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1. 发明授权

US5504251A Co-cracking of BPA and phenol process tars 失效
标题翻译： BPA和苯酚过程焦油的共裂化
公开(公告)号：US5504251A
公开(公告)日：1996-04-02
申请号：US401732
申请日：1995-03-09
申请人： Arkady S. Dyckman , Andrey V. Zinenkov , Boris I. Gorovits , Valentina Y. Shefter , John W. Fulmer , William D. Kight
发明人： Arkady S. Dyckman , Andrey V. Zinenkov , Boris I. Gorovits , Valentina Y. Shefter , John W. Fulmer , William D. Kight
IPC分类号： C07B63/02 , C07C7/148 , C07C15/085 , C07C15/44 , C07C37/00 , C07C37/52 , C07C37/86 , C07C39/04 , C07C37/68
CPC分类号： C07C7/148 , C07C37/52 , Y02P20/127
摘要： This invention relates to processing of a mixture of tars produced in phenol manufacture and in bisphenol manufacture. The heating of a bottom liquid from a bisphenol-A process together with phenol tar from in a cumene-to-phenol process in a distillation column-type thermal cracking reactor at 290.degree.-360.degree. C. at a mass ratio of 1:(1-10) is employed. The process is carried out by feed entering into the middle of the column and valuable products removed as overhead.
摘要翻译：本发明涉及在酚制造和双酚制造中生产的焦油混合物的加工。在蒸馏塔型热裂解反应器中，在290℃-360℃以1：3的质量比将来自双酚A工艺的底部液体与苯酚焦油一起从异丙苯到苯酚方法加热 1-10）。该过程由进入塔中部的饲料进行，有价值的产物作为塔顶除去。

2. 发明授权

US5457244A Phenol tar waste reduction process 失效
标题翻译：酚类焦油废物减少过程
公开(公告)号：US5457244A
公开(公告)日：1995-10-10
申请号：US330149
申请日：1994-10-04
申请人： Arkadys S. Dyckman , John Fulmer , William D. Kight , Andrey Zinenkov , Vadim P. Boyarsky , Boris I. Gorovits , Leontii M. Krasnov , Alexander S. Malinovski , Yury I. Petrov , Anatoly D. Sorokin , Sergey N. Chernukhin
发明人： Arkadys S. Dyckman , John Fulmer , William D. Kight , Andrey Zinenkov , Vadim P. Boyarsky , Boris I. Gorovits , Leontii M. Krasnov , Alexander S. Malinovski , Yury I. Petrov , Anatoly D. Sorokin , Sergey N. Chernukhin
IPC分类号： C07C27/12 , C07C37/50 , C07C37/74 , C07C37/86 , C07C39/04 , C07C49/78 , C07C37/68
CPC分类号： C07C37/86
摘要： An improved phenol tar cracking process using a rectification column as a hydrocracker obtains an increased yield of valuable products, phenol, cumene and alpha-methylstyrene, by taking from 50 to 100% of the acetophenone in the reactor overhead with the cracked product stream.
摘要翻译：使用精馏塔作为加氢裂化器的改进的苯酚焦油裂解方法通过在裂化产物流中在反应器塔顶馏出物中的50至100％的苯乙酮获得有价值的产物，苯酚，枯烯和α-甲基苯乙烯的产率。

3. 发明授权

US4626600A Process for purifying acetone 失效
标题翻译：丙酮纯化方法
公开(公告)号：US4626600A
公开(公告)日：1986-12-02
申请号：US703990
申请日：1985-02-21
申请人： John W. Fulmer , William D. Kight
发明人： John W. Fulmer , William D. Kight
IPC分类号： C07C45/53 , C07C45/80 , C07C45/81 , C07C45/82
CPC分类号： C07C45/81 , C07C45/53 , C07C45/80 , C07C45/82
摘要： In accordance with the invention there is a process for reducing the water content of acetone prepared from cumene which includes the steps ofa. adding cleaving effective catalytic quantities of sulfuric acid to a mixture comprising cumene hydroperoxide and cumene, the cumene hydroperoxide making up about 81 to 83 weight percent of the said mixture, thereby producing a mixture comprising phenol, acetone, cumene and sulfuric acid;b. neutralizing the said sulfuric acid with an aqueous alkali hydroxide and separating the alkali metal sulfate from the mixture comprising phenol, acetone, water and cumene, the water being from about 40 to 60 weight percent of the total weight of water and cumene, the cumene being present in sufficient quantities to cause the formation of two liquid phases upon condensing the acetone fraction distillate;c. separating by distillation the acetone fraction from the phenol fraction, said acetone fraction containing acetone, water, aldehyde, and other organics including cumene;d. condensing the said acetone fraction, the said acetone fraction separating into two phases, the bottom phase having a substantial portion of the water and aldehyde present in the said acetone fraction, the upper phase having a substantial portion of the cumene of the said acetone fraction, the acetone being partitioned between the bottom phase and the upper phase;e. recycling at least a portion of the bottom phase to the vessel in which the sulfuric acid is neutralized andf. processing the upper phase to achieve a separation of the acetone and water.
摘要翻译：根据本发明，存在一种降低由枯烯制备的丙酮的水含量的方法，其包括以下步骤：a。向包含氢过氧化异丙苯和异丙基苯的混合物中加入有效催化量的硫酸，氢过氧化异丙苯占所述混合物的约81-83％（重量），从而产生包含苯酚，丙酮，异丙基苯和硫酸的混合物; b。用碱金属氢氧化物中和所述硫酸，并从包括苯酚，丙酮，水和枯烯的混合物中分离出碱金属硫酸盐，水为水和异丙基苯的总重量的约40至60重量％，枯烯为存在足够的量以在冷凝丙酮馏分馏出物时形成两个液相; C。通过蒸馏从苯酚馏分中蒸馏出丙酮馏分，所述丙酮馏分含有丙酮，水，醛和其它有机物，包括枯烯; d。将所述丙酮馏分冷凝，将所述丙酮馏分分离成两相，底相具有存在于所述丙酮馏分中的大部分水和醛，上部相具有所述丙酮馏分的枯烯的相当大部分，丙酮被分配在底相和上相之间; e。将至少一部分底部相转移到其中硫酸中和的容器中。加工上相以实现丙酮和水的分离。

4. 发明授权

US5510543A Removal and neutralization of acid catalyst from products of cumene hydroperoxide cleavage 失效
标题翻译：从氢过氧化枯烯裂解产物中除去和中和酸催化剂
公开(公告)号：US5510543A
公开(公告)日：1996-04-23
申请号：US353004
申请日：1994-12-09
申请人： John W. Fulmer , Andrei K. Griaznov , William D. Kight , Vladimir M. Zakoshansky
发明人： John W. Fulmer , Andrei K. Griaznov , William D. Kight , Vladimir M. Zakoshansky
IPC分类号： C07C37/08 , C07C37/68 , C07C37/72 , C07C39/04 , C10C1/00
CPC分类号： C07C37/72 , C07C37/86 , Y02P20/52
摘要： The present invention is an improved method for the recovery of phenol from a cleavage mass resulting from the sulfuric acid cleavage of cumene hydroperoxide comprising neutralizing the cleavage mass, forming an aqueous phase and an organic phase, separating the organic phase into an acetone-rich stream and a phenol-rich stream, removing phenol tars from the phenol-rich stream and cracking the phenol tars wherein the improvement comprises maintaining the pH of the cleavage mass during neutralization between 4.0 and about 4.9 whereby the sulfuric acid is converted to the bisulfate salt and substantially no free sulfuric acid remains in the cleavage mass and corrosion of process equipment is reduced.As a result of this improved process, a phenol tar waste stream containing less than about 4 parts per million by weight of chromium is obtained.
摘要翻译：本发明是一种改进的方法，用于从由氢过氧化枯烯的硫酸裂解产生的裂解物质中回收苯酚，包括中和裂解物质，形成水相和有机相，将有机相分离成富含丙酮的物流和富酚的物流，从富酚流中除去酚焦油并裂解苯酚焦碳，其中改进包括在中和期间保持裂解物质的pH在4.0至约4.9之间，由此将硫酸转化为硫酸氢盐，并且在裂解物质中基本上不残留游离硫酸，并减少了工艺设备的腐蚀。作为这种改进方法的结果，获得了含有小于约4重量％的铬的酚焦油废液流。

5. 发明授权

US5908962A Cumene oxidation process 失效
标题翻译：枯烯氧化过程
公开(公告)号：US5908962A
公开(公告)日：1999-06-01
申请号：US20395
申请日：1998-02-09
申请人： Vladimir Mikhailovich Zakoshansky , Andrei Konstantinovich Griaznov , Irina I. Vasilieva , John W. Fulmer , William D. Kight
发明人： Vladimir Mikhailovich Zakoshansky , Andrei Konstantinovich Griaznov , Irina I. Vasilieva , John W. Fulmer , William D. Kight
IPC分类号： C07C407/00 , C07C409/10
CPC分类号： C07C409/10 , C07C407/00
摘要： Greater efficiency in a water-alkaline emulsion cumene oxidation process using a cascade of reactors is obtained by splitting the reactor cascade into 2 stages with the first stage utilizing NH.sub.4 NaCO.sub.3 as the active carbonate in the stage containing less than 18% by weight cumene hydroperoxide and using Na.sub.2 CO.sub.3 as the active carbonate in the stage containing more than 18% by weight cumene hydroperoxide. By directly injecting ammonia into a recycle stream organic acids are efficiently neutralized. A counter current water wash of the second stage also increases process efficiency by scrubbing out unwanted impurities. Control of pH in the process improves efficiency and reduces impurity levels.
摘要翻译：在使用级联反应器的水 - 碱性乳液异丙苯氧化过程中，通过将反应器级联分为两个阶段获得更高的效率，其中第一阶段利用NH 4 NaCO 3作为活性碳酸酯在含有少于18重量％氢过氧化枯烯的阶段中使用在含有超过18重量％氢过氧化枯烯的阶段中，作为活性碳酸钠的Na 2 CO 3。通过将氨直接注入循环流中，有机酸被有效地中和。第二阶段的逆流水洗还通过洗去不需要的杂质来提高工艺效率。该过程中pH值的控制可提高效率并降低杂质浓度。

6. 发明授权

US5767322A Cumene oxidation process 失效
公开(公告)号：US5767322A
公开(公告)日：1998-06-16
申请号：US670304
申请日：1996-06-27
申请人： Vladimir Mikhailovich Zakoshansky , Andrei Konstantinovich Griaznov , Irina I. Vasilieva , John W. Fulmer , William D. Kight
发明人： Vladimir Mikhailovich Zakoshansky , Andrei Konstantinovich Griaznov , Irina I. Vasilieva , John W. Fulmer , William D. Kight
IPC分类号： C07C407/00 , C07C409/10
CPC分类号： C07C409/10 , C07C407/00
摘要： Greater efficiency in a water-alkaline emulsion cumene oxidation process using a cascade of reactors is obtained by splitting the reactor cascade into 2 stages with the first stage utilizing NH.sub.4 NaCO.sub.3 as the active carbonate in the stage containing less than 18% by weight cumene hydroperoxide and using Na.sub.2 CO.sub.3 as the active carbonate in the stage containing more than 18% by weight cumene hydroperoxide. By directly injecting ammonia into a recycle stream organic acids are efficiently neutralized. A counter current water wash of the second stage also increases process efficiency by scrubbing out unwanted impurities. Control of pH in the process improves efficiency and reduces impurity levels.

7. 发明授权

US5355238A Method and apparatus for the monitoring and demarcation of synchronous optical networks 失效
标题翻译：用于同步光网络监控和划分的方法和装置
公开(公告)号：US5355238A
公开(公告)日：1994-10-11
申请号：US108338
申请日：1993-08-18
申请人： William D. Kight , Robert E. Pfister
发明人： William D. Kight , Robert E. Pfister
IPC分类号： H04B10/08 , H04J3/00 , H04J3/12 , H04J3/14 , H04J3/16 , H04Q11/04 , H04J14/08
CPC分类号： H04J3/14 , H04J3/12 , H04J3/1611 , H04J2203/0048 , H04J2203/0057
摘要： A method and apparatus for establishing an intelligent demarcation between facility and terminal segments of a synchronous optical network. Network management information contained with the overhead structure of the synchronous optical network signal is extracted and manipulated in accordance with a predetermined user specification; overhead data may be translated, terminated, or passed unaltered as required. Overhead processing towards the facility and terminal segments need not be symmetrical. Payload information is passed unaltered although future provisions for encrypting payload data exist. Full performance monitoring is supported along with a built-in-test and diagnostic capability. The device may be both locally and remotely controlled and monitored. Remote control is implemented via the overhead information contained within the synchronous optical network signal.
摘要翻译：一种用于在同步光网络的设备和终端段之间建立智能分界的方法和装置。根据预定的用户规格提取并操纵包含在同步光网络信号的开销结构中的网络管理信息; 开销数据可以根据需要进行翻译，终止或传递。对设备和终端段的开销处理不需要对称。尽管有效载荷数据的加密存在未来的规定，但是有效载荷信息仍然被改变。支持全性能监控以及内置测试和诊断功能。该设备可以在本地和远程控制和监视。通过同步光网络信号中包含的开销信息实现远程控制。

8. 发明授权

US5623357A Method and apparatus for the monitoring and demarcation of synchronous digital hierarchy networks 失效
标题翻译：用于同步数字分层网络监控和划分的方法和装置
公开(公告)号：US5623357A
公开(公告)日：1997-04-22
申请号：US475529
申请日：1995-06-07
申请人： William D. Kight , Robert E. Pfister
发明人： William D. Kight , Robert E. Pfister
IPC分类号： H04B10/08 , H04J3/00 , H04J3/12 , H04J3/14 , H04J3/16 , H04Q11/04 , H04J14/08
CPC分类号： H04J3/14 , H04J3/12 , H04J3/1611 , H04J2203/0048 , H04J2203/0057 , Y10S370/907
摘要： A method and apparatus for establishing an intelligent demarcation between facility and terminal segments of asynchronous optical network. Network management information contained with the overhead structure of the synchronous optical network signal is extracted and manipulated in accordance with a predetermined user specification; overhead data may be translated, terminated, or passed unaltered as required. Overhead processing towards the facility and terminal segments need not be symmetrical. Payload information is passed unaltered although future provisions for encrypting payload data exist. Full performance monitoring is supported along with a built-in-test and diagnostic capability. The device may be both locally and remotely controlled and monitored. Remote control is implemented via the overhead information contained within the synchronous optical network signal.
摘要翻译：一种用于在异步光网络的设备和终端段之间建立智能分界的方法和装置。根据预定的用户规格提取并操纵包含在同步光网络信号的开销结构中的网络管理信息; 开销数据可以根据需要进行翻译，终止或传递。对设备和终端段的开销处理不需要对称。尽管有效载荷数据的加密存在未来的规定，但是有效载荷信息仍然被改变。支持全性能监控以及内置测试和诊断功能。该设备可以在本地和远程控制和监视。通过同步光网络信号中包含的开销信息实现远程控制。

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