会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 8. 发明申请
    • SYNTHESIS OF LITHIUM-METAL-PHOSPHATES UNDER HYDROTHERMAL CONDITIONS
    • 在氢热条件下合成硫酸金属磷酸盐
    • US20110272639A1
    • 2011-11-10
    • US13142606
    • 2009-12-22
    • Kirill BramnikHartmut HibstJordan Keith LampertSimon Schroedle
    • Kirill BramnikHartmut HibstJordan Keith LampertSimon Schroedle
    • H01M4/58H01B1/12H01B1/18H01M4/04H01B1/14
    • C01B25/45H01M4/5825H01M4/625H01M10/0525
    • The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bM1bQ1-cM2cPd-eM3eOx (l), wherein Q has the oxidation state +2 and M1, M2, M3, a, b, c, d, e and x are: Q: Fe, Mn, Co, Ni, M1: Na, K, Rb and/or Cs, M2: Mg, Al, Ca, Ti, Co, Ni, Cr, V, Fe, Mn, wherein Q and M2 are different from each other, M3: Si, S, F a: 0.8-1.9, b: 0-0.3, c: 0-0.9, d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of Li, M1, M2, P, M3, wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one Q-comprising compound, in which Q has at least partially an oxidation state higher than +2, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and/or least one M3-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, and (B) heating the mixture obtained in step (A) at a temperature of 100 to 500° C. and at an autogeneous pressure to reduce Q to oxidation state +2 and to obtain a compound of general formula (I).
    • 本发明涉及制备通式(I)Lia-bM1bQ1-cM2cPd-eM3eOx(1)的化合物的方法,其中Q具有氧化态+2和M1,M2,M3,a,b,c, d,e和x为:Q:Fe,Mn,Co,Ni,M1:Na,K,Rb和/或Cs,M2:Mg,Al,Ca,Ti,Co,Ni,Cr,V,Fe,Mn 其中Q和M2彼此不同,M3:Si,S,F a:0.8-1.9,b:0-0.3,c:0-0.9,d:0.8-1.9,e:0-0.5,x: 取决于Li,M1,M2,P,M3的量和氧化态,其中通式(I)的化合物是中性带电的,包括以下步骤(A),提供包含至少一种锂 - 包含化合物,至少一种含Q的化合物,其中Q至少部分具有高于+2的氧化态,以及至少一种含M1化合物(如果存在)和/或至少一种含M2化合物,如果 存在和/或至少一种含M3化合物(如果存在)和至少一种被氧化成至少一种化合物c的还原剂 处于氧化态+5以上的至少一个磷原子,(B)在100〜500℃的温度和自动压力下加热步骤(A)中得到的混合物,将Q降低至氧化态+2,将 得到通式(I)的化合物。
    • 10. 发明申请
    • PROCESS FOR THE PREPARATION OF LIFEPO4-CARBON COMPOSITES
    • 制备LIFEPO4-碳复合材料的方法
    • US20120097901A1
    • 2012-04-26
    • US13379048
    • 2010-06-23
    • Simon SchroedleHartmut HibstBrian RobertsKirill BramnikJordan Keith Lampert
    • Simon SchroedleHartmut HibstBrian RobertsKirill BramnikJordan Keith Lampert
    • H01B1/04C04B35/64C04B35/52
    • H01M4/5825C01B25/45C01B25/455H01B1/24H01M4/131H01M4/1315H01M4/133H01M4/485H01M4/505H01M4/525H01M4/583H01M10/0525Y02E60/122
    • The present invention relates to a process for the preparation of particles comprising at least one compound according to general formula (I) M1aM2bM3cOoNnFf (I) wherein M1, M2, M3 O, N, F, a, b, c, o, n and f have the following meanings: M1 at least one alkaline metal, M2 at least one transition metal in oxidation state +2, M3 at least one non-metal chosen form S, Se, P, As, Si, Ge and/or B, O oxygen, N nitrogen, F fluorine, a 0.8-4.2, b 0.8-1.9, c 0.8-2.2, o 1.0-8.4, n 0-2.0 and f 0-2.0, wherein a, b, c, o, n and f are chosen to ensure electroneutrality of the compound according to general formula (I), and carbon, comprising at least the following steps: (A) providing an essentially aqueous mixture comprising at least one compound comprising M1, at least one compound comprising M2 having at least partially an oxidation state higher than +2, optionally at least one compound comprising M3, at least one compound comprising N, if present, and/or at least one compound comprising F, if present, at least one polysaccharide comprising glucose having a molecular weight M of at least 50000 g/mol as carbon precursor and at least one reducing agent, (B) drying the mixture provided in step (A), in order to obtain a solid particle and (C) calcining the solid particle obtained from step (B) at a temperature of 300 to 950° C.
    • 本发明涉及一种制备颗粒的方法,所述颗粒包含至少一种根据通式(I)的M1aM2bM3cOoNnFf(I)的化合物,其中M1,M2,M3O,N,F,a,b,c,o,n和 f具有以下含义:M1至少一种碱金属,M2至少一种氧化态过渡金属+2,M3至少一种非金属选择形式S,Se,P,As,Si,Ge和/或B, O氧,N氮,F氟,0.8-4.2,b 0.8-1.9,c 0.8-2.2,o 1.0-8.4,n 0-2.0和f 0-2.0,其中a,b,c,o,n和 选择f以确保根据通式(I)的化合物和至少包括以下步骤的碳的电中性:(A)提供基本上含水的混合物,其包含至少一种包含M1的化合物,至少一种包含M2的化合物,其包含具有 至少部分地高于+2的氧化态,任选地至少一种包含M3的化合物,至少一种包含N的化合物(如果存在)和/或至少一种包含F的化合物 送出至少一种包含分子量M至少为50000g / mol的葡萄糖作为碳前体和至少一种还原剂的至少一种多糖,(B)干燥步骤(A)中提供的混合物,以获得固体颗粒 和(C)在300-950℃的温度下煅烧由步骤(B)得到的固体颗粒。