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1. 发明授权

US4900628A Gaseous phase synthesized diamond and method for synthesizing same 失效
标题翻译：气相合成金刚石及其合成方法
公开(公告)号：US4900628A
公开(公告)日：1990-02-13
申请号：US76721
申请日：1987-07-22
申请人： Akihiko Ikegaya , Masaaki Tobioka
发明人： Akihiko Ikegaya , Masaaki Tobioka
IPC分类号： C30B25/02
CPC分类号： C30B25/02 , C30B29/04 , Y10T428/30
摘要： The present invention relates to gaseous phase synthesized diamond and a method of synthesizing the same. In order to obtain crystalline diamond having remarkably high completeness and hardly containing carbon having a construction other than that of diamond, raw material gases are thermally activated by a thermoelectron-radiating material heated at an extremely high temperature, the thermoelectron-radiating material being connected to a negative pole while a substrate to be coated is connected to a positive pole, by the use of a direct current power source, a plasma being formed between the thermoelectron-radiating material and the substrate by applying a direct current voltage, and a diamond film having an average particle size of 2 microns or less, compression residual stress and electric resistance of 10.sup.8 ohm.cm or more being formed on the substrate by using the activation by the thermoelectron-radiating material together with the activation by the formation of DC plasma.In addition, homogeneous diamond particles uniform in shape can be obtained by using this method.

2. 发明授权

US5112643A Gaseous phase synthesized diamond and method for synthesizing same 失效
标题翻译：气相合成金刚石及其合成方法
公开(公告)号：US5112643A
公开(公告)日：1992-05-12
申请号：US754318
申请日：1991-09-04
申请人： Akihiko Ikegaya , Masaaki Tobioka
发明人： Akihiko Ikegaya , Masaaki Tobioka
IPC分类号： C30B25/02
CPC分类号： C30B25/02 , C30B29/04 , Y10T428/30
摘要： The present invention relates to gaseous phase synthesized diamond and a method for synthesizing the same. In order to obtain crystalline diamond having remarkably high completeness and hardly containing carbon having a construction other than that of diamond, raw material gases are thermally activated by a thermoelectron-radiating material heated at an extremely high temperature, the thermoelectron-radiating material being connected to a negative pole while a substrate to be coated is connected to a positive pole, by the use of a direct current power source, a plasma being formed between the thermoelectron-radiating material and the substrate and the substrate by applying a direct current voltage, and a diamond film having an average particle size of 2 microns or less, compression residual stress and electric resistance of 10.sup.8 ohm.cm or more being formed on the substrate by using the activation by the thermoelectron-radiating material together with the activation by the formation of DC plasma.In addition, homogeneous diamond particles uniform in shape can be obtained by using this method.

3. 发明授权

US4859490A Method for synthesizing diamond 失效
标题翻译：金刚石合成方法
公开(公告)号：US4859490A
公开(公告)日：1989-08-22
申请号：US75470
申请日：1987-07-20
申请人： Akihiko Ikegaya , Masaaki Tobioka
发明人： Akihiko Ikegaya , Masaaki Tobioka
IPC分类号： C30B25/02
CPC分类号： C30B25/02 , C30B29/04
摘要： A method and apparatus for synthesizing diamond film or coating by applying low-pressurized vapor phase capable of precipitating diamond on the surface of a substrate by activating gas composed of carbon including solid carbon, hydrocarbon, and carbon tetrachloride respectively being mixed with hydrogen. More particularly, the invention relates to an apparatus and method of synthesizing diamond by disposing a grid between a thermoelectron-radiating material heated with activated material gas to a minimum of 1,600.degree. C., and the substrate to be coated, where the thermoelectron radiating material and grid are respectively used for the negative and positive electrodes, followed by provision of potentials by causing the positive and negative electrodes to respectively be connected to the grid and the substrate by arranging another power supply source. The method of synthesizing diamond according to the invention securely generates extremely fine crystalline diamond particles each having a maximum of 2 .mu.m of diameter and provides extremely consummate diamond film having a minimum of 10.sup.10 .OMEGA..multidot.cm of electric resistance, which is substantially the guide for determining the residal amount of carbon such as amorphous carbon and graphite.

4. 发明授权

US4675206A Process for the production of a surface-coated article 失效
标题翻译：用于生产表面涂层制品的方法
公开(公告)号：US4675206A
公开(公告)日：1987-06-23
申请号：US849523
申请日：1986-04-08
申请人： Akihiko Ikegaya , Masaaki Tobioka
发明人： Akihiko Ikegaya , Masaaki Tobioka
IPC分类号： C23C16/30 , C23C16/517 , B05D3/06
CPC分类号： C23C16/517 , C23C16/30
摘要： A surface-coated article or part, for example, hard material-coated steels or cemented carbides for cutting tools, wear resisting tools, sliding parts or decoration articles, having good properties comparable to those obtained by the PVD method, can be produced by a plasma CVD method characterized by using jointly a high frequency source and a direct current source as a plasma exciting source, holding a substrate or base metal at a negative potential by the direct current source and adjusting a high frequency power density applied to a plasma-forming space to 0.01 to 1 W/cm.sup.3, an absolute value of a direct current voltage to at most 1500 V and a gaseous atmosphere pressure to 0.05 to 5 Torr.
摘要翻译：表面涂层制品或部件，例如硬质材料涂覆的钢或用于切削工具的耐磨工具，滑动部件或装饰制品的硬质材料涂层钢或硬质合金，具有与通过PVD方法获得的性能相当的良好性能，可以通过等离子体CVD方法的特征在于共同使用高频源和直流电源作为等离子体激发源，通过直流源将衬底或母体金属保持在负电位，并调整施加到等离子体形成的高频功率密度空间为0.01〜1W / cm 3，直流电压的绝对值为1500V以下，气氛气压为0.05〜5Torr。

5. 发明授权

US5480601A Method for producing an elongated sintered article 失效
标题翻译：生产细长烧结制品的方法
公开(公告)号：US5480601A
公开(公告)日：1996-01-02
申请号：US355814
申请日：1994-12-14
申请人： Susumu Yamamoto , Teruyuki Murai , Nozomu Kawabe , Masaaki Tobioka
发明人： Susumu Yamamoto , Teruyuki Murai , Nozomu Kawabe , Masaaki Tobioka
IPC分类号： B22F3/12 , B23K35/32 , B23K35/40 , C22C29/06 , C04B33/34
CPC分类号： C22C29/06 , B22F3/12 , B22F3/1208 , B23K35/327 , B23K35/406 , B22F2998/00
摘要： Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult of shaping or moulding by conventional process such as wire-drawing, rolling or extrusion of powder material and are difficult of machining or processing after the powder material is sintered.
摘要翻译：一种细长烧结制品的制造方法，其特征在于包括将粉末材料填充到管中，对填充有粉末材料的管进行塑性变形，以及加热填充有粉末材料的管以烧结和/或烧结粉末材料。本发明的方法有利地适用于陶瓷线或棒的生产，特别是所谓的新陶瓷或微细陶瓷，烧结合金或它们的组合，其难以通过常规方法成形或成型，例如拉丝，轧制或粉末材料的挤出，并且在粉末材料烧结后难以进行机械加工或加工。

6. 发明授权

US4746563A Multilayer coated cemented carbides 失效
标题翻译：多层涂层硬质合金
公开(公告)号：US4746563A
公开(公告)日：1988-05-24
申请号：US729973
申请日：1985-05-02
申请人： Minoru Nakano , Masaaki Tobioka
发明人： Minoru Nakano , Masaaki Tobioka
IPC分类号： C23C16/30 , B23P15/28 , C23C16/32 , C23C16/34 , C23C16/36 , C23C16/40 , C23C30/00 , B32B7/02 , B24D3/02 , B32B9/00 , C23C16/00
CPC分类号： C23C30/005 , Y10S428/932 , Y10T428/12576 , Y10T428/24975 , Y10T428/24983
摘要： Multilayer coated cemented carbides excellent in wear resistance and toughness are provided comprising a substrate of cemented carbide, an inner layer contacted with the surface of the substrate, and an outer layer contacted with the inner layer, the inner layer being a single layer and/or laminated layers consisting of at least one member selected from the group consisting of carbides, nitrides, carbonitrides, carboxynitrides, oxynitrides, boronitrides and borocarbonitrides of Ti, and the outer layer being a multilayer with a total thickness of 5 to 20 .mu.m, consisting of a plurality of Al.sub.2 O.sub.3 layer each having a thickness of 0.01 to 2 .mu.m, each consisting of an Al.sub.2 O.sub.3 film in which titanium oxide is dissolved or at most 30 vol % of titanium oxide is coexistent and being respectively divided by interlayers each having a thickness of 0.01 to 2 .mu.m and each consisting of at least one member of the group consisting of TiC, TiN, TiCN, TiCNO, TiNO, Ti oxides Ti(B, N), Ti(B, N, C), SiC, AlN and AlON.
摘要翻译：提供耐磨性和韧性优异的多层涂层胶结碳化物，其包括硬质合金基材，与基材表面接触的内层和与内层接触的外层，内层为单层和/或由选自碳化物，氮化物，碳氮化物，羧基氮化物，氧氮化物，硼氮化物和硼碳氮化物中的至少一种的Ti组成的层叠层，外层为总厚度为5至20μm的多层，由多个Al 2 O 3层，各自具有0.01至2μm的厚度，每个Al 2 O 3层由其中溶解有氧化钛的Al 2 O 3膜或至多30vol％的氧化钛共存并分别由具有厚度为 0.01〜2μm，分别由TiC，TiN，TiCN，TiCNO，TiNO，Ti氧化物Ti（B，N），Ti（B，N，C），SiC，AlN 和Alon。

7. 发明授权

US5252288A Method for producing an elongated sintered article 失效
标题翻译：生产细长烧结制品的方法
公开(公告)号：US5252288A
公开(公告)日：1993-10-12
申请号：US883368
申请日：1992-05-15
申请人： Susumu Yamamoto , Teruyuki Murai , Nozomu Kawabe , Masaaki Tobioka
发明人： Susumu Yamamoto , Teruyuki Murai , Nozomu Kawabe , Masaaki Tobioka
IPC分类号： B22F3/12 , B23K35/32 , B23K35/40 , C22C29/06 , B22F3/24 , C22F1/00
CPC分类号： B22F3/12 , B22F3/1208 , B23K35/327 , B23K35/406 , C22C29/06 , B22F2998/00
摘要： Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult to shape or mold by conventional process such as wire-drawing, rolling or extrusion of powder material which is difficult to mold and machine after the powder material is sintered.
摘要翻译：一种细长烧结制品的制造方法，其特征在于包括将粉末材料填充到管中，对填充有粉末材料的管进行塑性变形，以及加热填充有粉末材料的管以烧结和/或烧结粉末材料。本发明的方法有利地适用于陶瓷线或棒的生产，特别是所谓的新陶瓷或微细陶瓷，烧结合金或它们的组合，其难以通过常规方法如拉丝，轧制形成或模制或挤出粉末材料，在粉末材料烧结后难以模塑和机械加工。

8. 发明授权

US4169913A Coated tool steel and machining tool formed therefrom 失效
标题翻译：包装工具钢和加工工具
公开(公告)号：US4169913A
公开(公告)日：1979-10-02
申请号：US882893
申请日：1978-03-01
申请人： Mitsunori Kobayashi , Yoshihiko Doi , Masaaki Tobioka , Takaharu Yamamoto
发明人： Mitsunori Kobayashi , Yoshihiko Doi , Masaaki Tobioka , Takaharu Yamamoto
IPC分类号： B23B27/14 , C23C14/06 , C23C30/00 , B32B15/18
CPC分类号： B23B27/148 , C23C14/06 , C23C30/00 , Y10S428/911 , Y10T428/24983 , Y10T428/31
摘要： There is provided a coated tool steel having a tool steel substrate and at least one layer of a hard film overcoated on the substrate. The film consists of a B-1 type solid solution selected from carbides, nitrides and carbonitrides of at least one of titanium, zirconium or hafnium, and the breadth of the peak, at half maximum intensity, of Cu-K.alpha. diffraction from the (200) plane of the film, being not less than 0.4 degree on a 2 .theta. scale. The invention further provides a machine tool having at least one cutting part thereof formed from the coated tool steel described above. The coated steel provided herein has excellent wear resistance.

9. 发明授权

US5266389A Surface-coated hard material for cutting tools or wear resistance tools 失效
标题翻译：用于切割工具或耐磨工具的表面涂层硬质材料
公开(公告)号：US5266389A
公开(公告)日：1993-11-30
申请号：US691020
申请日：1991-06-27
申请人： Naoya Omori , Kazuo Yamagata , Toshio Nomura , Masaaki Tobioka
发明人： Naoya Omori , Kazuo Yamagata , Toshio Nomura , Masaaki Tobioka
IPC分类号： C23C14/06
CPC分类号： C23C14/0641 , C23C14/0635 , C23C14/0664 , Y10T428/24975
摘要： A surface-coated hard material for a cutting tool or wear resistance tool is provided which is excellent in wear resistance, deposition resistance and breakage resistance and exhibits good cutting performances for a long time, as a cutting tool or a wear resistance tool, in not only a low speed cutting but also a high speed cutting, and in which a layer consisting of a carbide, nitride or carbonitride of Ti, Zr or Hf and a layer consisting of a carbide, nitride or carbonitride of Al are alternately laminated to form at least 10 hard coating layers.
摘要翻译： PCT No.PCT / JP90 / 01258 Sec。 371日期1991年6月27日 102（e）1991年6月27日PCT PCT 1990年9月28日PCT公布。第WO91 / 05076号公报日本1991年04月18日提供了一种用于切削工具或耐磨工具的表面涂层硬质材料，其耐磨性，耐沉积性和耐断裂性优异，长时间显示出良好的切割性能，作为切削工具或耐磨工具，不仅是低速切削而且是高速切削，其中由Ti，Zr或Hf的碳化物，氮化物或碳氮化物组成的层和由碳化物，氮化物或碳氮化物组成的层 Al交替层压以形成至少10个硬涂层。

10. 发明授权

US5116694A Coated cemented carbides 失效
标题翻译：涂层碳酸钙
公开(公告)号：US5116694A
公开(公告)日：1992-05-26
申请号：US709786
申请日：1991-06-03
申请人： Hiroshi Tsukada , Masaaki Tobioka , Toshio Nomura , Yasuhiro Saito
发明人： Hiroshi Tsukada , Masaaki Tobioka , Toshio Nomura , Yasuhiro Saito
IPC分类号： C04B41/89 , B23B27/14 , B23C5/16 , C23C14/06 , C23C30/00
CPC分类号： C23C14/0664 , C23C14/0635 , C23C30/005 , Y10T428/24975
摘要： A coated cemented carbide with an improved wear resistance without lowering the toughness as a tool is provided comprising a substrate of a cemented carbide, the surface of which is coated with a multilayer of TiC, TiN and TiCN by the PVD method, the innermost layer in contact with the substrate being a TiN layer with a thickness of 0.1 to 1 .mu.m.
摘要翻译：提供了具有改善的耐磨性的涂层硬质合金，而不降低作为工具的韧性，包括硬质合金的基材，其表面通过PVD方法涂覆有多层TiC，TiN和TiCN，最内层与厚度为0.1〜1μm的TiN层的基板接触。

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