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1. 发明专利

JP2010077024A Method for safely filling carbon nanotube, filling system and industrial plant employing the method 有权
标题翻译：碳纳米管填充方法，填充系统及使用方法的工业厂房
公开(公告)号：JP2010077024A
公开(公告)日：2010-04-08
申请号：JP2009292159
申请日：2009-12-24
申请人： Arkema France , アルケマフランス
发明人： BORDERE SERGE , GAILLARD PATRICE
IPC分类号： C01B31/02 , B65B1/06 , B65D90/00
CPC分类号： B65B1/16 , B65B1/28 , B65G69/182 , B65G69/183 , Y10T137/87925
摘要： PROBLEM TO BE SOLVED: To provide a method for filling with carbon nanotubes (CNT) by transferring from one container (106) to another container (200) through a coupling (300) comprising a double-valve device (30).
SOLUTION: The method is applied to the packaging of CNTs in containers, in which one valve is coupled to one container; each valve (31, 32) is independently closed and sealed; and only when both the valves are coupled, the double-valve device is opened.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：解决的问题：提供一种通过包括双阀装置（30）的联接器（300）从一个容器（106）转移到另一容器（200）来填充碳纳米管（CNT）的方法。
解决方案：该方法适用于容器中CNT的包装，其中一个阀联接到一个容器; 每个阀（31,32）被独立地封闭并密封; 并且只有当两个阀联接时，双阀装置打开。版权所有（C）2010，JPO＆INPIT

2. 发明专利

JP2009184911A Method for safely filling with carbon nanotube, filling system and industrial plant employing the method 审中-公开
标题翻译：碳纳米管充填方法，充填系统和采用该方法的工业厂房
公开(公告)号：JP2009184911A
公开(公告)日：2009-08-20
申请号：JP2009022088
申请日：2009-02-03
申请人： Arkema France , アルケマフランス
发明人： BORDERE SERGE , GAILLARD PATRICE
IPC分类号： C01B31/02 , B65B1/16 , B65B1/32 , B65D90/62 , B65D90/64
CPC分类号： B65B1/16 , B65B1/28 , B65G69/182 , B65G69/183 , Y10T137/87925
摘要： PROBLEM TO BE SOLVED: To provide an industrial method for safely filling a receptacle with carbon nanotubes (CNT) from another receptacle, to provide a filling system employing the method, and to provide a plant for the safe packaging of carbon nanotubes, which is equipped with the filling system. SOLUTION: Disclosed is a method for filling a receptacle (200) with carbon nanotubes (CNT) from another receptacle (106) whereby the CNTs are passed from one receptacle (106) to the other (200) by means of a coupling (300) comprising a double-valve device (30), each of the valves (31, 32) being coupled to one of the receptacles, the valves (31, 32) being closed independently and being openable only when they are coupled to one another. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种用于从另一个容器安全地用碳纳米管（CNT）填充容器的工业方法，以提供采用该方法的填充系统，并提供用于碳纳米管的安全包装的设备，配有灌装系统。解决方案：公开了一种用于从另一容器（106）向碳纳米管（CNT）填充容器（200）的方法，由此通过联接器将CNT从一个容器（106）传递到另一个（106）（300）包括双阀装置（30），每个所述阀（31,32）联接到所述容器之一，所述阀（31,32）独立地关闭，并且仅当它们联接到一个另一个。版权所有（C）2009，JPO＆INPIT

3. 发明专利

JP2008255006A Method of producing carbon nanotube using renewable raw material 审中-公开
标题翻译：使用可再生原料生产碳纳米管的方法
公开(公告)号：JP2008255006A
公开(公告)日：2008-10-23
申请号：JP2008099647
申请日：2008-04-07
申请人： Arkema France , アルケマフランス
发明人： BORDERE SERGE , COCHARD DANIEL , DUTILH ERIC , GAILLARD PATRICE , LOZOWSKI ANDRE , PLEE DOMINIQUE
IPC分类号： C01B31/02 , B01J23/745 , C10J1/213
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162
摘要： PROBLEM TO BE SOLVED: To provide a method of producing carbon nanotubes using renewable raw materials. SOLUTION: The method of producing carbon nanotubes comprising the following stages: (a) the synthesis of alcohol by fermentation of at least one vegetable material and the purification of the product obtained, (b) the dehydration of the alcohol obtained in (a) in order to produce, in a first reactor 3, a mixture of an alkene and water and optionally the purification of the product obtained, (c) the introduction in a second reactor 7, in particular the introduction into a fluidized bed, of a powdery catalyst at a temperature ranging from 450 to 850°C, this catalyst comprising at least one catalytic metal supported by an inert solid substrate, the grains of catalyst having a d50 of less than 300 μm, (d) bringing the alkene produced in (b) into contact with the powdery catalyst of stage (c), optionally in a fluidized bed, in order to form carbon nanotubes and hydrogen on the surface of the catalyst by catalytic decomposition of the alkene, and (e) the recovery of the carbon nanotubes produced in (d). COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供使用可再生原料生产碳纳米管的方法。解决方案：制备碳纳米管的方法包括以下步骤：（a）通过至少一种植物材料的发酵合成醇并纯化所获得的产物，（b）将（ a）为了在第一反应器3中生产烯烃和水的混合物，并任选地纯化得到的产物，（c）在第二反应器7中引入，特别是引入流化床，在450〜850℃的温度范围内的粉末状催化剂，该催化剂含有至少一种由惰性固体基质担载的催化剂金属，催化剂颗粒的d50小于300μm，（d）将生成的烯烃（b）任选地在流化床中与阶段（c）的粉末状催化剂接触，以便通过催化分解烯烃在催化剂的表面上形成碳纳米管和氢，和（e）回收碳纳米管在（d）中生产。版权所有（C）2009，JPO＆INPIT

4. 发明专利

JP2010281024A Method for producing conductive composite fiber having high nanotube ratio 审中-公开
标题翻译：用于生产具有高纳米比率的导电复合纤维的方法
公开(公告)号：JP2010281024A
公开(公告)日：2010-12-16
申请号：JP2010119151
申请日：2010-05-25
申请人： Arkema France , Centre National De La Recherche Scientifique , アルケマフランス , サントル・ナショナル・ドゥ・ラ・ルシェルシュ・シャンティフィクCentre National De La Recherche Scientifique
发明人： GAILLARD PATRICE , POULIN PHILIPPE , MERCADIER CELIA , MAUGEY MARYSE , MOISAN SANDY , DERRE ALAIN , ZAKRI CECILE
IPC分类号： D01F6/50 , C08J5/06 , D01D1/02
CPC分类号： D01F1/09 , D01F6/14
摘要： PROBLEM TO BE SOLVED: To provide conductive composite fibers based on a vinyl alcohol homo- or copolymer, containing thermal and/or electrical conductivity-imparting nanotube especially carbon nanotube at a high ratio.
SOLUTION: The conductive composite fibers are provided by stabilizing nanotube dispersed in a vinyl alcohol homo- or copolymer solution by using a stabilizer, injecting the dispersion liquid into a coagulation solution to form pre-fibers, and washing and drying.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供基于乙烯醇均聚物或共聚物的导电复合纤维，其以高比率含有导热性和/或导电性纳米管，特别是碳纳米管。解决方案：导电复合纤维通过使用稳定剂将分散在乙烯醇均聚物或共聚物溶液中的纳米颗粒稳定化，将分散液注入凝固溶液中以形成预纤维，并进行洗涤和干燥来提供。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2010222581A Process for preparing thermosetting composite material with high nanotube content 有权
标题翻译：制备具有高纳米含量的热固性复合材料的方法
公开(公告)号：JP2010222581A
公开(公告)日：2010-10-07
申请号：JP2010066078
申请日：2010-03-23
申请人： Arkema France , アルケマフランス
发明人： KORZHENKO ALEXANDER , MIAUDET PIERRE , MERCERON AMELIE , GAILLARD PATRICE
IPC分类号： C08J3/22 , B29B7/90 , B29B9/12 , C08K3/04 , C08L101/00
CPC分类号： B82Y30/00 , B29K2105/167 , C08J3/226 , C08J5/005 , C08J5/24 , C08J2363/00 , C08J2463/00 , C08K3/04 , C08K7/24 , C08L63/00
摘要： PROBLEM TO BE SOLVED: To provide a process for preparing a composite material containing from 15 to 60 wt.% of nanotubes, an obtained composite material, use of the same in production of a composite product. SOLUTION: The process for preparing the composite material comprising: (a) introducing a liquid polymer composition comprising at least one thermosetting resin in a liquid state, nanotubes and optionally a rheology modifier into a compounding device, (b) mixing the polymer composition and the nanotubes within the device, to form a composite material, and (c) a step of recovering the composite material, optionally after forming the same to pellets. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种制备复合材料的方法，所述复合材料含有15至60重量％的纳米管，所得复合材料在复合产品的制备中使用。制备复合材料的方法包括：（a）将液体聚合物组合物引入液态聚合物组合物中，所述组合物包含液态的至少一种热固性树脂，纳米管和任选的流变改性剂至配混装置中，（b）将聚合物组合物和装置内的纳米管，以形成复合材料，和（c）任选地在将复合材料形成颗粒之后回收复合材料的步骤。版权所有（C）2011，JPO＆INPIT

6. 发明公开

KR20200133765A 함침된 섬유 재료의 웹, 그 제조 방법 및 3 차원 복합 부품의 제조를 위한 그 용도 审中-公开
公开(公告)号：KR20200133765A
公开(公告)日：2020-11-30
申请号：KR20207029728
申请日：2019-03-19
申请人： ARKEMA FRANCE
发明人： SAVART THIBAUT , HOCHSTETTER GILLES , FLORENCIE ANTHONY , GAILLARD PATRICE , SALINIER AXEL , BABEAU ARTHUR PIERRE
IPC分类号： B29B15/12 , B29C70/06 , B29C70/38 , B29K67/00 , B29K77/00 , B29K105/08 , B29K105/12 , B29K307/04
摘要： 따라서, 본발명은서로에대해적층및/또는결합되는섬유재료(들)의 N 개의개별테이프를포함하는함침된섬유재료(들)의웹에관한것으로, 상기 N 개의테이프는서로부착되고적어도부분적으로중첩될수 있다. 본발명에따르면, 섬유재료(들)의테이프는적어도하나의열가소성중합체, 및선택적으로사슬연장제로함침된연속섬유를포함한다. 웹은섬유들축에수직인단면에서표면 S 를가지며, 이표면 S 는 S th 로나타내는, 각초기개별테이프의, 섬유들축에수직인단면에서의표면의합과실질적으로동일하고, S th 는 N x l x Ep 과동일하며, 여기서 l 는테이프의평균폭을나타내고 Ep는테이프의평균두께를나타내고, N은 2 내지 2000 이며, 각개별테이프의평균두께는 150 ㎛이하, 바람직하게는 100 ㎛이하, 특히 10 내지 100 ㎛인 것을웹은특징으로한다.

7. 发明公开

KR20200135413A 두께가 100 마이크로미터 이하인 열가소성 중합체로 함침된 섬유 재료 및 그의 제조 방법 审中-公开
公开(公告)号：KR20200135413A
公开(公告)日：2020-12-02
申请号：KR20207029727
申请日：2019-03-19
申请人： ARKEMA FRANCE
发明人： HOCHSTETTER GILLES , SAVART THIBAUT , BABEAU ARTHUR PIERRE , FLORENCIE ANTHONY , GAILLARD PATRICE , SALINIER AXEL
IPC分类号： C08J5/24 , C08J5/04
摘要： 본발명은함침된섬유재료에관한것으로서, 연속섬유로이루어진적어도하나의섬유재료및: 적어도하나의비반응성열가소성중합체매트릭스, 또는선택적으로사슬연장제와혼합되는, 상기비반응성열가소성중합체의전구체인, 적어도하나의반응성열가소성예비중합체를포함하고, 상기적어도하나의비반응성열가소성중합체또는상기반응성예비중합체는유리전이온도가 Tg ≥ 80℃, 특히 Tg ≥ 100℃, 특히≥ 120℃, 보다특히≥ 140℃인 비정질중합체또는예비중합체이거나, 또는용융온도 Tf ≥ 150℃인 반결정질중합체또는예비중합체이고, 상기예비함침된섬유재료에서섬유함량은 45 내지 65 부피%, 바람직하게는 50 내지 60 부피%, 특히 54 내지 60 부피% 이고, 상기함침된섬유재료의평균두께는, 함침전상기섬유재료에존재하는섬유의수와무관하게, 100 ㎛이하인것을특징으로한다.

8. 发明申请

WO2012066241A2 METHOD FOR PRODUCING FIBROUS MATERIALS PRE-IMPREGNATED WITH A THERMOHARDENABLE POLYMER 审中-公开
标题翻译：用热稳定聚合物预先制备纤维材料的方法
公开(公告)号：WO2012066241A2
公开(公告)日：2012-05-24
申请号：PCT/FR2011052670
申请日：2011-11-17
申请人： ARKEMA FRANCE , GAILLARD PATRICE , HAVEL MICKAEL , KORZHENKO ALEXANDER
发明人： GAILLARD PATRICE , HAVEL MICKAEL , KORZHENKO ALEXANDER
IPC分类号： B29B15/12 , B29C70/00 , B29C70/02 , B82Y30/00 , C08J3/24 , C08J5/24
CPC分类号： B32B37/02 , B29B15/12 , B29B15/125 , B29C70/025 , B29K2105/167 , B82Y30/00 , C08J3/242 , C08J5/24 , D06M11/74 , D06M15/55
摘要： The invention relates to a method for producing a fibrous material comprising carbon fibres or glass fibres or plant fibres or polymer-based fibres, that are used alone or in a mixture, and are impregnated by a thermohardenable polymer or a mixture of thermohardenable polymers, using a mixture containing a hardener and carbon nanofillers, such as carbon nanotubes (CNT). According to the invention, a mixture containing said nanofillers, such as CNTs, and the hardener is used to introduce said nanofillers, such as CNTs, into the fibrous material. The pre-impregnated fibrous materials are used to produce parts with a three-dimensional structure.
摘要翻译：本发明涉及一种用于生产包含碳纤维或玻璃纤维或植物纤维或聚合物基纤维的纤维材料的方法，其单独使用或混合使用，并且由可热固化的聚合物或可热硬化聚合物的混合物浸渍，使用含有碳纳米管（CNT）的固化剂和碳纳米填料的混合物。根据本发明，使用含有纳米填料（例如CNT）和硬化剂的混合物将所述纳米填料如CNTs引入纤维材料中。预浸渍的纤维材料用于制造具有三维结构的部件。

9. 发明申请

WO2011020970A3 SUPPORTED FE/MO CATALYST, PROCESS FOR PREPARING SAME AND USE FOR THE MANUFACTURE OF NANOTUBES 审中-公开
标题翻译：支持的FE / MO催化剂，其制备方法和用于制造纳米管的方法
公开(公告)号：WO2011020970A3
公开(公告)日：2011-04-14
申请号：PCT/FR2010051716
申请日：2010-08-16
申请人： ARKEMA FRANCE , INST NAT POLYTECHNIQUE , GAILLARD PATRICE , BORDERE SERGE , COCHARD DANIEL , SERP PHILIPPE , CAUSSAT BRIGITTE , BEAUSOLEIL JULIEN
发明人： GAILLARD PATRICE , BORDERE SERGE , COCHARD DANIEL , SERP PHILIPPE , CAUSSAT BRIGITTE , BEAUSOLEIL JULIEN
IPC分类号： B01J23/881 , B01J37/02 , C01B31/02
CPC分类号： B01J35/023 , B01J21/04 , B01J23/881 , B01J37/0201 , B82Y30/00 , B82Y40/00 , C01B32/162
摘要： The invention relates to a catalyst material for preparing nanotubes, especially carbon nanotubes, said material being in the form of solid particles, said particles comprising a porous substrate having a BET specific surface area of greater than 50 m2/g, preferably between 70 and 400 m2/g, covered with at least one catalytic layer of a mixture of iron and molybdenum, said catalytic layer representing from 30% to 70%, preferably from 40 to 55% by weight of the total weight of the catalyst material, the iron content being at least 25%, preferably from 30% to 40% by weight of the total weight of the catalyst material, and the iron/molybdenum weight ratio being between 11 and 1.5, preferably between 5 and 2. The invention also relates to the process for preparing same and to a process for the synthesis of CNTs using this catalyst material.
摘要翻译：本发明涉及用于制备纳米管，尤其是碳纳米管的催化剂材料，所述材料为固体颗粒形式，所述颗粒包含BET比表面积大于50m 2 / g，优选70-400 用至少一层铁和钼的混合物的催化层覆盖，所述催化层占催化剂材料总重量的30％至70％，优选40至55％，铁含量为催化剂材料总重量的至少25重量％，优选30重量％-40重量％，铁/钼重量比为11-1.5，优选5-2。本发明还涉及该方法用于制备它们以及使用该催化剂材料合成CNT的方法。

10. 发明申请

WO2015121584A2 METHOD OF MANUFACTURING A FIBROUS MATERIAL PREIMPREGNATED WITH THERMOPLASTIC POLYMER USING AN AQUEOUS DISPERSION OF POLYMER 审中-公开
标题翻译：使用聚合物的水分散体制备用热塑性聚合物预处理的纤维材料的方法
公开(公告)号：WO2015121584A2
公开(公告)日：2015-08-20
申请号：PCT/FR2015050332
申请日：2015-02-11
申请人： ARKEMA FRANCE
发明人： GAILLARD PATRICE , HOCHSTETTER GILLES , SAVART THIBAUT
IPC分类号： B29B15/12 , B29C70/50 , B29K101/12
CPC分类号： B29C70/504 , B29B15/12 , B29B15/125 , B29K2101/12 , B29K2105/08 , B29K2507/04 , B29L2007/007
摘要： The invention relates to a method of manufacturing a preimpregnated fibrous material comprising a fibrous material of continuous fibres and a thermoplastic polymer matrix, characterized in that said preimpregnated fibrous material is produced as a unidirectional single tape or a plurality of unidirectional parallel tapes and in that said method comprises the following steps: i) a step of impregnating said fibrous material while it is in the form of several parallel rovings, said impregnation step comprising: ia) immersing said fibrous material in a bath containing an aqueous dispersion (22) of said thermoplastic polymer, said immersion being followed by ib) a drying (25) of said fibrous material, then ii) a step of shaping said parallel rovings of said fibrous material impregnated according to step i) by calendering using at least one heated calender (51, 52, 53) into the form of a plurality of unidirectional parallel tapes using said heated calender comprising a plurality of calendering grooves (73), preferably up to 200 calendering grooves, according to the number of said tapes and with a pressure and/or separation between the rolls (71, 75) of said calender regulated by a control system.
摘要翻译：本发明涉及一种制造预浸渍纤维材料的方法，其包括连续纤维和热塑性聚合物基质的纤维材料，其特征在于，所述预浸渍纤维材料被制成单向单条带或多个单向平行带，并且所述方法包括以下步骤：i）当所述纤维材料呈几个平行粗纱的形式时浸渍所述纤维材料的步骤，所述浸渍步骤包括：ia）将所述纤维材料浸入含有所述热塑性塑料的水分散体（22）的浴中聚合物，所述浸渍之后是ib）所述纤维材料的干燥（25），然后ii）根据步骤i）浸渍的所述纤维材料的平行粗纱的成型步骤是通过使用至少一个加热的压延机（51， 52,53）形成多个单向平行带的形式，使用包括多个压延机的所述加热压延机根据所述带的数量以及由控制系统调节的所述压延机的辊（71,75）之间的压力和/或间隔，优选地多达200个压延槽。

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