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1. 发明申请

US20070135609A1 Poly(arylene ether) copolymer 有权
标题翻译：聚（亚芳基醚）共聚物
公开(公告)号：US20070135609A1
公开(公告)日：2007-06-14
申请号：US11298182
申请日：2005-12-08
申请人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
发明人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
IPC分类号： C08G61/02
CPC分类号： C08G65/44 , H05K1/0326
摘要： A poly(arylene ether) copolymer is the product of oxidative copolymerization of monomers including a monohydric phenol and a dihydric phenol. It has an intrinsic viscosity of about 0.04 to about 0.15 deciliter per gram and, on average, about 1.8 to about 2 hydroxyl groups per molecule. The poly(arylene ether) copolymer is enriched in low molecular weight copolymer chains and copolymer chains that include a terminal unit derived from the dihydric phenol.
摘要翻译：聚（亚芳基醚）共聚物是包括一元酚和二元酚的单体的氧化共聚的产物。其特性粘度为约0.04至约0.15分升每克，平均每分子约1.8至约2个羟基。聚（亚芳基醚）共聚物富含低分子量共聚物链和共聚物链，其包括源自二元酚的末端单元。

2. 发明申请

US20070106051A1 Polyfunctional poly(arylene ether) method 审中-公开
标题翻译：多官能聚（亚芳基醚）法
公开(公告)号：US20070106051A1
公开(公告)日：2007-05-10
申请号：US11272119
申请日：2005-11-10
申请人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
发明人： Alvaro Carrillo , Erik Delsman , Hua Guo , Alexey Kruglov , Edward Peters
IPC分类号： C08G61/02
CPC分类号： C08G65/44 , C08G65/46 , H05K1/0326
摘要： A polyfunctional poly(arylene ether) resin may be prepared by a method that includes oxidatively copolymerizing a monohydric phenol and a polyhydric phenol in an aromatic hydrocarbon solvent in the presence of a catalyst comprising a metal ion and a nitrogen-containing ligand to form a solution comprising a polyfunctional poly(arylene ether) having an intrinsic viscosity of about 0.04 to about 0.3 deciliter per gram at 25° C. in chloroform; and contacting the polyfunctional poly(arylene ether) solution with an aqueous solution of a chelating agent to extract the metal ion from the solution; wherein the chelating agent and metal ion are present in a molar ratio of about 1.0 to about 1.5. The method reduces the formation of a dispersion during the chelation step.
摘要翻译：多官能聚（亚芳基醚）树脂可以通过包括在包含金属离子和含氮配体的催化剂存在下在芳烃溶剂中将一元酚和多元酚氧化共聚以形成溶液的方法来制备包括在25℃下在氯仿中特性粘度为约0.04至约0.3分升/克的多官能聚（亚芳基醚）并使多官能聚（亚芳基醚）溶液与螯合剂的水溶液接触，从溶液中提取金属离子; 其中所述螯合剂和金属离子以约1.0至约1.5的摩尔比存在。该方法减少了螯合步骤期间分散体的形成。

3. 发明授权

US07541421B2 Poly(arylene ether) copolymer 有权
标题翻译：聚（亚芳基醚）共聚物
公开(公告)号：US07541421B2
公开(公告)日：2009-06-02
申请号：US11298182
申请日：2005-12-08
申请人： Alvaro Carrillo , Erik René Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
发明人： Alvaro Carrillo , Erik René Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
IPC分类号： C08G61/02 , C08G65/38
CPC分类号： C08G65/44 , H05K1/0326
摘要： A poly(arylene ether) copolymer is the product of oxidative copolymerization of monomers including a monohydric phenol and a dihydric phenol. It has an intrinsic viscosity of about 0.04 to about 0.15 deciliter per gram and, on average, about 1.8 to about 2 hydroxyl groups per molecule. The poly(arylene ether) copolymer is enriched in low molecular weight copolymer chains and copolymer chains that include a terminal unit derived from the dihydric phenol.
摘要翻译：聚（亚芳基醚）共聚物是包括一元酚和二元酚的单体的氧化共聚的产物。其特性粘度为约0.04至约0.15分升每克，平均每分子约1.8至约2个羟基。聚（亚芳基醚）共聚物富含低分子量共聚物链和共聚物链，其包括源自二元酚的末端单元。

4. 发明申请

US20090247724A1 POLY(ARYLENE ETHER) COPOLYMER 有权
标题翻译： POLY（ARYLENE ETHER）COPOLYMER
公开(公告)号：US20090247724A1
公开(公告)日：2009-10-01
申请号：US12414856
申请日：2009-03-31
申请人： Alvaro Carrillo , Erik Rene Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
发明人： Alvaro Carrillo , Erik Rene Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
IPC分类号： C08G65/44 , C08G65/38
CPC分类号： C08G65/44 , H05K1/0326
摘要： A poly(arylene ether) copolymer is the product of oxidative copolymerization of monomers including a monohydric phenol and a dihydric phenol. It has an intrinsic viscosity of about 0.04 to about 0.15 deciliter per gram and, on average, about 1.8 to about 2 hydroxyl groups per molecule. The poly(arylene ether) copolymer is enriched in low molecular weight copolymer chains and copolymer chains that include a terminal unit derived from the dihydric phenol.
摘要翻译：聚（亚芳基醚）共聚物是包括一元酚和二元酚的单体的氧化共聚的产物。其特性粘度为约0.04至约0.15分升每克，平均每分子约1.8至约2个羟基。聚（亚芳基醚）共聚物富含低分子量共聚物链和共聚物链，其包括源自二元酚的末端单元。

5. 发明授权

US07595367B2 Poly(arylene ether) preparation method 有权
标题翻译：聚（亚芳基醚）的制备方法
公开(公告)号：US07595367B2
公开(公告)日：2009-09-29
申请号：US11845823
申请日：2007-08-28
申请人： Alvaro Carrillo , Hua Guo , Alexey Kruglov , Edward Norman Peters
发明人： Alvaro Carrillo , Hua Guo , Alexey Kruglov , Edward Norman Peters
IPC分类号： C08F283/08
CPC分类号： C08G65/44 , C08G65/485 , C08L2205/05
摘要： Capped poly(arylene ether)s are prepared by a method that includes reacting a poly(arylene ether) with a capping agent to form a capping reaction mixture, washing the capping reaction mixture with a concentrated basic aqueous solution, and isolating the capped poly(arylene ether) by a total isolation method. The washing method is effective for removal of capping-related impurities, and surprisingly does not result in decomposition of the capped poly(arylene ether).
摘要翻译：通过包括使聚（亚芳基醚）与封端剂反应形成封端反应混合物，用浓缩的碱性水溶液洗涤封端反应混合物并分离封端的聚（亚芳基醚）的聚（亚芳基醚）亚芳基醚）。洗涤方法对于除去封盖相关杂质是有效的，并且令人惊讶地不会导致封端的聚（亚芳基醚）的分解。

6. 发明授权

US07671167B2 Poly(arylene ether) copolymer 有权
标题翻译：聚（亚芳基醚）共聚物
公开(公告)号：US07671167B2
公开(公告)日：2010-03-02
申请号：US12414856
申请日：2009-03-31
申请人： Alvaro Carrillo , Erik René Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
发明人： Alvaro Carrillo , Erik René Delsman , Hua Guo , Alexey Kruglov , Edward N. Peters
IPC分类号： C08G65/38
CPC分类号： C08G65/44 , H05K1/0326
摘要： A poly(arylene ether) copolymer is the product of oxidative copolymerization of monomers including a monohydric phenol and a dihydric phenol. It has an intrinsic viscosity of about 0.04 to about 0.15 deciliter per gram and, on average, about 1.8 to about 2 hydroxyl groups per molecule. The poly(arylene ether) copolymer is enriched in low molecular weight copolymer chains and copolymer chains that include a terminal unit derived from the dihydric phenol.
摘要翻译：聚（亚芳基醚）共聚物是包括一元酚和二元酚的单体的氧化共聚的产物。其特性粘度为约0.04至约0.15分升每克，平均每分子约1.8至约2个羟基。聚（亚芳基醚）共聚物富含低分子量共聚物链和共聚物链，其包括源自二元酚的末端单元。

7. 发明申请

US20090062478A1 POLY(ARYLENE ETHER) PREPARATION METHOD 有权
标题翻译： POLY（ARYLENE ETHER）制备方法
公开(公告)号：US20090062478A1
公开(公告)日：2009-03-05
申请号：US11845823
申请日：2007-08-28
申请人： Alvaro Carrillo , Hua Guo , Alexey Kruglov , Edward Norman Peters
发明人： Alvaro Carrillo , Hua Guo , Alexey Kruglov , Edward Norman Peters
IPC分类号： C08G65/48
CPC分类号： C08G65/44 , C08G65/485 , C08L2205/05
摘要： Capped poly(arylene ether)s are prepared by a method that includes reacting a poly(arylene ether) with a capping agent to form a capping reaction mixture, washing the capping reaction mixture with a concentrated basic aqueous solution, and isolating the capped poly(arylene ether) by a total isolation method. The washing method is effective for removal of capping-related impurities, and surprisingly does not result in decomposition of the capped poly(arylene ether).
摘要翻译：通过包括使聚（亚芳基醚）与封端剂反应形成封端反应混合物，用浓缩的碱性水溶液洗涤封端反应混合物并分离封端的聚（亚芳基醚）的聚（亚芳基醚）亚芳基醚）。洗涤方法对于去除封端相关杂质是有效的，并且令人惊奇地不会导致封端的聚（亚芳基醚）的分解。

8. 发明授权

US08722837B2 Poly(phenylene ether)-polysiloxane composition and method 有权
标题翻译：聚（苯醚） - 聚硅氧烷组合物和方法
公开(公告)号：US08722837B2
公开(公告)日：2014-05-13
申请号：US13362426
申请日：2012-01-31
申请人： Alvaro Carrillo , Hua Guo , Scott Fisher
发明人： Alvaro Carrillo , Hua Guo , Scott Fisher
IPC分类号： C08G65/38 , C08G77/46
CPC分类号： C08L83/12 , C08G65/44 , C08G77/46 , C08K5/34924 , C08L25/00 , C08L27/00 , C08L71/12 , C08L71/123 , C08L71/126
摘要： A composition is prepared by oxidative copolymerization of specific amounts of 2,6-dimethylphenol, 2,3,6-trimethylphenol, and a hydroxyaryl-terminated polysiloxane. The composition exhibits an increased heat resistance relative to a corresponding composition prepared by copolymerizing 2,6-dimethylphenol and hydroxyaryl-terminated polysiloxane, without 2,3,6-trimethylphenol. The composition is useful as a flame-retardant additive in polymer compositions that require high heat resistance.
摘要翻译：通过特定量的2,6-二甲基苯酚，2,3,6-三甲基苯酚和羟基芳基封端的聚硅氧烷的氧化共聚制备组合物。该组合物相对于不含2,3,6-三甲基苯酚共聚2,6-二甲基苯酚和羟基芳基封端的聚硅氧烷制备的相应组合物，具有增加的耐热性。该组合物可用作需要高耐热性的聚合物组合物中的阻燃添加剂。

9. 发明授权

US08669332B2 Poly(arylene ether)-polysiloxane composition and method 有权
标题翻译：聚（亚芳基醚） - 聚硅氧烷组合物和方法
公开(公告)号：US08669332B2
公开(公告)日：2014-03-11
申请号：US13169137
申请日：2011-06-27
申请人： Alvaro Carrillo , Hua Guo
发明人： Alvaro Carrillo , Hua Guo
IPC分类号： C08L71/12 , C08G77/46
CPC分类号： C08G77/46 , C08G77/16 , C08G77/80 , C08G81/00 , C08G2261/126 , C08L71/12 , C08L83/12 , C08L2205/05 , C08L83/04
摘要： A thermoplastic composition that includes a poly(arylene ether)-polysiloxane block copolymer is prepared by a method that includes oxidatively copolymerizing a monohydric phenol and a hydroxyaryl-terminated polysiloxane. The oxidative polymerization includes a monohydric phenol addition period characterized by a first temperature, a build period following the addition period and characterized by a second temperature greater than the first temperature, and a temperature ramp period between the addition period and the build period. During the temperature ramp period, the temperature is increased at an average rate of about 0.01 to about 0.35° C. per minute, which improves the efficiency with which the hydroxyaryl-terminated polysiloxane is incorporated into the poly(arylene ether)-polysiloxane block copolymer.
摘要翻译：包括聚（亚芳基醚） - 聚硅氧烷嵌段共聚物的热塑性组合物通过包括使一元酚和羟基芳基封端的聚硅氧烷氧化共聚的方法制备。氧化聚合包括一元酚添加时间，其特征在于第一温度，加入时间之后的生成周期，并且特征在于大于第一温度的第二温度，以及添加周期和构建周期之间的温度斜坡期间。在温度升高期间，温度以每分钟约0.01至约0.35℃的平均速率增加，这提高了聚（亚芳基醚） - 聚硅氧烷嵌段共聚物中加入羟基芳基封端的聚硅氧烷的效率。

10. 发明申请

US20120329961A1 POLY(ARYLENE ETHER)-POLYSILOXANE COMPOSITION AND METHOD 有权
标题翻译：聚（亚乙基醚） - 聚硅氧烷组合物和方法
公开(公告)号：US20120329961A1
公开(公告)日：2012-12-27
申请号：US13169137
申请日：2011-06-27
申请人： Alvaro Carrillo , Hua Guo
发明人： Alvaro Carrillo , Hua Guo
IPC分类号： C08L83/12 , C08L71/12 , C08L25/06 , C08L77/00 , C08L23/02 , C08G77/46 , C08L67/00
CPC分类号： C08G77/46 , C08G77/16 , C08G77/80 , C08G81/00 , C08G2261/126 , C08L71/12 , C08L83/12 , C08L2205/05 , C08L83/04
摘要： A thermoplastic composition that includes a poly(arylene ether)-polysiloxane block copolymer is prepared by a method that includes oxidatively copolymerizing a monohydric phenol and a hydroxyaryl-terminated polysiloxane. The oxidative polymerization includes a monohydric phenol addition period characterized by a first temperature, a build period following the addition period and characterized by a second temperature greater than the first temperature, and a temperature ramp period between the addition period and the build period. During the temperature ramp period, the temperature is increased at an average rate of about 0.01 to about 0.35° C. per minute, which improves the efficiency with which the hydroxyaryl-terminated polysiloxane is incorporated into the poly(arylene ether)-polysiloxane block copolymer.
摘要翻译：包含聚（亚芳基醚） - 聚硅氧烷嵌段共聚物的热塑性组合物通过包括使一元酚和羟基芳基封端的聚硅氧烷氧化共聚的方法制备。氧化聚合包括一元酚添加时间，其特征在于第一温度，加入时间之后的生成周期，并且特征在于大于第一温度的第二温度，以及添加周期和构建周期之间的温度斜坡期间。在温度升高期间，温度以每分钟约0.01至约0.35℃的平均速率增加，这提高了聚（亚芳基醚） - 聚硅氧烷嵌段共聚物中加入羟基芳基封端的聚硅氧烷的效率。

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