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1. 发明授权

US5332789A Polypropylene block copolymer resin and compositions 失效
标题翻译：聚丙烯嵌段共聚物树脂和组合物
公开(公告)号：US5332789A
公开(公告)日：1994-07-26
申请号：US974591
申请日：1993-02-26
申请人： Akira Tanaka , Masaru Nakagawa , Hideo Kusuyama , Sueto Miyazaki , Tatsuya Housaki
发明人： Akira Tanaka , Masaru Nakagawa , Hideo Kusuyama , Sueto Miyazaki , Tatsuya Housaki
IPC分类号： C08F110/06 , C08F210/06 , C08F297/08 , C08L51/06
CPC分类号： C08L51/06 , C08F210/06 , C08F297/083 , C08F110/06 , Y10S526/905
摘要： Polypropylene based resins and compositions comprising the resin having extremely high stiffness, heat resistance and impact strength, with these properties being well-balanced, are provided. The polypropylene based resins are characterized by comprising:(1) a propylene polymer having a content of alpha-olefin other than propylene of not more than 4 mole percent, and the following properties (2), (3) and (4):(2) a pentad fraction (mmmm fraction) measured by .sup.13 C-NMR of not less than 96.0 percent,(3) a main elution fraction peak position of not less than 118.0.degree. C. and a peak half value width of less than 4.0, these values being measured by the temperature raising separation method, and(4) an intrinsic viscosity of not less than 0.5 dl/g, but not more than 5.0 dl/g; and,(5) a rubber content measured by pulse NMR of more than 25 percent.
摘要翻译： PCT No.PCT / JP92 / 00807 Sec。 371日期：1993年2月26日 102（e）日期1993年2月26日PCT提交1992年6月25日PCT公布。出版物WO93 / 00375 日本1993年1月7日。提供了包含具有非常高的刚度，耐热性和冲击强度的树脂的聚丙烯基树脂和组合物，这些性能是均衡的。聚丙烯类树脂的特征在于包括：（1）具有不大于4摩尔％的丙烯以外的α-烯烃含量的丙烯聚合物和以下性质（2），（3）和（4）：（ 2）通过13 C-NMR测定的五元组分数（mmmm分数）不小于96.0％，（3）主洗脱分数峰位置不低于118.0℃，峰值半值宽度小于4.0，这些通过升温分离法测定的值，（4）特性粘度为0.5dl / g以上，5.0dl / g以下，和（5）通过脉冲NMR测量的橡胶含量超过25％。

2. 发明授权

US5231163A Polyarylene sulfide from aromatic compound having at least three functional groups 失效
标题翻译：具有至少三个官能团的芳族化合物的聚芳硫醚
公开(公告)号：US5231163A
公开(公告)日：1993-07-27
申请号：US746819
申请日：1991-08-15
申请人： Wataru Kosaka , Minoru Senga , Norio Ogata , Tatsuya Housaki
发明人： Wataru Kosaka , Minoru Senga , Norio Ogata , Tatsuya Housaki
IPC分类号： C08G75/02 , C08K7/14
CPC分类号： C08G75/025 , C08G75/0222 , C08G75/0231 , C08K7/14
摘要： A polyarylene sulfide has an inherent viscosity [.eta..sub.i n h ] of 0.1 to 0.5 dl/g, a weight-average molecular weight of 1.times.10.sup.4 to 2.times.10.sup.5 ; a ratio of the inherent viscosity [.eta..sub.i n h ] to a calculated viscosity [.eta.].sub.calc ([.eta..sub.i n h /[.eta.].sub.calc) of 0.4/1 to 0.8/1; and a degree of whiteness of 50 or higher when measured in accordance with whiteness testing procedures (JIS P8123). The polyarylene sulfide is prepared by reaction by contacting at least one member of a metallic sulfide (A) selected from an alkali metal sulfide and an alkali metal hydrosulfide with a dihalogen aromatic compound (B) and an aromatic compound (C) having three or more than three functional groups in a polar solvent in a molar ratio of the dihalogen aromatic compound (B) to the metallic sulfide (A) [(B)/(A)] ranging from 1.035/1 to 1.300/1 and in a molar ratio of the aromatic compound (C) to the dihalogen aromatic compound (B) [(C)/(B)] ranging from 0.003/1 to 0.05/1.A polyarylene sulfide resin composition contains the polyarylene sulfide having the above properties and and at least one member of a filler selected from a fiber filler and a powdery or granular filler.The polyarylene sulfide resin composition has the mechanical strength, heat resistance, long-term stability, and chemical resistance superior to the polyarylene sulfide.
摘要翻译：聚芳硫醚的特性粘度[η]为0.1〜0.5dl / g，重均分子量为1×10 4〜2×105; 特性粘度[η] h与计算出的粘度η（h /η/ calc）的比值为0.4 / 1至0.8 / 1; 并且根据白度测试程序（JIS P8123）测量时白度为50或更高。通过使选自碱金属硫化物和碱金属氢硫化物的金属硫化物（A）的至少一种与二卤代芳香族化合物（B）和具有三个以上的碱金属硫化物的芳香族化合物（C）接触而使反应来制备聚芳硫醚在极性溶剂中的三官能团，二卤代芳香族化合物（B）与金属硫化物（A）[（B）/（A）]的摩尔比为1.035 / 1〜1.300 / 1，摩尔比的芳族化合物（C）与二卤代芳香族化合物（B）[（C）/（B）]的比例为0.003 / 1〜0.05 / 1。聚芳硫醚树脂组合物含有具有上述性能的聚芳硫醚和至少一种选自纤维填料和粉末或颗粒填料的填料。聚芳硫醚树脂组合物具有优于聚芳硫醚的机械强度，耐热性，长期稳定性和耐化学性。

3. 发明授权

US07531605B2 Process for producing polyolefin resin composition and polypropylene composition 失效
标题翻译：生产聚烯烃树脂组合物和聚丙烯组合物的方法
公开(公告)号：US07531605B2
公开(公告)日：2009-05-12
申请号：US10469701
申请日：2002-03-12
申请人： Shuji Machida , Masayuki Shinohara , Tatsuya Housaki
发明人： Shuji Machida , Masayuki Shinohara , Tatsuya Housaki
IPC分类号： C08F210/06 , C08F210/16 , C08F236/02 , C08F4/642 , C08F4/6592
CPC分类号： C08L23/10 , C08F4/65904 , C08F4/65912 , C08F4/65927 , C08F10/00 , C08F10/06 , C08F110/06 , C08F210/06 , C08F212/08 , C08F255/00 , C08F257/02 , C08F297/06 , C08F297/08 , C08L23/02 , C08L51/06 , C08L2205/02 , C08L2205/025 , C08L2308/00 , C08F4/65916 , C08F2/001 , C08L2666/06 , C08L2666/04 , C08L2666/02 , C08F2500/12 , C08F2500/18 , C08F2500/11 , C08F2500/17 , C08F210/08 , C08F210/14 , C08F2500/09 , C08F236/20 , C08F210/18 , C08F210/16
摘要： A process for producing a polyolefin-based resin composition comprises, in the first polymerization stage, polymerizing an α-olefin having 4 to 20 carbon atoms, a styrene or a cyclic olefin in the presence of a specific catalyst and, in the second polymerization stage, copolymerizing the obtained polymer with an α-olefin having 2 to 20 carbon atoms, a styrene or a cyclic olefin in the presence of a polyene. A polypropylene composition has a branching parameter a and a branching index g in specific ranges. The curve showing the change in viscosity under elongation with time, the degradation parameter D or the content of a high molecular weight component is specified. The polyolefin-based resin composition exhibits excellent uniformity and improved workability in melting due to improved tension in melted condition. The polypropylene composition exhibits excellent melting elasticity and secondary workability and provides foamed molded articles, sheets and blow molded articles.
摘要翻译：聚烯烃类树脂组合物的制造方法在第一聚合阶段中，在特定催化剂的存在下，使具有4〜20个碳原子的α-烯烃，苯乙烯或环状烯烃聚合，在第二聚合阶段在多烯存在下，使得到的聚合物与碳原子数2〜20的α-烯烃，苯乙烯或环状烯烃共聚。聚丙烯组合物具有特定范围内的支化参数a和支化指数g。规定了随时间延伸的粘度变化，降解参数D或高分子量成分的含量的曲线。聚烯烃类树脂组合物由于熔融条件下的张力提高而表现出优异的均匀性和改善的熔融加工性。聚丙烯组合物显示出优异的熔融弹性和二次加工性，并提供发泡成型制品，片材和吹塑制品。

4. 发明授权

US06310167B1 Ethylene homopolymer and its molded article 失效
标题翻译：乙烯均聚物及其模塑制品
公开(公告)号：US06310167B1
公开(公告)日：2001-10-30
申请号：US09373194
申请日：1999-08-12
申请人： Mitsugu Kanzawa , Fumio Okuda , Tatsuya Housaki , Tomio Tatsumi
发明人： Mitsugu Kanzawa , Fumio Okuda , Tatsuya Housaki , Tomio Tatsumi
IPC分类号： C08F1002
CPC分类号： C08F110/02 , C08F10/00 , C08F2500/10 , C08F2500/12 , C08F2500/08 , C08F4/7006
摘要： Provided are an ethylene homopolymer having well-balanced properties of good heat resistance, good heat-sealability and good moldability, and its molded articles. The ethylene homopolymer is characterized in that the number of butyl branches per 100 methyl branches therein falls between 1 and 20, as measured through 13C-NMR, that its density, d (kg/m3), falls between 880 and 980, and that the density, d, and its melting point, Tm (° C.) , satisfy the conditions defined by the following formulae (1) to (3): Tm≧1.2×d−982 (980≧d≧925) (1), Tm≧0.6×d−430 (925>d≧915) (2), Tm≧0.16×d−28.4 (915>d≧880) (3). The ethylene homopolymer is molded into moldings.
摘要翻译：提供具有良好的耐热性，良好的热封性和良好的成型性的良好平衡性的乙烯均聚物及其模塑制品。乙烯均聚物的特征在于，通过13 C-NMR测量，其每100个甲基支链中的丁基支链数目在1和20之间，其密度d（kg / m 3）在880和980之间，密度d及其熔点Tm（℃）满足由下式（1）至（3）定义的条件：将乙烯均聚物模塑成型。

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