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    • 8. 发明授权
    • Method of producing a ceramic product
    • 陶瓷制品的制造方法
    • US4127416A
    • 1978-11-28
    • US815454
    • 1977-07-13
    • Roland J. LumbyBernard NorthAlfred J. Taylor
    • Roland J. LumbyBernard NorthAlfred J. Taylor
    • C04B35/597C04B35/50C04B35/58
    • C04B35/597
    • A method of producing a ceramic product which comprises the step of forming a powder mixture consisting essentially of a first component consisting of compounds containing the elements silicon, aluminum, oxygen and nitrogen in proportion such that the ratio of the total number of silicon and aluminum atoms to the total number of oxygen and nitrogen atoms lies in the range 0.735 to 0.77 and such that said compounds react together during the subsequent sintering process to produce a single phase ceramic material obeying the general formula:Si.sub.6-z Al.sub.z O.sub.z N.sub.8-zwhere z is between 0.38 and 1.5, and between 0.1 and 10% by weight of a second component in the form of an oxide of at least one of the further elements yttrium, scandium, cerium, lanthanum and the metals of the lanthanide series. The mixture is then sintered in a protective environment at a temperature between 1600.degree. C and 2000.degree. C and for a time, decreasing with increasing temperature, of at least 10 minutes to at least 5 hours so as to produce a ceramic material containing at least 80% by volume of said single phase ceramic material together with a second phase containing said at least one further element.
    • 一种制造陶瓷产品的方法,其包括以下步骤:形成粉末混合物,所述粉末混合物基本上由第一组分组成,所述第一组分由含有元素硅,铝,氧和氮的化合物组成,其比例使得硅和铝原子的总数 氧原子和氮原子的总数位于0.735至0.77的范围内,并且使得所述化合物在随后的烧结过程中一起反应以制备符合以下通式的单相陶瓷材料:
    • 9. 发明授权
    • Method of forming a sintered ceramic product
    • 形成烧结陶瓷制品的方法
    • US3989782A
    • 1976-11-02
    • US535513
    • 1974-12-23
    • Roland John LumbyBernard North
    • Roland John LumbyBernard North
    • C04B35/111C04B35/597C04B33/32C04B35/58
    • C04B35/597C04B35/111
    • In a method of forming a sintered, ceramic product, aluminium nitride is reacted with silica at a temperature of between 1200.degree. and 2000.degree. C to form a single phase silicon aluminium oxynitride ceramic material, the reaction mixture at said temperature containing not more than 60% by weight of the aluminium nitride and also containing first and second metal oxides other than silica. The metal oxides are arranged so that they do not introduce into the mixture a combination of magnesium oxide and alumina alone and further are arranged so that during the reaction they combine with part of said silica to form a silicate glass having a liquidus temperature below that of the silicate glass which would be formed from silica with either of said metal oxides alone. The silicate glass formed then aids densification of the ceramic material during sintering.
    • 在形成烧结陶瓷产品的方法中,氮化铝与二氧化硅在1200至2000℃的温度下反应形成单相硅铝氧氮化物陶瓷材料,所述温度下的反应混合物不超过60 重量百分比的氮化铝,并且还含有除二氧化硅以外的第一和第二金属氧化物。 金属氧化物的布置使得它们不会将氧化镁和氧化铝的组合单独引入到混合物中,并且进一步布置成使得在反应期间,它们与部分二氧化硅结合以形成液体温度低于 将由二氧化硅与任何一种所述金属氧化物单独形成的硅酸盐玻璃。 所形成的硅酸盐玻璃在烧结过程中有助于陶瓷材料的致密化。