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1. 发明授权

US09040732B2 Process for preparing diaryl carbonates from dialkyl carbonates 有权
标题翻译：由碳酸二烷基酯制备碳酸二芳基酯的方法
公开(公告)号：US09040732B2
公开(公告)日：2015-05-26
申请号：US12483669
申请日：2009-06-12
申请人： Andre Düx , Guenter Olf , Kaspar Hallenberger , Georg Ronge , Ricarda Leiberich , Johan Vanden Eynde , Wim Wuytack , Pieter Ooms , Johann Rechner
发明人： Andre Düx , Guenter Olf , Kaspar Hallenberger , Georg Ronge , Ricarda Leiberich , Johan Vanden Eynde , Wim Wuytack , Pieter Ooms , Johann Rechner
IPC分类号： C07C69/96 , C07C68/06
CPC分类号： C07C68/06 , Y02P20/124 , C07C69/96
摘要： The invention provides a process for preparing diaryl carbonates from dialkyl carbonates and aromatic hydroxyl compounds using at least two reaction columns, a process section for recovering the dialkyl carbonate used in the reaction and for removing the alcohol of reaction, one or more process steps for removing the by-products obtained in the process which have a boiling point between that of the dialkyl carbonate and that of the alkyl aryl carbonate formed during the preparation of the diaryl carbonate, and a process step for further purification of the diaryl carbonate obtained from the reaction columns.
摘要翻译：本发明提供了一种使用至少两个反应塔从碳酸二烷基酯和芳族羟基化合物制备碳酸二芳基酯的方法，用于回收反应中使用的二烷基碳酸酯和用于除去反应醇的工艺部分，一个或多个除去工艺步骤在碳酸二烷基酯碳酸二烷基酯和碳酸二芳基酯的碳酸烷基芳基酯的沸点相同的过程中获得的副产物，以及从反应中得到的进一步纯化碳酸二芳基酯的工艺步骤列。

2. 发明申请

US20110206568A1 PROCESS FOR THE PREPARATION OF DIARYL CARBONATES OR ARYLALKYL CARBONATES FROM DIALKYL CARBONATES 审中-公开
标题翻译：从碳酸二甲酯制备二元碳酸酯或碳酸亚乙酯的方法
公开(公告)号：US20110206568A1
公开(公告)日：2011-08-25
申请号：US13102255
申请日：2011-05-06
申请人： Andre Düx , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Düx , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： B01J8/06
CPC分类号： C07C68/06 , B01D3/009 , Y02P20/127 , C07C69/96
摘要： The invention provides a process for the preparation of diaryl carbonates and/or alkylaryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using one or more intermediate condensers for improving heat integration.
摘要翻译：本发明提供了一种使用一种或多种中间冷凝器制备碳酸二芳基酯和/或碳酸二烷基酯从碳酸二烷基酯和芳族羟基化合物制备方法，用于改善热量积分。

3. 发明申请

US20100010252A1 PROCESS FOR PREPARING DIARYL CARBONATES FROM DIALKYL CARBONATES 有权
标题翻译：从碳酸二乙酯制备二元碳酸盐的方法
公开(公告)号：US20100010252A1
公开(公告)日：2010-01-14
申请号：US12483669
申请日：2009-06-12
申请人： Andre Düx , Guenter Olf , Kaspar Hallenberger , Georg Ronge , Ricarda Leiberich , Johan Vanden Eynde , Wim Wuytack , Pieter Ooms , Johann Rechner
发明人： Andre Düx , Guenter Olf , Kaspar Hallenberger , Georg Ronge , Ricarda Leiberich , Johan Vanden Eynde , Wim Wuytack , Pieter Ooms , Johann Rechner
IPC分类号： C07C69/96
CPC分类号： C07C68/06 , Y02P20/124 , C07C69/96
摘要： The invention provides a process for preparing diaryl carbonates from dialkyl carbonates and aromatic hydroxyl compounds using at least two reaction columns, a process section for recovering the dialkyl carbonate used in the reaction and for removing the alcohol of reaction, one or more process steps for removing the by-products obtained in the process which have a boiling point between that of the dialkyl carbonate and that of the alkyl aryl carbonate formed during the preparation of the diaryl carbonate, and a process step for further purification of the diaryl carbonate obtained from the reaction columns.
摘要翻译：本发明提供了一种使用至少两个反应塔从碳酸二烷基酯和芳族羟基化合物制备碳酸二芳基酯的方法，用于回收反应中使用的二烷基碳酸酯和用于除去反应醇的工艺部分，一个或多个除去工艺步骤在碳酸二烷基酯碳酸二烷基酯和碳酸二芳基酯的碳酸烷基芳基酯的沸点相同的过程中获得的副产物，以及从反应中得到的进一步纯化碳酸二芳基酯的工艺步骤列。

4. 发明授权

US08039659B2 Processes for preparing diaryl and/or alkylaryl carbonates from dialkyl carbonates 有权
标题翻译：由碳酸二烷基酯制备二芳基和/或烷基芳基碳酸酯的方法
公开(公告)号：US08039659B2
公开(公告)日：2011-10-18
申请号：US12210279
申请日：2008-09-15
申请人： Andre Düx , Pieter Ooms , Johann Rechner , Matthias Böhm , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Düx , Pieter Ooms , Johann Rechner , Matthias Böhm , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C69/96
CPC分类号： C07C68/06 , C07C69/96
摘要： Processes comprising: reacting a dialkyl carbonate and an aromatic hydroxy compound in the presence of a transesterification catalyst in a first reaction column, the first reaction column comprising a top section, a bottom section, a rectifying section in an upper portion of the column and a reaction zone below the rectifying section; feeding a bottom product from the first reaction column to a further reaction column; the bottom product comprising a diaryl carbonate, an alkylaryl carbonate, or both, and residual unreacted dialkyl carbonate and aromatic hydroxy compound; the further reaction column comprising a top section, a rectifying section in an upper portion of the column and a reaction zone below the rectifying section; and reacting the residual unreacted dialkyl carbonate and aromatic hydroxy compound in the further reaction column; feeding a process stream to a distillation column, the process stream comprising a mixture of unreacted dialkyl carbonate and one or more reaction-product alcohols drawn from the first reaction column, the further reaction column, or both, such that the unreacted dialkyl carbonate is separated from the one or more reaction-product alcohols; and recycling the separated, unreacted dialkyl carbonate to the first reaction column; wherein the further reaction column comprises one or more condensers, and heat of condensation from the one or more condensers is fed back into the process.
摘要翻译：方法包括：在第一反应塔中的酯交换催化剂存在下使碳酸二烷基酯和芳族羟基化合物反应，所述第一反应塔包括塔的上部的顶部，底部，精馏段和整流段下方的反应区; 将底部产物从第一反应塔进料至另一反应塔; 底部产物包含碳酸二芳基酯，碳酸二烷基酯或二者，和残留的未反应的碳酸二烷基酯和芳族羟基化合物; 所述另外的反应塔包括顶部，所述塔的上部的精馏部和所述精馏部下方的反应区; 并使残留的未反应的碳酸二烷基碳酸酯和芳族羟基化合物在另外的反应塔中反应; 将工艺流输送到蒸馏塔，所述工艺流包含未反应的碳酸二烷基酯和从第一反应塔，进一步的反应塔或两者中抽出的一种或多种反应产物醇的混合物，使得未反应的碳酸二烷基酯被分离由一种或多种反应产物醇; 并将分离的未反应的碳酸二烷基酯再循环到第一反应塔中; 其中所述另外的反应塔包括一个或多个冷凝器，并且将来自所述一个或多个冷凝器的冷凝热反馈到所述方法中。

5. 发明授权

US08022240B2 Processes for purifying diaryl carbonates 有权
标题翻译：净化碳酸二芳基酯的方法
公开(公告)号：US08022240B2
公开(公告)日：2011-09-20
申请号：US12274776
申请日：2008-11-20
申请人： Pieter Ooms , Johann Rechner , Matthias Böhm , Andre Düx , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Pieter Ooms , Johann Rechner , Matthias Böhm , Andre Düx , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C67/02
CPC分类号： C07C68/08 , B01D3/14 , B01D3/141 , Y02P20/57 , C07C69/96
摘要： Processes comprising: transesterifying a dialkyl carbonate and an aromatic hydroxyl compound in the presence of a transesterification catalyst to provide a diaryl carbonate product comprising the transesterification catalyst as an impurity; subjecting the diaryl carbonate product to distillation in a first distillation column having an upper part and a lower part, wherein the upper part comprises a rectifying section and the lower part comprises a stripping section; and withdrawing a first sidestream from the first distillation column, wherein the first sidestream comprises a purified diaryl carbonate.
摘要翻译：方法包括：在酯交换催化剂存在下酯交换碳酸二烷基酯和芳族羟基化合物，得到包含酯交换催化剂作为杂质的碳酸二芳酯产物; 在具有上部和下部的第一蒸馏塔中对碳酸二芳基酯进行蒸馏，其中上部包括精馏段，下部包含汽提段; 以及从所述第一蒸馏塔排出第一侧流，其中所述第一侧流包含纯化的碳酸二芳基酯。

6. 发明授权

US08003817B2 Process for the preparation of diaryl carbonates or arylalkyl carbonates from dialkyl carbonates 失效
标题翻译：从碳酸二烷基酯制备碳酸二芳基酯或碳酸芳基酯的方法
公开(公告)号：US08003817B2
公开(公告)日：2011-08-23
申请号：US12121873
申请日：2008-05-16
申请人： Andre Düx , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Düx , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C69/96
CPC分类号： C07C68/06 , B01D3/009 , Y02P20/127 , C07C69/96
摘要： The invention provides a process for the preparation of diaryl carbonates and/or alkylaryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using one or more intermediate condensers for improving heat integration.
摘要翻译：本发明提供了一种使用一种或多种中间冷凝器制备碳酸二芳基酯和/或碳酸二烷基酯从碳酸二烷基酯和芳族羟基化合物制备方法，用于改善热量积分。

7. 发明申请

US20090137832A1 PROCESSES FOR PURIFYING DIARYL CARBONATES 有权
标题翻译：纯化二氧化碳的方法
公开(公告)号：US20090137832A1
公开(公告)日：2009-05-28
申请号：US12274776
申请日：2008-11-20
申请人： Pieter Ooms , Johann Rechner , Matthias Bohm , Andre Dux , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Pieter Ooms , Johann Rechner , Matthias Bohm , Andre Dux , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C68/06
CPC分类号： C07C68/08 , B01D3/14 , B01D3/141 , Y02P20/57 , C07C69/96
摘要： Processes comprising: transesterifying a dialkyl carbonate and an aromatic hydroxyl compound in the presence of a transesterification catalyst to provide a diaryl carbonate product comprising the transesterification catalyst as an impurity; subjecting the diaryl carbonate product to distillation in a first distillation column having an upper part and a lower part, wherein the upper part comprises a rectifying section and the lower part comprises a stripping section; and withdrawing a first sidestream from the first distillation column, wherein the first sidestream comprises a purified diaryl carbonate.
摘要翻译：方法包括：在酯交换催化剂存在下酯交换碳酸二烷基酯和芳族羟基化合物，得到包含酯交换催化剂作为杂质的碳酸二芳酯产物; 在具有上部和下部的第一蒸馏塔中对碳酸二芳基酯进行蒸馏，其中上部包括精馏段，下部包含汽提段; 以及从所述第一蒸馏塔排出第一侧流，其中所述第一侧流包含纯化的碳酸二芳基酯。

8. 发明申请

US20090076293A1 PROCESSES FOR PREPARING DIARYL AND/OR ALKYLARYL CARBONATES FROM DIALKYL CARBONATES 有权
标题翻译：从碳酸二甲酯制备二元和/或烷基碳酸的方法
公开(公告)号：US20090076293A1
公开(公告)日：2009-03-19
申请号：US12210279
申请日：2008-09-15
申请人： Andre Dux , Pieter Ooms , Johann Rechner , Matthias Bohm , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Dux , Pieter Ooms , Johann Rechner , Matthias Bohm , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C68/06
CPC分类号： C07C68/06 , C07C69/96
摘要： Processes comprising: reacting a dialkyl carbonate and an aromatic hydroxy compound in the presence of a transesterification catalyst in a first reaction column, the first reaction column comprising a top section, a bottom section, a rectifying section in an upper portion of the column and a reaction zone below the rectifying section; feeding a bottom product from the first reaction column to a further reaction column; the bottom product comprising a diaryl carbonate, an alkylaryl carbonate, or both, and residual unreacted dialkyl carbonate and aromatic hydroxy compound; the further reaction column comprising a top section, a rectifying section in an upper portion of the column and a reaction zone below the rectifying section; and reacting the residual reacted dialkyl carbonate and aromatic hydroxy compound in the further reaction column; feeding a process stream to a distillation column, the process stream comprising a mixture of unreacted dialkyl carbonate and one or more reaction-product alcohols drawn from the first reaction column, the further reaction column, or both, such that the unreacted dialkyl carbonate is separated from the one or more reaction-product alcohols; and recycling the separated, unreacted dialkyl carbonate to the first reaction column; wherein the further reaction column comprises one or more condensers, and heat of condensation from the one or more condensers is fed back into the process.
摘要翻译：方法包括：在第一反应塔中的酯交换催化剂存在下使碳酸二烷基酯和芳族羟基化合物反应，所述第一反应塔包括塔的上部的顶部，底部，精馏段和整流段下方的反应区; 将底部产物从第一反应塔进料至另一反应塔; 底部产物包含碳酸二芳基酯，碳酸二烷基酯或二者，和残留的未反应的碳酸二烷基酯和芳族羟基化合物; 所述另外的反应塔包括顶部，所述塔的上部的精馏部和所述精馏部下方的反应区; 并使残留的反应后的碳酸二烷基酯和芳香族羟基化合物反应进一步反应塔中; 将工艺流输送到蒸馏塔，所述工艺流包含未反应的碳酸二烷基酯和从第一反应塔，进一步的反应塔或两者中抽出的一种或多种反应产物醇的混合物，使得未反应的碳酸二烷基酯被分离由一种或多种反应产物醇; 并将分离的未反应的碳酸二烷基酯再循环到第一反应塔中; 其中所述另外的反应塔包括一个或多个冷凝器，并且将来自所述一个或多个冷凝器的冷凝热反馈到所述方法中。

9. 发明申请

US20080293960A1 Process For The Preparation Of Diaryl Carbonates Or Arylalkyl Carbonates From Dialkyl Carbonates 失效
标题翻译：从碳酸二烷基酯制备碳酸二芳基酯或芳基烷基碳酸酯的方法
公开(公告)号：US20080293960A1
公开(公告)日：2008-11-27
申请号：US12121873
申请日：2008-05-16
申请人： Andre Dux , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
发明人： Andre Dux , Pieter Ooms , Johann Rechner , Kaspar Hallenberger , Georg Ronge , Johan Vanden Eynde
IPC分类号： C07C69/96 , B01J19/00
CPC分类号： C07C68/06 , B01D3/009 , Y02P20/127 , C07C69/96
摘要： The invention provides a process for the preparation of diaryl carbonates and/or alkylaryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using one or more intermediate condensers for improving heat integration.
摘要翻译：本发明提供了一种使用一种或多种中间冷凝器制备碳酸二芳基酯和/或碳酸二烷基酯从碳酸二烷基酯和芳族羟基化合物制备方法，用于改善热量积分。

10. 发明授权

US08952189B2 Process for preparing diaryl carbonates or alkyl aryl carbonates from dialkyl carbonates 有权
标题翻译：由碳酸二烷基酯制备碳酸二芳基酯或碳酸烷基酯的方法
公开(公告)号：US08952189B2
公开(公告)日：2015-02-10
申请号：US12755873
申请日：2010-04-07
申请人： Andre Düx , Helmut Mothes , Kaspar Hallenberger , Georg Ronge , Rafael Warsitz , Pieter Ooms , Johann Rechner
发明人： Andre Düx , Helmut Mothes , Kaspar Hallenberger , Georg Ronge , Rafael Warsitz , Pieter Ooms , Johann Rechner
IPC分类号： C07C68/06 , C07C69/96
CPC分类号： C07C68/06 , Y02P20/127 , C07C69/96
摘要： The invention relates to a process for preparing diaryl carbonates and/or alkyl aryl carbonates from dialkyl carbonates and aromatic hydroxy compounds using a reactive dividing wall column.
摘要翻译：本发明涉及使用反应性分隔壁塔从碳酸二烷基酯和芳族羟基化合物制备碳酸二芳基酯和/或烷基芳基碳酸酯的方法。

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