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1. 发明申请

WO2008074733A1 PROCESS FOR THE CATALYTIC HALOGENATION OF A HYDROXYLATED ORGANIC COMPOUND 审中-公开
标题翻译：羟化有机化合物催化反应的方法
公开(公告)号：WO2008074733A1
公开(公告)日：2008-06-26
申请号：PCT/EP2007/063944
申请日：2007-12-14
申请人： AKZO NOBEL N.V. , TEN KATE, Antoon , MAYER, Mateo Jozef Jacques , VAN STRIEN, Cornelis Johannes Govardus , KUZMANOVIC, Boris , DIRIX, Carolina Anna Maria Christina
发明人： TEN KATE, Antoon , MAYER, Mateo Jozef Jacques , VAN STRIEN, Cornelis Johannes Govardus , KUZMANOVIC, Boris , DIRIX, Carolina Anna Maria Christina
IPC分类号： C07C29/62 , C07D301/26 , C07D303/14
CPC分类号： C07C29/62 , C07C31/36 , C07C31/42
摘要： The present invention relates to a process for the catalytic halogenation of an organic compound comprising at least one aliphatic hydroxyl group which comprises the step of contacting the organic compound comprising at least one aliphatic hydroxyl group with a hydrogen halide in the presence of a catalyst which is an organic polymer which comprises at least one carbonyl group, has a vapour pressure at the reaction temperature of less than 1 mbar, has a weight average molecular weight M w of 500 g/mole or more, and is soluble in the reaction mixture at the reaction temperature.
摘要翻译：本发明涉及一种包含至少一种脂族羟基的有机化合物的催化卤化方法，该方法包括在催化剂存在下使包含至少一个脂族羟基的有机化合物与卤化氢接触的步骤包含至少一个羰基的反应温度小于1毫巴的蒸气压的有机聚合物的重均分子量M w w为500g / mol以上，并且为在反应温度下可溶于反应混合物。

2. 发明申请

WO2006045795A2 PROCESSES INVOLVING THE USE OF ANTISOLVENT CRYSTALLIZATION 审中-公开
标题翻译：涉及使用抗溶剂结晶的过程
公开(公告)号：WO2006045795A2
公开(公告)日：2006-05-04
申请号：PCT/EP2005/055527
申请日：2005-10-25
申请人： AKZO NOBEL N.V. , BARGEMAN, Gerrald , DEMMER, René, Lodewijk, Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis, Elizabeth, Johannus , MAYER, Mateo, Jozef, Jacques , SCHUTYSER, Maarten, André, Irène , VAN STRIEN, Cornelis, Johannes, Govardus
发明人： BARGEMAN, Gerrald , DEMMER, René, Lodewijk, Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis, Elizabeth, Johannus , MAYER, Mateo, Jozef, Jacques , SCHUTYSER, Maarten, André, Irène , VAN STRIEN, Cornelis, Johannes, Govardus
CPC分类号： C01D3/16 , C01D3/06
摘要： The present invention pertains to a process involving the use of an antisolvent comprising the steps of - feeding water to a salt source to form an aqueous solution comprising said salt if the salt source is not yet in the form of an aqueous salt solution, - feeding said aqueous solution to a crystallizer/settler, - contacting said aqueous solution with one or more antisolvents which force the salt to at least partly crystallize, with one or more crystal growth inhibitors being present in the antisolvents and/or in the aqueous solution, and/or one or more scaling inhibitors being present in the antisolvents and/or in the aqueous solution, - subjecting an overflow of the crystallizer/settler comprising one or more antisolvents and an aqueous salt solution to a separation step wherein one or more antisolvents are separated from the aqueous salt solution by one or more techniques selected from the group consisting of adsorption, ion-exchange, a temperature change induced phase split, a pH change induced phase split, a complexation induced phase split, a pressure induced phase split, evaporation, and extraction, optionally in combination with a nanofiltration step, - removing the crystallized salt from the crystallizer/settler in an aqueous slurry, - optionally, recycling the one or more antisolvents to the crystallizer/settler, and - optionally, recycling mother liquor from the slurry to the first dissolution step and/or to the crystallizer/settler. Preferably, the process is a closed loop process and the salt is sodium chloride. Preferably, the process further comprises a reverse osmosis step before the overflow of the crystallizer/settler is subjected to the separation step.
摘要翻译：本发明涉及涉及使用抗溶剂的方法，所述方法包括以下步骤： - 如果盐源尚未处于形式，则将水供给至盐源以形成包含所述盐的水溶液 - 将所述水溶液加入结晶器/沉降器中， - 将所述水溶液与一种或多种抗溶剂接触，所述抗溶剂迫使盐至少部分结晶，其中一种或多种晶体生长抑制剂存在于抗溶剂中，和 /或在水溶液中，和/或一种或多种结垢抑制剂存在于抗溶剂和/或水溶液中， - 使包含一种或多种抗溶剂和盐水溶液的结晶器/沉降器的溢流经受分离其中通过选自以下的一种或多种技术从盐水溶液中分离出一种或多种抗溶剂：吸附，离子交换，温度变化诱导的相分离，pH变化诱导相分离，络合诱导相分离，压力诱导相分离，蒸发和萃取，任选地与纳米过滤步骤组合， - 在含水浆液中从结晶器/沉降器中除去结晶盐， - 任选地，将所述一种或多种反溶剂再循环至结晶器/沉降器，以及 - 任选地将母液从淤浆循环至第一溶解步骤和/或结晶器/沉降器。优选地，该过程是闭环过程并且盐是氯化钠。优选地，该方法还包括在结晶器/沉降器溢流进行分离步骤之前的反渗透步骤。

3. 发明申请

WO2009016235A2 CHELATING AGENT BASED IONIC LIQUIDS, A PROCESS TO PREPARE THEM, AND THEIR USE 审中-公开
标题翻译：基于代理的离子液体，制备方法及其使用
公开(公告)号：WO2009016235A2
公开(公告)日：2009-02-05
申请号：PCT/EP2008/060066
申请日：2008-07-31
申请人： Akzo Nobel N.V. , DE WOLF, Cornelia Adriana , KUZMANOVIC, Boris , BEMELAAR, Johanna Hendrika , VAN STRIEN, Cornelis Johannes Govardus , HEUS, Martin , TEN KATE, Antoon
发明人： DE WOLF, Cornelia Adriana , KUZMANOVIC, Boris , BEMELAAR, Johanna Hendrika , VAN STRIEN, Cornelis Johannes Govardus , HEUS, Martin , TEN KATE, Antoon
IPC分类号： C07C211/63 , C07C215/40 , C07C229/16 , C07C229/76 , C07F9/54
CPC分类号： C07C229/16 , C07C211/63 , C07C215/40 , C07C229/76 , C07F9/5407
摘要： The present invention relates to ionic liquids of the formula: (M m+ ) x H + y nN + R 1 R 2 R 3 R 4 Z-N(-CHXCOO - ) p Y 2-p or (M m+ ) x H + y nP + R 1 R 2 R 3 R 4 Z-N(-CHXCOO - ) p Y 2-p wherein any one of R 1 to R 4 independently represents a hydrogen, alkyl, cycloalkyl, aryl or aralkyl group that may be unsubstituted or substituted with one or more groups selected from OH, Cl, Br, F, I, phenyl, NH 2 , CN, NO 2, an ether group, COOR 5 , CHO, COR 5 or OR 5 , wherein R 5 is an alkyl or cycloalkyl group, and wherein two of the groups R 1 to R 4 together with the N atom may form a heteroaromatic or heterocyclic group such as a pyridinium, pyrrolidinium or imidazolium group; the Z-N(-CHXCOO - )pY 2-p is the anion derived from a chelating agent, wherein Z is a group selected from hydrogen, alkyl, an alkyl group optionally substituted with one or more carboxylate groups, hydroxyl groups and/or optionally containing one or more ether functionalities, or Z is a group of the formula -CH 2 -CHR 6 -R 7 -N-(CH 2 COO - ) 2 , R 6 is hydrogen or a C 1 -C 3 alkyl group, R 7 is a single bond, a C 1 -C 3 alkylene group or one or more groups of the formula -N(CH 2 COO - )-CH 2 -CHR 6 -R 8 -, R 8 is a single bond or a C 1 -C 3 alkylene group, p is 2 or 1, X is H, an aryl group that may be unsubstituted or substituted with an OH and/or CH 3 substituent, or CH 2 COO - , and when p is 1, Y is H, a benzyl group that may be unsubstituted or substituted with an OH and/or CH 3 group, or a phenyl group that may be unsubstituted or substituted with an OH and/or CH 3 substituent, M m+ is a m-valent metal cation, n is 1 or higher, x is from 0 to 5, y is from 0 to 3, the total positive charge of (M m+ ) x , H + y ,and nN + R 1 R 2 R 3 R 4 or nP + R 1 R 2 R 3 R 4 equals the negative charge of the Z-N(-CHXCOO - ) p Y 2-p anion, wherein at least one of the following conditions is fulfilled: i) the chelating agent has a connectivity index 1 X/ 3 X of below 2.17, ii) at least two different cations are present in the salt, whereby a proton cation does not count as one of the at least two, iii) at least one cation is a bivalent, trivalent, tetravalent or pentavalent cation, and having a melting point below 120°C. The invention further relates to a process to prepare them and their use.
摘要翻译：本发明涉及下式的离子液体：（Mm +）xH + y nN + R1R2R3R4ZN（-CHXCOO-）pY2-p或（Mm +）xH + ynP + R1R2R3R4Z-N（-CHXCOO-）pY2-p其中任何 R 1至R 4中的一个独立地表示氢，烷基，环烷基，芳基或芳烷基，其可以是未取代的或被一个或多个选自OH，Cl，Br，F，I，苯基，NH 2，CN，NO 2，醚基，COOR 5，CHO，COR 5或OR 5，其中R 5是烷基或环烷基，并且其中R 1至R 4中的两个与N原子一起可以形成杂芳族或杂环基，例如吡啶鎓，吡咯烷鎓或咪唑鎓基团 ; ZN（-CHXCOO-）pY2-p是衍生自螯合剂的阴离子，其中Z是选自氢，烷基，任选被一个或多个羧酸酯基团取代的烷基，羟基和/或任选地含有一个或更多的醚官能团，或Z是式-CH2-CHR6-R7-N-（CH2COO-）2的基团，R6是氢或C1-C3烷基，R7是单键，C1-C3亚烷基基团或一个或多个式-N（CH 2 COO - ） - CH 2 - CHR 6 -R 8 - 的基团，R 8是单键或C 1 -C 3亚烷基，p是2或1，X是H，可以是未被取代的或被OH和/或CH 3取代基或CH 2 COO-取代的，当p是1时，Y是H，可以是未取代的或被OH和/或CH 3基团取代的苄基或苯基其可以是未取代的或被OH和/或CH 3取代基取代，M m +是m价金属阳离子，n为1或更高，x为0至5，y为0至3，（ Mm +）x，H + y和nN + R1R2R3R4或 nP + R1R2R3R4等于ZN（-CHXCOO-）pY2-p阴离子的负电荷，其中满足以下条件中的至少一个：i）螯合剂具有低于2.17的连续性指数1 X / 3 X，ii ）盐中存在至少两种不同的阳离子，其中质子阳离子不计为至少两种，iii）至少一种阳离子之一是二价，三价，四价或五价阳离子，并且具有低于 120℃。本发明还涉及制备它们及其用途的方法。

4. 发明申请

WO2006087303A1 PROCESS TO PREPARE CHLORINE-CONTAINING COMPOUNDS 审中-公开
标题翻译：制备含氯化合物的方法
公开(公告)号：WO2006087303A1
公开(公告)日：2006-08-24
申请号：PCT/EP2006/050870
申请日：2006-02-13
申请人： AKZO NOBEL N.V. , BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
发明人： BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
IPC分类号： C01B7/03 , C01B11/14 , C01D3/14
CPC分类号： C01D3/14 , B01D61/027 , B01D61/04 , B01D2311/04 , B01D2311/06 , B01D2311/12 , B01D2311/25 , B01D2311/2684 , C01B7/03 , C01B11/14 , C25B1/26 , C25B1/265 , C25B15/08
摘要： The present invention relates to process to prepare a chlorine-containing compound using an aqueous salt solution containing at least 100 g/l of sodium chloride and a contaminating amount of polyvalent cations comprising the steps of (i) preparing an aqueous salt solution containing at least 100 g/l of sodium chloride and at least 0.01 ppm of polyvalent cations by dissolving a sodium chloride source in water, (ii) adding an effective amount of at least one positive retention enhancing component to the aqueous solution, (iii) subsequently subjecting the solution to a nanofiltration step, thereby separating the solution into a retentate which is enriched for polyvalent cations and a permeate which is the purified aqueous salt solution, (iv) reacting the chloride anions in the permeate to a chlorine- containing compound by an electrolysis step, and (v) recycling at least part of the retentate to dissolution step (i).
摘要翻译：本发明涉及使用含有至少100g / l氯化钠和污染量的多价阳离子的盐水溶液制备含氯化合物的方法，包括以下步骤：（i）制备至少含有盐水溶液通过将氯化钠源溶解在水中，将100g / l氯化钠和至少0.01ppm的多价阳离子，（ii）向该水溶液中加入有效量的至少一种阳性凝固促进组分，（iii）溶液，从而将溶液分离成富含多价阳离子的保留物和作为纯化的盐水溶液的渗透物，（iv）通过电解步骤使渗透物中的氯阴离子与含氯化合物反应，和（v）将至少部分滞留物再循环到溶解步骤（i）中。

5. 发明申请

WO2006087302A1 PROCESS TO PREPARE SALT 审中-公开
标题翻译：处理盐的过程
公开(公告)号：WO2006087302A1
公开(公告)日：2006-08-24
申请号：PCT/EP2006/050869
申请日：2006-02-13
申请人： AKZO NOBEL N.V. , BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
发明人： BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
IPC分类号： C01D3/08 , C01D3/14
CPC分类号： C01D3/14 , C01D3/08
摘要： The present invention relates to a process to prepare salt comprising the following steps: (i) preparing an aqueous salt solution containing at least 100 g/l of sodium chloride and at least 0.01 ppm of polyvalent cations by dissolving a sodium chloride source in industrial water, (ii) adding an effective amount of at least one positive retention enhancing component to the aqueous salt solution, (iii) subsequently subjecting the solution to a nanofiltration step, thereby separating the solution into a retentate which is enriched for the polyvalent cations and a permeate which is the purified aqueous salt solution, and (iv) concentrating the permeate to produce salt.
摘要翻译：本发明涉及一种制备盐的方法，包括以下步骤：（i）通过将氯化钠源溶解在工业水中制备含有至少100g / l氯化钠和至少0.01ppm多价阳离子的盐水溶液，（ii）向所述盐水溶液中加入有效量的至少一种阳性滞留增强组分，（iii）随后使所述溶液经受纳滤过程，从而将所述溶液分离成富含多价阳离子的滞留物和渗透物，其是纯化的盐水溶液，和（iv）浓缩渗透物以产生盐。

6. 发明授权

EP1858806B1 PROCESS TO PREPARE SALT 有权转让
标题翻译：用于生产SALT
公开(公告)号：EP1858806B1
公开(公告)日：2009-02-11
申请号：EP06708211.5
申请日：2006-02-13
申请人： Akzo Nobel N.V.
发明人： BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
IPC分类号： C01D3/08 , C01D3/14
CPC分类号： C01D3/14 , C01D3/08

7. 发明公开

EP1858806A1 PROCESS TO PREPARE SALT 有权转让
标题翻译：用于生产SALT
公开(公告)号：EP1858806A1
公开(公告)日：2007-11-28
申请号：EP06708211.5
申请日：2006-02-13
申请人： Akzo Nobel N.V.
发明人： BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
IPC分类号： C01D3/08 , C01D3/14
CPC分类号： C01D3/14 , C01D3/08
摘要： The present invention relates to a process to prepare salt comprising the following steps: (i) preparing an aqueous salt solution containing at least 100 g/l of sodium chloride and at least 0.01 ppm of polyvalent cations by dissolving a sodium chloride source in industrial water, (ii) adding an effective amount of at least one positive retention enhancing component to the aqueous salt solution, (iii) subsequently subjecting the solution to a nanofiltration step, thereby separating the solution into a retentate which is enriched for the polyvalent cations and a permeate which is the purified aqueous salt solution, and (iv) concentrating the permeate to produce salt.

8. 发明公开

EP1848661A1 PROCESS TO PREPARE CHLORINE-CONTAINING COMPOUNDS 有权转让
标题翻译：用于生产含氯化合物
公开(公告)号：EP1848661A1
公开(公告)日：2007-10-31
申请号：EP06708212.3
申请日：2006-02-13
申请人： Akzo Nobel N.V.
发明人： BARGEMAN, Gerrald , DEMMER, René Lodewijk Maria , TEN KATE, Antoon , KUZMANOVIC, Boris , VAN LARE, Cornelis Elizabeth Johannus , MAYER, Mateo Jozef Jacques , SCHUTYSER, Maarten André Irène , WESTERINK, Jan Barend
IPC分类号： C01B7/03 , C01B11/14 , C01D3/14
CPC分类号： C01D3/14 , B01D61/027 , B01D61/04 , B01D2311/04 , B01D2311/06 , B01D2311/12 , B01D2311/25 , B01D2311/2684 , C01B7/03 , C01B11/14 , C25B1/26 , C25B1/265 , C25B15/08
摘要： The present invention relates to process to prepare a chlorine-containing compound using an aqueous salt solution containing at least 100 g/l of sodium chloride and a contaminating amount of polyvalent cations comprising the steps of (i) preparing an aqueous salt solution containing at least 100 g/l of sodium chloride and at least 0.01 ppm of polyvalent cations by dissolving a sodium chloride source in water, (ii) adding an effective amount of at least one positive retention enhancing component to the aqueous solution, (iii) subsequently subjecting the solution to a nanofiltration step, thereby separating the solution into a retentate which is enriched for polyvalent cations and a permeate which is the purified aqueous salt solution, (iv) reacting the chloride anions in the permeate to a chlorine-containing compound by an electrolysis step, and (v) recycling at least part of the retentate to dissolution step (i).

9. 发明公开

EP2170808A2 CHELATING AGENT BASED IONIC LIQUIDS, A PROCESS TO PREPARE THEM, AND THEIR USE 审中-公开
标题翻译： ON促排剂类离子液体及其制造方法和使用
公开(公告)号：EP2170808A2
公开(公告)日：2010-04-07
申请号：EP08786691.9
申请日：2008-07-31
申请人： Akzo Nobel N.V.
发明人： DE WOLF, Cornelia Adriana , KUZMANOVIC, Boris , BEMELAAR, Johanna Hendrika , VAN STRIEN, Cornelis Johannes Govardus , HEUS, Martin , TEN KATE, Antoon
IPC分类号： C07C211/63 , C07C215/40 , C07C229/16 , C07C229/76 , C07F9/54
CPC分类号： C07C229/16 , C07C211/63 , C07C215/40 , C07C229/76 , C07F9/5407
摘要： The present invention relates to ionic liquids of the formula: (Mm+)xH+y nN+R1R2R3R4 Z-N(-CHXCOO-)pY2-p or (Mm+)x H+y nP+R1R2R3R4 Z-N(-CHXCOO-)pY2-p wherein any one of R1 to R4 independently represents a hydrogen, alkyl, cycloalkyl, aryl or aralkyl group that may be unsubstituted or substituted with one or more groups selected from OH, Cl, Br, F, I, phenyl, NH2, CN, NO2, an ether group, COOR5, CHO, COR5 or OR5, wherein R5 is an alkyl or cycloalkyl group, and wherein two of the groups R1 to R4 together with the N atom may form a heteroaromatic or heterocyclic group such as a pyridinium, pyrrolidinium or imidazolium group; the Z-N(-CHXCOO-)pY2-p is the anion derived from a chelating agent, wherein Z is a group selected from hydrogen, alkyl, an alkyl group optionally substituted with one or more carboxylate groups, hydroxyl groups and/or optionally containing one or more ether functionalities, or Z is a group of the formula -CH2-CHR6-R7-N-(CH2COO-)2, R6 is hydrogen or a C1-C3 alkyl group, R7 is a single bond, a C1-C3 alkylene group or one or more groups of the formula -N(CH2COO-)-CH2-CHR6-R8-, R8 is a single bond or a C1-C3 alkylene group, p is 2 or 1, X is H, an aryl group that may be unsubstituted or substituted with an OH and/or CH3 substituent, or CH2COO-, and when p is 1, Y is H, a benzyl group that may be unsubstituted or substituted with an OH and/or CH3 group, or a phenyl group that may be unsubstituted or substituted with an OH and/or CH3 substituent, Mm+ is a m-valent metal cation, n is 1 or higher, x is from 0 to 5, y is from 0 to 3, the total positive charge of (Mm+)x, H+y,and nN+R1R2R3R4 or nP+R1R2R3R4 equals the negative charge of the Z-N(-CHXCOO-)pY2-p anion, wherein at least one of the following conditions is fulfilled: i) the chelating agent has a connectivity index 1 X/3 X of below 2.17, ii) at least two different cations are present in the salt, whereby a proton cation does not count as one of the at least two, iii) at least one cation is a bivalent, trivalent, tetravalent or pentavalent cation, and having a melting point below 120°C. The invention further relates to a process to prepare them and their use.

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