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1. 发明申请

US20060246344A1 Supports for fuel cell catalysts 有权
标题翻译：支持燃料电池催化剂
公开(公告)号：US20060246344A1
公开(公告)日：2006-11-02
申请号：US11415358
申请日：2006-05-01
申请人： Ion Halalay , Belabbes Merzougui , Michael Carpenter , Swathy Swathirajan , Gregory Garabedian , Andrew Mance , Mei Cai
发明人： Ion Halalay , Belabbes Merzougui , Michael Carpenter , Swathy Swathirajan , Gregory Garabedian , Andrew Mance , Mei Cai
IPC分类号： H01M4/96
CPC分类号： H01M4/921 , H01M4/8605 , H01M4/8647 , H01M4/92 , H01M4/925 , H01M4/926 , H01M8/08 , H01M8/083 , H01M8/086 , H01M8/1007 , H01M2004/8689 , H01M2008/1095
摘要： The durability of a fuel cell having a polymer electrolyte membrane with an anode on one surface and an oxygen-reducing cathode on the other surface is improved by substituting electrically conductive titanium carbide or titanium nitride particles for carbon particles as oxygen-reducing and hydrogen-oxidizing catalyst supports. For example nanosize platinum particles deposited on nanosize titanium carbide or titanium nitride support particles provide good oxygen reduction capability and are corrosion resistant in an acid environment. It is preferred that the catalyst-on-titanium carbide (nitride) particles be mixed with non-catalyst-bearing carbon in the electrode material for improved electrode performance,
摘要翻译：通过用导电碳化钛或氮化钛颗粒代替碳颗粒作为氧还原和氢氧化来改善具有在一个表面上具有阳极的聚合物电解质膜和另一表面上的除氧阴极的燃料电池的耐久性催化剂载体。例如，沉积在纳米尺寸碳化钛或氮化钛载体颗粒上的纳米级铂颗粒提供良好的氧还原能力，并且在酸性环境中具有耐腐蚀性。优选的是，碳化钛（氮化物）颗粒与电极材料中的不含催化剂的碳混合以改善电极性能，

2. 发明申请

US20060222920A1 Metal cations chelators for fuel cells 审中-公开
标题翻译：用于燃料电池的金属阳离子螯合剂
公开(公告)号：US20060222920A1
公开(公告)日：2006-10-05
申请号：US11097112
申请日：2005-04-01
申请人： Belabbes Merzougui , Andrew Mance , Ion Halalay
发明人： Belabbes Merzougui , Andrew Mance , Ion Halalay
IPC分类号： H01M8/10 , H01M4/86
CPC分类号： H01M8/1039 , H01M8/0289 , H01M8/1023
摘要： A fuel cell having a polymer electrolyte membrane containing fluorine atoms distributed along the polymer chains, and metal conductors and/or catalysts. The cell is protected from metal ion degradation of cell components, especially the polymer electrolyte, by a metal ion sequestering or chelating agent fixed in the cell or flowing through the cell. In a preferred embodiment, the metal ion-sequestering agent comprises a suitable number of metal ion-binding molecular crown moieties attached to polymer constituents in the electrolyte membrane or in electrodes.
摘要翻译：具有聚合物电解质膜的燃料电池，其具有沿聚合物链分布的氟原子，以及金属导体和/或催化剂。通过金属离子螯合剂或螯合剂固定在电池中或流过电池来保护电池免受电池组分，特别是聚合物电解质的金属离子降解。在优选的实施方案中，金属离子螯合剂包含与电解质膜或电极中的聚合物组分相连的适当数量的金属离子结合分子冠部分。

3. 发明申请

US20060046120A1 Constituents and methods for protecting fuel cell components, including PEMS 有权
标题翻译：保护燃料电池组件的成分和方法，包括PEMS
公开(公告)号：US20060046120A1
公开(公告)日：2006-03-02
申请号：US10929190
申请日：2004-08-30
申请人： Belabbes Merzougui , Andrew Mance , Tao Xie , Ion Halalay
发明人： Belabbes Merzougui , Andrew Mance , Tao Xie , Ion Halalay
IPC分类号： H01M8/04 , H01M8/10
CPC分类号： H01M4/8605 , H01M8/02 , H01M8/0273 , H01M8/04223 , H01M2008/1095
摘要： A fuel cell comprising a membrane electrode assembly (MEA) that is made up of a membrane sandwiched between first and second electrodes, a contaminant peroxide, damaging to the MEA, and at least one constituent with the contaminant peroxide that prevents, or at least inhibits, decomposition of at least one of the first electrode, the second electrode, the membrane, and any combination thereof.
摘要翻译：一种燃料电池，包括由夹在第一和第二电极之间的膜构成的膜电极组件（MEA），对MEA有损害的过氧化物污染物，以及至少一种具有防止或至少抑制，第一电极，第二电极，膜中的至少一个的分解及其任何组合。

4. 发明申请

US20060222921A1 Fluoride ion scavenger for fuel cell components 有权
公开(公告)号：US20060222921A1
公开(公告)日：2006-10-05
申请号：US11097457
申请日：2005-04-01
申请人： Andrew Mance , Belabbes Merzougui , Ion Halalay
发明人： Andrew Mance , Belabbes Merzougui , Ion Halalay
IPC分类号： H01M8/10
CPC分类号： H01M8/1023 , H01M4/8605 , H01M4/8652 , H01M8/1004 , H01M8/1039 , H01M8/1051
摘要： A fuel cell having a polymer electrolyte membrane containing fluorine atoms distributed along the polymer chains, and metal conductors and/or catalysts, is protected from fluoride ion degradation of the metal components by a fluoride ion sequestering agent fixed in the cell or flowing through the cell. In a preferred embodiment, the fluoride ion scavenger comprises a suitable number of azacrown moieties attached to polymer constituents in the electrolyte membrane or in electrodes.

5. 发明申请

US20060251954A1 Conductive matrices for fuel cell electrodes 有权
标题翻译：燃料电池电极导电基体
公开(公告)号：US20060251954A1
公开(公告)日：2006-11-09
申请号：US11415346
申请日：2006-05-01
申请人： Belabbes Merzougui , Ion Halalay , Michael Carpenter , Swathy Swathirajan
发明人： Belabbes Merzougui , Ion Halalay , Michael Carpenter , Swathy Swathirajan
IPC分类号： H01M4/96 , H01M8/10 , H01M4/92
CPC分类号： H01M4/90 , H01M4/86 , H01M4/9075 , H01M4/92 , H01M4/925 , H01M8/1004 , H01M2004/8689 , H01M2008/1095
摘要： The durability of a fuel cell having a polymer electrolyte membrane with an anode on one surface and an oxygen-reducing cathode on the other surface is improved by replacing conductive carbon matrix materials in an electrode with a matrix of electrically conductive metal compound particles. The electrode includes a catalyst supported on a nanosize metal oxides and electrically conductive nanosize matrix particles of a metal compound. One or more metal compounds such as a boride, carbide, nitride, silicide, carbonitride, oxyboride, oxycarbide, or oxynitride of a metal such as cobalt, chromium, nickel, molybdenum, neodymium niobium, tantalum, titanium, tungsten, vanadium, and zirconium is suitable. For example, the combination of platinum particles deposited on titanium dioxide support particles mixed in a conductive matrix of titanium carbide particles provides an electrode with good oxygen reduction capability and corrosion resistance in an acid environment.
摘要翻译：通过用导电金属化合物颗粒的基体代替电极中的导电性碳基体材料，改善了具有在一个表面上具有阳极的聚合物电解质膜和另一表面上的除氧阴极的燃料电池的耐久性。电极包括负载在纳米尺寸金属氧化物上的催化剂和金属化合物的导电纳米尺寸基质颗粒。金属如钴，铬，镍，钼，钕，铌，钽，钛，钨，钒和锆的一种或多种金属化合物，例如硼化物，碳化物，氮化物，硅化物，碳氮化物，氧硼化物，碳氧化物或氧氮化物适合。例如，沉积在二氧化钛载体颗粒上的铂颗粒的组合在碳化钛颗粒的导电基质中混合提供了在酸性环境中具有良好的氧还原能力和耐腐蚀性的电极。

6. 发明申请

US20070080055A1 Metallic reagent 有权
标题翻译：金属试剂
公开(公告)号：US20070080055A1
公开(公告)日：2007-04-12
申请号：US11230047
申请日：2005-09-19
申请人： Andrew Mance , Tao Xie , Belabbes Merzougui
发明人： Andrew Mance , Tao Xie , Belabbes Merzougui
IPC分类号： C23C14/32
CPC分类号： B01J23/755
摘要： A reagent suitable for use as a catalyst comprises a first metal species substrate having a second reduced metal species coated thereon, the second reduced metal species being less electropositive than the first metal. Methods of manufacture are also provided.
摘要翻译：适合用作催化剂的试剂包括其上涂覆有第二还原金属物质的第一金属物质基质，第二还原金属物质比第一金属具有更低的正电性。还提供了制造方法。

7. 发明申请

US20070066828A1 Method for making nitrogen aromatic oligomers and polymers 失效
标题翻译：制备氮芳烃低聚物和聚合物的方法
公开(公告)号：US20070066828A1
公开(公告)日：2007-03-22
申请号：US11230046
申请日：2005-09-19
申请人： Andrew Mance , Tao Xie , Belabbes Merzougui , Charlene Hayden
发明人： Andrew Mance , Tao Xie , Belabbes Merzougui , Charlene Hayden
IPC分类号： C07D213/22 , C07D403/00 , C08G73/06
CPC分类号： C08G73/0633 , C07D213/22 , C08G61/12 , C08G73/06 , C08G73/0627
摘要： Methods for synthesizing dimeric or higher polymeric reaction products of nitrogen aromatics comprise contacting a composition comprising the nitrogen aromatic with a catalyst composition. The catalyst is in particulate form and comprises a first metal substrate having a second reduced metal coated on the substrate.
摘要翻译：合成氮芳烃的二聚或更高级聚合反应产物的方法包括将包含氮芳族化合物的组合物与催化剂组合物接触。催化剂是颗粒形式，并且包括具有涂覆在基材上的第二还原金属的第一金属基材。

8. 发明授权

US09252431B2 Fuel cell catalyst with metal oxide/phosphate support structure and method of manufacturing same 有权
标题翻译：具有金属氧化物/磷酸盐载体结构的燃料电池催化剂及其制造方法
公开(公告)号：US09252431B2
公开(公告)日：2016-02-02
申请号：US13147375
申请日：2009-02-10
申请人： Belabbes Merzougui , Tetsuo Kawamura
发明人： Belabbes Merzougui , Tetsuo Kawamura
IPC分类号： H01M4/92 , B01J21/06 , B01J23/89 , H01M4/88 , B01J21/18 , B01J37/02 , H01M4/90
CPC分类号： H01M4/8803 , B01J21/18 , B01J23/89 , B01J37/024 , H01M4/9008 , H01M4/92 , Y02E60/50
摘要： A fuel cell supported catalyst includes an underlying support structure having at least one of a metal oxide and a metal phosphate. Catalyst particles are arranged onto and in engagement with the support structure. An intermediate conductive, corrosion-resistant layer, such as boron-doped-diamond, is arranged onto and in engagement with the support structure to surround the catalyst particles. The supported catalyst is produced by depositing the intermediate layer onto the support structure after the catalyst particles have been deposited on the underlying support structure, in one example. In another example, voids are provided in the intermediate layer, which has been deposited onto the underlying support structure, to subsequently receive the catalyst particles.
摘要翻译：燃料电池负载催化剂包括具有金属氧化物和金属磷酸盐中的至少一种的下面的支撑结构。催化剂颗粒被布置在支撑结构上并与支撑结构接合。中间导电耐腐蚀层，例如硼掺杂金刚石，布置在支撑结构上并与载体结构接合以围绕催化剂颗粒。在一个实例中，在将催化剂颗粒沉积在下面的支撑结构上之后，通过将中间层沉积到载体结构上来制备负载的催化剂。在另一个实例中，在已经沉积到下面的支撑结构上的中间层中提供空隙以随后接收催化剂颗粒。

9. 发明授权

US08389175B2 Fuel cell having a stabilized cathode catalyst 有权
标题翻译：具有稳定的阴极催化剂的燃料电池
公开(公告)号：US08389175B2
公开(公告)日：2013-03-05
申请号：US12867162
申请日：2008-05-16
申请人： Minhua Shao , Belabbes Merzougui , Patrick L. Hagans , Susanne M. Opalka
发明人： Minhua Shao , Belabbes Merzougui , Patrick L. Hagans , Susanne M. Opalka
IPC分类号： H01M4/02 , H01M4/36 , H01M4/92 , H01M8/00 , H01M8/10 , B01J23/00
CPC分类号： H01M4/8647 , H01M4/921 , H01M8/086 , H01M8/1007 , H01M2008/1095 , Y02E60/521 , Y10S977/773 , Y10S977/775
摘要： A fuel cell (70) having an anode (72), a cathode (78) and an electrolyte (76) between the anode (72) and the cathode (78) includes a cathode catalyst (80) formed of a plurality of nanoparticles. Each nanoparticle (20) has a plurality of terraces (26) formed of platinum surface atoms (14), and a plurality of edge (28) and corner regions (29) formed of atoms from a second metal (30)—The cathode catalyst may be formed by combining a platinum nanoparticle with a metal salt in a solution. Ions from the second metal react with platinum and replace platinum atoms on the nanoparticle. The second metal atoms at the corner and edge regions of the nanoparticle, as well as at any surface defects, result in a more stable catalyst structure. In some embodiments, the fuel cell (70) is a proton exchange membrane fuel cell and the nanoparticles are tetrahedron-shaped. In some embodiments, the fuel cell (70) is a phosphoric acid fuel cell and the nanoparticles are cubic-shaped.
摘要翻译：在阳极（72）和阴极（78）之间具有阳极（72），阴极（78）和电解质（76）的燃料电池（70）包括由多个纳米颗粒形成的阴极催化剂（80）。每个纳米颗粒（20）具有由铂表面原子（14）形成的多个梯田（26），以及由第二金属（30）的原子形成的多个边缘（28）和拐角区域（29）。阴极催化剂可以通过将铂纳米颗粒与溶液中的金属盐组合而形成。来自第二金属的离子与铂反应并且替换纳米颗粒上的铂原子。在纳米颗粒的角落和边缘区域的第二个金属原子以及任何表面缺陷导致更稳定的催化剂结构。在一些实施例中，燃料电池（70）是质子交换膜燃料电池，并且纳米颗粒是四面体形状。在一些实施例中，燃料电池（70）是磷酸燃料电池，并且纳米颗粒是立方体形状。

10. 发明授权

US08304365B2 Stabilized platinum catalyst 有权
标题翻译：稳定的铂催化剂
公开(公告)号：US08304365B2
公开(公告)日：2012-11-06
申请号：US12867153
申请日：2008-05-16
申请人： Minhua Shao , Belabbes Merzougui , Patrick L. Hagans , Susanne M. Opalka
发明人： Minhua Shao , Belabbes Merzougui , Patrick L. Hagans , Susanne M. Opalka
IPC分类号： B01J23/00 , H01M8/00
CPC分类号： B01J35/0013 , B01J23/42 , B01J23/56 , B01J37/0226 , B01J37/347 , B01J37/348
摘要： A stabilized platinum nanoparticle has a core portion surrounded by a plurality of outer surfaces. The outer surfaces include terrace regions formed of platinum atoms, and edge and corner regions formed of atoms from a second metal. The stabilized nanoparticle may be formed by combining a platinum nanoparticle with a metal salt in a solution. Ions of the second metal react with platinum and replace platinum atoms on the nanoparticle. Platinum atoms from the edge and corner regions react with the second metal ions quicker than surface atoms from the terraces, due to a greater difference in electrode potential between the platinum atoms at the edge and corner regions, as compared to the second metal in the solution. The platinum nanoparticle may include surface defects, such as steps and kinks, which may also be replaced with atoms of the second metal. In an exemplary embodiment, the platinum nanoparticle is a cathode catalyst in an electro-chemical cell.
摘要翻译：稳定的铂纳米颗粒具有由多个外表面包围的芯部分。外表面包括由铂原子形成的平台区域，以及由第二金属原子形成的边缘和拐角区域。稳定的纳米颗粒可以通过将铂纳米颗粒与溶液中的金属盐组合而形成。第二金属的离子与铂反应，并取代纳米颗粒上的铂原子。由于与溶液中的第二金属相比，在边缘和拐角区域处的铂原子与边缘和角部区域上的铂原子之间的电极电位差异更大，所以来自边缘和角区域的铂原子与第二金属离子比来自梯田的表面原子更快地反应。铂纳米颗粒可以包括表面缺陷，例如步骤和扭结，其也可以被第二金属的原子替代。在示例性实施方案中，铂纳米颗粒是电化学电池中的阴极催化剂。

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