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1. 发明申请

US20090221846A1 METHOD FOR PRODUCING ISOCYANATES 有权
标题翻译：生产异氰酸酯的方法
公开(公告)号：US20090221846A1
公开(公告)日：2009-09-03
申请号：US12065964
申请日：2006-08-23
申请人： Andreas Wölfert , Carsten Knösche , Andreas Daiss , Tsung-Chieh Cheng , Torsten Mattke , Eckhard Stroefer
发明人： Andreas Wölfert , Carsten Knösche , Andreas Daiss , Tsung-Chieh Cheng , Torsten Mattke , Eckhard Stroefer
IPC分类号： C07C263/10 , B01J19/24
CPC分类号： C07C263/10 , B01F5/0453 , B01F5/0456 , B01F5/0466 , B01F5/0646 , B01F5/0652 , B01J19/26 , C07C265/14 , C07C265/12
摘要： The present invention relates to a process for preparing isocyanates and an apparatus suitable for this purpose, and also its use.
摘要翻译：本发明涉及一种制备异氰酸酯的方法和适用于该目的的装置及其用途。

2. 发明授权

US08829232B2 Process for preparing aromatic isocyanates 有权
标题翻译：制备芳族异氰酸酯的方法
公开(公告)号：US08829232B2
公开(公告)日：2014-09-09
申请号：US13057869
申请日：2009-08-06
申请人： Ulrich Penzel , Torsten Mattke , Andreas Wölfert , Johannes Jacobs , Tsung-Chieh Cheng , Kerstin Heinen , Eckhard Stroefer , Stefan Maixner , Wolfgang Mackenroth , Christian Tragut , Kai Thiele , Myung Un Won
发明人： Ulrich Penzel , Torsten Mattke , Andreas Wölfert , Johannes Jacobs , Tsung-Chieh Cheng , Kerstin Heinen , Eckhard Stroefer , Stefan Maixner , Wolfgang Mackenroth , Christian Tragut , Kai Thiele , Myung Un Won
IPC分类号： C07C263/00 , C07C263/10
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing isocyanates by reacting the corresponding amines with phosgene in the liquid phase, if appropriate in the presence of at least one inert medium, in which the amine and the phosgene are first mixed in a mixing chamber (1) to give a reaction mixture and the reaction mixture is fed to a reactor, the amine being added through an orifice (3) arranged coaxially to the mixing chamber (1) and the phosgene being added through feed orifices (5) in at least two planes (7, 9) arranged at right angles to the axis (11) of the mixing chamber (1), or the phosgene being added through the orifice (3) arranged coaxially to the mixing chamber and the amine through the feed orifices (5) in at least two planes (7, 9) arranged at right angles to the axis (11) of the mixing chamber (1). At least one plane (9) is arranged upstream and at least one plane (7) downstream of the orifice (3) arranged coaxially to the mixing chamber (1) in main flow direction of the reaction mixture. The mean residence time of the reaction mixture in the mixing chamber (1) is not more than 20 ms.
摘要翻译：本发明涉及通过使相应的胺与液相中的光气反应制备异氰酸酯的方法，如果合适的话，在至少一种惰性介质存在下，其中胺和光气首先在混合室（1）中混合，得到反应混合物并将反应混合物加入到反应器中，通过与混合室（1）同轴设置的孔口（3）加入胺，通过进料孔（5）在至少两个平面中加入光气（7,9），其与所述混合室（1）的轴线（11）成直角排列，或者通过所述孔（3）加入的光气通过所述孔（3）同轴地配置到所述混合室，所述胺通过所述进料孔（5）在与所述混合室（1）的轴线（11）成直角布置的至少两个平面（7,9）中。至少一个平面（9）布置在上游，并且孔（3）下游的至少一个平面（7）在反应混合物的主流动方向上与混合室（1）同轴布置。反应混合物在混合室（1）中的平均停留时间不超过20ms。

3. 发明授权

US09061971B2 Method for purifying residues containing isocyanates 有权
标题翻译：纯化含异氰酸酯残留物的方法
公开(公告)号：US09061971B2
公开(公告)日：2015-06-23
申请号：US12067104
申请日：2006-09-21
申请人： Andreas Wölfert , Carsten Knösche , Matthias Klötzer , Hermann Ascherl , Eckhard Stroefer , Heinrich-Josef Blankertz , Michael Schönherr , Martin Karches , Christian Benz
发明人： Andreas Wölfert , Carsten Knösche , Matthias Klötzer , Hermann Ascherl , Eckhard Stroefer , Heinrich-Josef Blankertz , Michael Schönherr , Martin Karches , Christian Benz
IPC分类号： C07C249/00 , C07C251/00 , C07C257/00 , C07C265/00 , C07C267/00 , C07C291/00 , C07C263/20
CPC分类号： C07C263/20 , C07C2601/14 , C07C265/14
摘要： The present invention comprises a process for purifying isocyanate-comprising residues.
摘要翻译：本发明包括用于纯化含异氰酸酯的残留物的方法。

4. 发明申请

US20060223966A1 Method for producing polyisocyanates 失效
公开(公告)号：US20060223966A1
公开(公告)日：2006-10-05
申请号：US10546890
申请日：2004-02-20
申请人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Wölfert , Steffen Oehlenschläger
发明人： Andreas Brodhagen , Martin Sohn , Filip Nevejans , Eckhard Stroefer , Andreas Wölfert , Steffen Oehlenschläger
IPC分类号： C08G18/00
CPC分类号： B01J19/242 , B01J19/243 , B01J2219/00166 , B01J2219/182 , B01J2219/185 , B01J2219/187 , C07C263/10 , C07C265/14
摘要： The invention relates to a process for preparing polyisocyanates by reacting primary amines with phosgene, which comprises the steps a) mixing the amine with the phosgene, b) reacting the amine with the phosgene in a residence reactor and, if desired, c) transferring the output from the reactor of step b) into a distillation column, wherein the residence reactor in step b) is configured as a tube reactor.

5. 发明申请

US20050070734A1 Production of isocyanates in the gaseous phase 失效
标题翻译：在气相中生产异氰酸酯
公开(公告)号：US20050070734A1
公开(公告)日：2005-03-31
申请号：US10495757
申请日：2002-11-19
申请人： Andreas Wölfert , Christian Muller , Eckhard Stroefer , Joachim Pfeffinger , Markus Weber , Carsten Knosche
发明人： Andreas Wölfert , Christian Muller , Eckhard Stroefer , Joachim Pfeffinger , Markus Weber , Carsten Knosche
IPC分类号： C07C263/10 , B01J12/00 , C07C265/14
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a method for producing isocyanates by reacting primary amines with phosgene in the gaseous phase. Said method is characterized in that the reaction of amine and phosgene occurs in a reaction channel, the internal dimensions of which have a width/height ratio of at least 2/1.
摘要翻译：本发明涉及通过使伯胺与气相中的光气反应制备异氰酸酯的方法。所述方法的特征在于胺和光气的反应发生在反应通道中，其内部尺寸的宽/高比至少为2/1。

6. 发明授权

US06833469B2 Method for producing isocynates 失效
标题翻译：异氰酸酯的制备方法
公开(公告)号：US06833469B2
公开(公告)日：2004-12-21
申请号：US10480240
申请日：2003-12-10
申请人： Andreas Wölfert , Christian Müller , Eckhard Stroefer
发明人： Andreas Wölfert , Christian Müller , Eckhard Stroefer
IPC分类号： C07C26300
CPC分类号： C07C263/10 , C07C265/14
摘要： The invention relates to a process for the production of isocyanates by reaction of primary amines with phosgene, in which isocyanate is used as solvent, wherein some or all of isocyanate used as solvent is added to the reaction mixture only after the amine and phosgene have been physically combined.
摘要翻译：本发明涉及通过使伯胺与光气反应生产异氰酸酯的方法，其中使用异氰酸酯作为溶剂，其中仅在胺和光气已经被加入到反应混合物中之后用作溶剂的一部分或全部异氰酸酯加入到反应混合物中身体结合。

7. 发明授权

US06677408B1 Method for producing ethylene homo-and copolymers by intensively mixing a reactive reaction component with a mobile flow medium 有权
标题翻译：通过将反应性反应成分与流动介质强烈混合来生产乙烯均聚物和共聚物的方法
公开(公告)号：US06677408B1
公开(公告)日：2004-01-13
申请号：US10009923
申请日：2001-12-06
申请人： Frank-Olaf Mähling , Andreas Daiss , Georg Groos , Andreas Wölfert
发明人： Frank-Olaf Mähling , Andreas Daiss , Georg Groos , Andreas Wölfert
IPC分类号： C08F206
CPC分类号： B01J19/2415 , B01F5/0473 , B01F5/0614 , B01F5/0644 , B01F5/0646 , B01F5/0652 , B01F2215/0431 , B01J19/26 , C08F10/02 , C08F110/02 , C08F4/28 , C08F2/01 , C08F2/00 , C08F2500/12
摘要： The invention relates to a method for producing ethylene homo- and copolymers in a tubular reactor at pressures above 1000 bar and temperatures in the range from 120 to 350° C. by free-radical polymerization, in which firstly small amounts of free-radical chain initiators are added to a mobile flow medium comprising ethylene, molecular weight regulator and optionally polyethylene, and the polymerization is then carried out. In accordance with the invention, the mobile flow medium is firstly split into two volume elements flowing separately from one another, the volume elements flowing separately from one another are then set in rotation in opposite directions by means of suitable flow elements, the flowing volume elements rotating in opposite directions are then recombined to form a mobile flow medium, and then, at the moment of or shortly after the combining of the flowing volume elements rotating in opposite directions, the free-radical chain initiator is fed into the sheared interfacial region between the flowing volume elements rotating in opposite directions. The invention also relates to an apparatus for carrying out this method.
摘要翻译：本发明涉及一种通过自由基聚合在管状反应器中制备乙烯均聚物和共聚物的方法，其中压力高于1000巴，温度范围为120-350℃，其中首先将少量的自由基链将引发剂加入到包含乙烯，分子量调节剂和任选的聚乙烯的流动介质中，然后进行聚合。根据本发明，移动流媒体首先被分成彼此分开流动的两个体积元件，然后通过合适的流动元件将相互分开流动的体积元件以相反方向旋转，流动体积元件然后在相反方向旋转以形成移动流动介质，然后在相反方向旋转的流动体积元件组合之后或不久之后，将自由基链引发剂进料到剪切界面区域之间，流动体积元件以相反的方向旋转。本发明还涉及一种用于执行该方法的装置。

8. 发明申请

US20100015036A1 REACTOR AND METHOD FOR PRODUCTION OF HYDROGEN SULPHIDE 有权
标题翻译：反应器和硫化氢生产方法
公开(公告)号：US20100015036A1
公开(公告)日：2010-01-21
申请号：US12523227
申请日：2008-01-10
申请人： Andreas Wölfert , Herald Jachow , Heinz Driess
发明人： Andreas Wölfert , Herald Jachow , Heinz Driess
IPC分类号： C01B17/16 , B01J19/00
CPC分类号： C01B17/162 , B01J8/008 , B01J8/065 , B01J8/067 , B01J10/005 , B01J19/0053 , B01J19/242
摘要： The present invention describes a reactor (1) for continuously preparing hydrogen sulfide H2S from hydrogen and sulfur, comprising a distributor device (15) for distributing gaseous hydrogen in a sulfur melt (9) present at least in a lower part of the reactor. The distributor device (15) is arranged in the sulfur melt (9) and comprises a distributor plate (16) which is arranged in the reactor (1) and has an edge (17) extending downward and, if appropriate, has passage orifices (19). The hydrogen from a hydrogen bubble which forms below the distributor plate (16) is (for example through the passage orifices (19)) distributed in the sulfur melt (9) via the distributor plate (16).
摘要翻译：本发明描述了一种用于从氢和硫连续制备硫化氢H 2 S的反应器（1），包括用于在至少在反应器的下部存在的硫磺熔体（9）中分配气态氢的分配器装置（15）。分配器装置（15）布置在硫磺熔体（9）中并且包括布置在反应器（1）中的分配器板（16），并且具有向下延伸的边缘（17），并且如果适当的话具有通道孔 19）。来自分配器板（16）下方形成的来自氢气泡的氢气（例如通过通道孔口（19））经由分配板（16）分布在硫磺熔体（9）中。

9. 发明授权

US07871594B2 Reactor and method for production of hydrogen sulphide 有权
标题翻译：用于生产硫化氢的反应器和方法
公开(公告)号：US07871594B2
公开(公告)日：2011-01-18
申请号：US12523227
申请日：2008-01-10
申请人： Andreas Wölfert , Herald Jachow , Heinz Drieβ
发明人： Andreas Wölfert , Herald Jachow , Heinz Drieβ
IPC分类号： C01B17/16
CPC分类号： C01B17/162 , B01J8/008 , B01J8/065 , B01J8/067 , B01J10/005 , B01J19/0053 , B01J19/242
摘要： The present invention describes a reactor (1) for continuously preparing hydrogen sulfide H2S from hydrogen and sulfur, comprising a distributor device (15) for distributing gaseous hydrogen in a sulfur melt (9) present at least in a lower part of the reactor. The distributor device (15) is arranged in the sulfur melt (9) and comprises a distributor plate (16) which is arranged in the reactor (1) and has an edge (17) extending downward and, if appropriate, has passage orifices (19). The hydrogen from a hydrogen bubble which forms below the distributor plate (16) is (for example through the passage orifices (19)) distributed in the sulfur melt (9) via the distributor plate (16).
摘要翻译：本发明描述了一种用于从氢和硫连续制备硫化氢H 2 S的反应器（1），包括用于在至少在反应器的下部存在的硫磺熔体（9）中分配气态氢的分配器装置（15）。分配器装置（15）布置在硫磺熔体（9）中并且包括布置在反应器（1）中的分配器板（16），并且具有向下延伸的边缘（17），并且如果适当的话具有通道孔 19）。来自分配器板（16）下方形成的来自氢气泡的氢气（例如通过通道孔口（19））经由分配板（16）分布在硫磺熔体（9）中。

10. 发明申请

US20090317322A1 METHOD AND DEVICE FOR THE CONTINUOUS PRODUCTION OF HYDROGEN SULFIDE 有权
标题翻译：连续生产硫化氢的方法和装置
公开(公告)号：US20090317322A1
公开(公告)日：2009-12-24
申请号：US12522189
申请日：2008-01-14
申请人： Andreas Wölfert , Herald Jachow , Heinz Driess
发明人： Andreas Wölfert , Herald Jachow , Heinz Driess
IPC分类号： C01B17/16 , C01B17/20 , F28D21/00
CPC分类号： B01J8/067 , B01J8/065 , B01J2208/00212 , B01J2208/0053 , C01B17/021 , C01B17/0226 , C01B17/162
摘要： The invention relates to a process and to an apparatus for preparing hydrogen sulfide H2S by converting a reactant mixture which comprises gaseous sulfur and hydrogen over a solid catalyst. The reactant mixture is converted at a pressure of from 0.5 to 10 bar absolute, a temperature of from 300 to 450° C. and a sulfur excess in a reactor (1). The sulfur excess corresponds to a ratio of excess sulfur to H2S prepared of from 0.2 to 3 kg of sulfur per kg of H2S prepared.
摘要翻译：本发明涉及通过在固体催化剂上转化包含气态硫和氢的反应物混合物来制备硫化氢H 2 S的方法和装置。将反应混合物在绝对压力为0.5至10巴，温度为300至450℃，反应器（1）中的硫过量转化。硫过量对应于制备的每公斤H2S中0.2至3kg硫的过量硫与H 2 S的比例。

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