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1. 发明申请

US20090175121A1 Process and mixing unit for the preparation of isocyanates by phosgenation of primary amines 失效
标题翻译：用于通过伯胺光气化制备异氰酸酯的工艺和混合单元
公开(公告)号：US20090175121A1
公开(公告)日：2009-07-09
申请号：US12316716
申请日：2008-12-16
申请人： Andreas Rausch , Christian Steffens , Dietmar Wastian , Manfred Keller-Killewald , Matthias Bohm , Joachim Ritter , Marcus Grunewald
发明人： Andreas Rausch , Christian Steffens , Dietmar Wastian , Manfred Keller-Killewald , Matthias Bohm , Joachim Ritter , Marcus Grunewald
IPC分类号： B01F13/00 , B01F15/04 , C07C263/10
CPC分类号： B01J19/1806 , B01F7/00766 , B01F13/1013 , B01F13/1016 , B01J2219/182 , C07C263/10 , C07C265/14
摘要： The invention relates to a mixer reactor of the rotor-stator type. This mixer reactor comprises a substantially rotationally symmetric housing which has a distributing chamber, a mixing chamber, a front plate that modifies the cross-section of the housing between these two chambers, and there are separate inlets into the mixing chamber for at least two substances and an outlet for removing the mixed material or product. The inlet for the first substance is provided in the axis of rotation of the mixing chamber. Two or more channels are aligned radially outward from this inlet, and the first substance is transported through these channels and into the mixing chamber. The inlet for the at least second substance is constructed in the form of a plurality of openings in the front plate, these inlet openings being are arranged rotationally symmetrically to the axis of rotation. Each of these inlet openings for the at least second substance has a corresponding pin which can be displaced in the axial direction.
摘要翻译：本发明涉及转子 - 定子类型的混合器反应器。该混合器反应器包括基本上旋转对称的壳体，其具有分配室，混合室，改变壳体在这两个室之间的横截面的前板，并且在混合室中有独立的入口用于至少两种物质以及用于除去混合材料或产品的出口。第一物质的入口设置在混合室的旋转轴线中。两个或更多个通道从该入口径向向外对准，并且第一物质被输送通过这些通道并进入混合室。用于至少第二物质的入口以前板中的多个开口的形式构造，这些入口开口相对于旋转轴线旋转对称地布置。用于至少第二物质的这些入口中的每一个具有可在轴向方向上移位的相应销。

2. 发明授权

US08079752B2 Process and mixing unit for the preparation of isocyanates by phosgenation of primary amines 失效
标题翻译：用于通过伯胺光气化制备异氰酸酯的工艺和混合单元
公开(公告)号：US08079752B2
公开(公告)日：2011-12-20
申请号：US12316716
申请日：2008-12-16
申请人： Andreas Rausch , Christian Steffens , Dietmar Wastian , Manfred Keller-Killewald , Matthias Böhm , Joachim Ritter , Marcus Grünewald
发明人： Andreas Rausch , Christian Steffens , Dietmar Wastian , Manfred Keller-Killewald , Matthias Böhm , Joachim Ritter , Marcus Grünewald
IPC分类号： B01F7/10
CPC分类号： B01J19/1806 , B01F7/00766 , B01F13/1013 , B01F13/1016 , B01J2219/182 , C07C263/10 , C07C265/14
摘要： The invention relates to a mixer reactor of the rotor-stator type. This mixer reactor comprises a substantially rotationally symmetric housing which has a distributing chamber, a mixing chamber, a front plate that modifies the cross-section of the housing between these two chambers, and there are separate inlets into the mixing chamber for at least two substances and an outlet for removing the mixed material or product. The inlet for the first substance is provided in the axis of rotation of the mixing chamber. Two or more channels are aligned radially outward from this inlet, and the first substance is transported through these channels and into the mixing chamber. The inlet for the at least second substance is constructed in the form of a plurality of openings in the front plate, these inlet openings being are arranged rotationally symmetrically to the axis of rotation. Each of these inlet openings for the at least second substance has a corresponding pin which can be displaced in the axial direction.
摘要翻译：本发明涉及转子 - 定子类型的混合器反应器。该混合器反应器包括基本上旋转对称的壳体，其具有分配室，混合室，改变壳体在这两个室之间的横截面的前板，并且在混合室中有独立的入口用于至少两种物质以及用于除去混合材料或产品的出口。第一物质的入口设置在混合室的旋转轴线中。两个或更多个通道从该入口径向向外对准，并且第一物质被输送通过这些通道并进入混合室。用于至少第二物质的入口以前板中的多个开口的形式构造，这些入口开口相对于旋转轴线旋转对称地布置。用于至少第二物质的这些入口中的每一个具有可在轴向方向上移位的相应销。

3. 发明授权

US06984762B2 Process for the two-step production of dinitrotoluene 有权
标题翻译：两步生产二硝基甲苯的方法
公开(公告)号：US06984762B2
公开(公告)日：2006-01-10
申请号：US10780266
申请日：2004-02-17
申请人： Erwin Dieterich , Anke Hielscher , Berthold Keggenhoff , Manfred Keller-Killewald , Jürgen Münnig , Dietmar Wastian
发明人： Erwin Dieterich , Anke Hielscher , Berthold Keggenhoff , Manfred Keller-Killewald , Jürgen Münnig , Dietmar Wastian
IPC分类号： C07C205/00
CPC分类号： C07C201/16 , C07C201/08 , C07C205/06
摘要： The invention relates to a process for the production of dinitrotoluene by the two-stage nitration of toluene. In the first stage of this process, toluene was reacted adiabatically with nitrating acid so that at least 90% of the toluene was reacted off and no more than 70% of the toluene formed dinitrotoluene. The resulting organic phase containing mononitrotoluene and the aqueous acid phase containing sulfuric acid were separated, and the aqueous acid phase containing sulfuric acid was concentrated by flash evaporation. The resulting concentrated sulfuric acid was recycled into the reaction in the first stage, and/or into the reaction in the second stage, and/or into the concentration in the second stage.In the second stage, the organic phase containing mononitrotoluene from the first stage was completely reacted isothermally with nitrating acid. The organic phase and the aqueous acid phase containing sulfuric acid were then separated, and the aqueous acid phase containing sulfuric acid was concentrated by vacuum evaporation. The resulting concentrated sulfuric acid was recycled into the reaction in the first stage and/or the second stage.
摘要翻译：本发明涉及通过甲苯二段硝化生产二硝基甲苯的方法。在该方法的第一阶段，将甲苯与硝酸进行绝热反应，使得甲苯的至少90％反应，并且不超过70％的甲苯形成二硝基甲苯。分离含有单硝基甲苯和含硫酸水相的所得有机相，通过闪蒸浓缩含硫酸水相。将所得浓硫酸在第一阶段循环进入反应，和/或在第二阶段进入反应，和/或在第二阶段中浓缩。在第二阶段，含有来自第一阶段的一硝基甲苯的有机相与硝酸一起等温共同反应。然后分离含有硫酸的有机相和含水酸相，真空蒸发浓缩含硫酸的酸水溶液。所得浓硫酸在第一阶段和/或第二阶段循环进入反应。

4. 发明授权

US07202384B2 Process for producing 5-nitro-3,4-dihydro-1(2H)-naphthalinone, 1,5-naphthalenediamine and 1,5-naphthalene diisocyanate 有权
标题翻译：制备5-硝基-3,4-二氢-1（2H） - 萘酮，1,5-萘二胺和1,5-萘二异氰酸酯的方法
公开(公告)号：US07202384B2
公开(公告)日：2007-04-10
申请号：US11400007
申请日：2006-04-07
申请人： Joachim Zechlin , Kai Verkerk , Dietmar Wastian , Kartin Joschek , Tim Loddenkemper , Wilfried Pinke , Michael Schelhaas , Georg Ronge
发明人： Joachim Zechlin , Kai Verkerk , Dietmar Wastian , Kartin Joschek , Tim Loddenkemper , Wilfried Pinke , Michael Schelhaas , Georg Ronge
IPC分类号： C07C45/00
CPC分类号： C07C209/68 , C07C201/12 , C07C211/58 , C07C263/10 , C07C265/14 , C07C205/56 , C07C205/45
摘要： The present invention relates to a process for producing 5-nitro-3,4-dihydro-1(2H)-naphthalinone, 1,5-naphthalenediamine and 1,5-naphthalene diisocyanate, in which 4-(2-nitrophenyl)-n-butyronitrile is converted to 4-(2-nitrophenyl)-n-butyric acid.
摘要翻译：本发明涉及5-硝基-3,4-二氢-1（2H） - 萘酮，1,5-萘二胺和1,5-萘二异氰酸酯的制备方法，其中4-（2-硝基苯基）-n - 丁腈转化成4-（2-硝基苯基） - 正丁酸。

5. 发明授权

US07202378B2 Process for producing 5-nitro-3,4-dihydro-1(H)-naphthalinone, 1,5-naphthalenediamine and 1,5-naphthalene diisocyanate 有权
标题翻译：制备5-硝基-3,4-二氢-1（H） - 萘酮，1,5-萘二胺和1,5-萘二异氰酸酯的方法
公开(公告)号：US07202378B2
公开(公告)日：2007-04-10
申请号：US11399962
申请日：2006-04-07
申请人： Joachim Zechlin , Kai Verkerk , Dietmar Wastian , Katrin Joschek , Tim Loddenkemper , Wilfried Pinke , Michael Schelhaas , Georg Ronge
发明人： Joachim Zechlin , Kai Verkerk , Dietmar Wastian , Katrin Joschek , Tim Loddenkemper , Wilfried Pinke , Michael Schelhaas , Georg Ronge
IPC分类号： C07C261/00
CPC分类号： C07C209/68 , C07C201/12 , C07C211/58 , C07C263/10 , C07C265/14 , C07C205/56 , C07C205/45
摘要： The present invention relates to a process for producing 5-nitro-3,4-dihydro-1(2H)-naphthalinone, 1,5-naphthalenediamine and 1,5-naphthalene diisocyanate, in which 4-(2-nitrophenyl)-n-butyronitrile is converted to 4-(2-nitrophenyl)-n-butyric acid.
摘要翻译：本发明涉及5-硝基-3,4-二氢-1（2H） - 萘酮，1,5-萘二胺和1,5-萘二异氰酸酯的制备方法，其中4-（2-硝基苯基）-n - 丁腈转化为4-（2-硝基苯基） - 正丁酸。

6. 发明申请

US20060183946A1 Process for producing 5-nitro-3,4-dihydro-1(H)-naphthalinone, 1,5-naphthalenediamine and 1,5-naphthalene diisocyanate 有权
标题翻译：制备5-硝基-3,4-二氢-1（H） - 萘酮，1,5-萘二胺和1,5-萘二异氰酸酯的方法
公开(公告)号：US20060183946A1
公开(公告)日：2006-08-17
申请号：US11399962
申请日：2006-04-07
申请人： Joachim Zechlin , Kai Verkerk , Dietmar Wastian , Katrin Joschek , Tim Loddenkemper , Wilfried Pinke , Michael Schelhaas , Georg Ronge
发明人： Joachim Zechlin , Kai Verkerk , Dietmar Wastian , Katrin Joschek , Tim Loddenkemper , Wilfried Pinke , Michael Schelhaas , Georg Ronge
IPC分类号： C07C205/45
CPC分类号： C07C209/68 , C07C201/12 , C07C211/58 , C07C263/10 , C07C265/14 , C07C205/56 , C07C205/45
摘要： The present invention relates to a process for producing 5-nitro-3,4-dihydro-1(2H)-naphthalinone, 1,5-naphthalenediamine and 1,5-naphthalene diisocyanate, in which 4-(2-nitrophenyl)-n-butyronitrile is converted to 4-(2-nitrophenyl)-n-butyric acid.
摘要翻译：本发明涉及5-硝基-3,4-二氢-1（2H） - 萘酮，1,5-萘二胺和1,5-萘二异氰酸酯的制备方法，其中4-（2-硝基苯基）-n - 丁腈转化为4-（2-硝基苯基） - 正丁酸。

7. 发明授权

US07612234B2 Processes for separating carbon monoxide from a hydrogen chloride-containing gas 失效
标题翻译：从含氯化氢的气体中分离一氧化碳的方法
公开(公告)号：US07612234B2
公开(公告)日：2009-11-03
申请号：US11752391
申请日：2007-05-23
申请人： Michel Haas , Dietmar Wastian , Tim Loddenkemper , Bernd Rüffer
发明人： Michel Haas , Dietmar Wastian , Tim Loddenkemper , Bernd Rüffer
IPC分类号： C07C51/58
CPC分类号： C01B7/0706 , B01D53/62 , B01D2251/502 , B01D2257/502 , C01B32/80 , Y02A50/2341
摘要： Processes for separating carbon monoxide from a hydrogen chloride-containing gas, which comprise reacting the carbon monoxide with chlorine to form phosgene and then optionally separating the phosgene from the hydrogen chloride-containing gas. The hydrogen chloride-containing gas that is used preferably derives from a phosgenation or isocyanate forming reaction.
摘要翻译：用于从含氯化氢的气体中分离一氧化碳的方法，其包括使一氧化碳与氯气反应以形成光气，然后任选地从含氯化氢的气体中分离光气。所用的含氯化氢的气体优选来自光气化或异氰酸酯形成反应。

8. 发明申请

US20070276158A1 PROCESSES FOR SEPARATING CARBON MONOXIDE FROM A HYDROGEN CHLORIDE-CONTAINING GAS 失效
标题翻译：从含有氯化氢的气体中分离一氧化碳的方法
公开(公告)号：US20070276158A1
公开(公告)日：2007-11-29
申请号：US11752391
申请日：2007-05-23
申请人： Michel Haas , Dietmar Wastian , Tim Loddenkemper , Bernd Ruffer
发明人： Michel Haas , Dietmar Wastian , Tim Loddenkemper , Bernd Ruffer
IPC分类号： C07C51/58
CPC分类号： C01B7/0706 , B01D53/62 , B01D2251/502 , B01D2257/502 , C01B32/80 , Y02A50/2341
摘要： Processes for separating carbon monoxide from a hydrogen chloride-containing gas, which comprise reacting the carbon monoxide with chlorine to form phosgene and then optionally separating the phosgene from the hydrogen chloride-containing gas. The hydrogen chloride-containing gas that is used preferably derives from a phosgenation or isocyanate forming reaction.
摘要翻译：用于从含氯化氢的气体中分离一氧化碳的方法，其包括使一氧化碳与氯气反应以形成光气，然后任选地从含氯化氢的气体中分离光气。所用的含氯化氢的气体优选来自光气化或异氰酸酯形成反应。

9. 发明授权

US07041858B1 Process for the production of dinitrotoluene 有权
标题翻译：生产二硝基甲苯的方法
公开(公告)号：US07041858B1
公开(公告)日：2006-05-09
申请号：US11054012
申请日：2005-02-09
申请人： Juergen Muennig , Bernd Pennemann , Dietmar Wastian , Volker Michele , Jesse Caravaggio , John F. Gisch, Jr.
发明人： Juergen Muennig , Bernd Pennemann , Dietmar Wastian , Volker Michele , Jesse Caravaggio , John F. Gisch, Jr.
IPC分类号： C07C205/00
CPC分类号： C07C201/08 , C07C205/06
摘要： The present invention is directed to a process for the isothermal nitration of aromatic organic compounds, wherein an aromatic organic compound is brought into contact and reacted with a mixture of sulfuric acid and nitric acid. The mixture of sulfuric acid and nitric acid, and the aromatic organic compound are brought into contact with each other through a mixing nozzle which comprises a substantially cylindrical tubular reactor and an annular gap which surrounds the tubular reactor. The aromatic organic compound flows through the tubular reactor, and the mixture of sulfuric acid and nitric acid flows through the annular gap, and they are mixed together upon emerging from the tubular reactor and the annular gap, wherein the ratio of the average rates of flow of the aromatic organic compound in the tubular reactor, and of the mixture of sulphuric acid and nitric acid in the annular gap ranges from 0.5:1 to 10:1.
摘要翻译：本发明涉及芳族有机化合物的等温硝化方法，其中使芳族有机化合物与硫酸和硝酸的混合物接触并反应。硫酸和硝酸的混合物和芳香族有机化合物通过混合喷嘴相互接触，所述混合喷嘴包括基本上圆柱形的管式反应器和围绕管状反应器的环形间隙。芳族有机化合物流过管状反应器，硫酸和硝酸的混合物流过环形间隙，并且在从管式反应器和环形间隙出现时将它们混合在一起，其中平均流速的管状反应器中的芳族有机化合物，以及环状间隙中的硫酸和硝酸的混合物的范围为0.5:1至10:1。

10. 发明授权

US08097751B2 Process for preparing polyisocyanates by the adiabatic phosgenation of primary amines 有权
标题翻译：通过伯胺的绝热光气化制备多异氰酸酯的方法
公开(公告)号：US08097751B2
公开(公告)日：2012-01-17
申请号：US11171572
申请日：2005-06-30
申请人： Daniel Koch , Spotswood Miller , Ricardo Serra , Dietmar Wastian , Jürgen Kirsch , Gerhard Wegener
发明人： Daniel Koch , Spotswood Miller , Ricardo Serra , Dietmar Wastian , Jürgen Kirsch , Gerhard Wegener
IPC分类号： C07C249/00
CPC分类号： C07C263/10 , C07C265/14
摘要： A two-stage process for the preparation of organic isocyanates by reacting primary amines with phosgene in which: a) in a first stage, amine and phosgene are reacted in an adiabatically managed reaction, in which the temperature of reaction is restricted to values between 100 and 220° C. by actively adjusting the absolute pressure in the reactor to values between 8 and 50 bar by decompression, and the temperature is held at values between 100 and 220° C. until the stoichiometric conversion of phosgene has reached at least 80%; and then b) in a second stage, the reaction mixture from a) is decompressed to an absolute pressure of 1 to 15 bar and the reaction mixture is reacted further at temperatures between 90 and 240° C., optionally with the introduction of heat.
摘要翻译：通过使伯胺与光气反应来制备有机异氰酸酯的两阶段方法，其中：a）在第一阶段中，胺和光气在绝热管理的反应中反应，其中反应温度限于100 通过减压将反应器中的绝对压力积极调节至8巴和50巴之间，并将温度保持在100至220℃之间，直到光气的化学计量转化率达到至少80％ ; 然后b）在第二阶段中，将来自a）的反应混合物减压至1至15巴的绝对压力，并且反应混合物进一步在90-240℃的温度下进行反应，任选地加热。

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