in a homogeneous liquid phase mixture, of an alkylene carbonate of the formula ##STR1## in which R is either hydrogen or methyl. This is accomplished by using an amount of water in excess of stoichiometry and using potassium carbonate as the preferred catalyst. The reaction is effected under a carbon dioxide pressure of at least 80 psig and the reaction temperature is desirably between about 85.degree. C. and 500.degree. C.
摘要翻译：本发明涉及通过水解在均相液相混合物中制备式HOCHRCH 2 OH的二醇，其中R为氢或甲基的式“IMAGE”的亚烷基碳酸酯。这通过使用一定量的超过化学计量的水并使用碳酸钾作为优选的催化剂来实现。反应在至少80psig的二氧化碳压力下进行，反应温度优选在约85℃至500℃之间。

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