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1. 发明申请

WO2009024519A1 GLUTAMIC ACID N,N-DIACETIC AMIDE, GLUTAMIC ACID N-ACETIC AMIDE N-ACETONITRILE, ALKALI METAL SALTS THEREOF, PROCESS TO PREPARE THEM AND THEIR USE 审中-公开
标题翻译：谷氨酸N，N-二酰胺，谷氨酸N-乙酰胺N-乙酸酯，其碱金属盐，其制备方法及其用途
公开(公告)号：WO2009024519A1
公开(公告)日：2009-02-26
申请号：PCT/EP2008/060656
申请日：2008-08-14
申请人： AKZO NOBEL N.V. , BOONSTRA, Tjerk, Oedse , HEUS, Martin , CARSTENS, Axel , LEPAGE, Jim
发明人： BOONSTRA, Tjerk, Oedse , HEUS, Martin , CARSTENS, Axel , LEPAGE, Jim
IPC分类号： C07C231/06 , C07C233/05 , C11D3/33
CPC分类号： C11D3/33 , C07C227/26 , C07C229/24 , C07C237/06 , C07C255/25 , C09K8/86 , C11D7/3245 , D21C9/10
摘要： The present invention relates to glutamic acid N,N-diacetic amide, potassium or sodium glutamate N,N-diacetic amide, glutamic acid N-acetic amide N-acetonithle, potassium or sodium glutamate N-acetic amide N-acetonitrile, to processes to prepare such compounds and the use thereof.
摘要翻译：本发明涉及谷氨酸N，N-二乙酰胺，谷氨酸钾或谷氨酸钠N，N-二乙酸酰胺，谷氨酸N-乙酰胺N-乙腈，谷氨酸钾或谷氨酸N-乙酰胺N-乙腈，以处理制备这些化合物及其用途。

2. 发明申请

WO2009024518A1 ALKALI METAL SALT OF GLUTAMIC ACID N,N-DIACETIC ACID, A PROCESS TO PREPARE SUCH SALT, AND THE USE THEREOF 审中-公开
标题翻译：谷氨酸金属盐，N-二酸，制备这种盐的方法及其用途
公开(公告)号：WO2009024518A1
公开(公告)日：2009-02-26
申请号：PCT/EP2008/060655
申请日：2008-08-14
申请人： AKZO NOBEL N.V. , BOONSTRA, Tjerk, Oedse , HEUS, Martin
发明人： BOONSTRA, Tjerk, Oedse , HEUS, Martin
IPC分类号： C07C229/24 , C07C227/26 , C11D3/33
CPC分类号： C11D3/33 , C07C227/26 , C07C229/24 , C07C237/06 , C07C255/25 , C09K8/86 , C11D7/3245 , D21C9/10
摘要： The present invention relates to an alkalimetal salt of glutamic acid-N,N-diacetic acid (GLDA) of the formula Na x K y H z GLDA, wherein x is equal to or more than 2 and lower than 4 and y is more than 0 and equal to or lower than 2, x+y is 3.5-4, and x+y+z = 4, to processes to prepare such salt and the use thereof.
摘要翻译：本发明涉及式NaxKyHzGLDA的谷氨酸-N，N-二乙酸（GLDA）的碱金属盐，其中x等于或大于2且低于4且y大于0且等于或低于 2，x + y为3.5-4，x + y + z = 4，以制备这种盐及其用途。

3. 发明申请

WO2010139755A1 PROCESS TO PREPARE A CHELATING AGENT OR PRECURSOR THEREOF USING A CYANIDE SALT 审中-公开
标题翻译：使用氰化物盐制备螯合剂或其前体的方法
公开(公告)号：WO2010139755A1
公开(公告)日：2010-12-09
申请号：PCT/EP2010/057776
申请日：2010-06-03
申请人： AKZO NOBEL CHEMICALS INTERNATIONAL B.V. , LAMMERS, Hans , HEUS, Martin , BOONSTRA, Tjerk Oedse , REICHWEIN, Adrianus Maria
发明人： LAMMERS, Hans , HEUS, Martin , BOONSTRA, Tjerk Oedse , REICHWEIN, Adrianus Maria
IPC分类号： C07C253/08 , C07C255/25 , C07C227/28 , C07C229/24
CPC分类号： C07C253/08 , C07C229/24 , C07C255/25
摘要： The present invention relates to a process comprising the reaction of a cyanide with an amino acid and an aldehyde, characterized in that the cyanide is a cyanide salt, the amino acid is aspartic acid and/or glutamic acid in the acidic form, and the process is performed under acidic pH by the addition of between 0 and 1 equivalent of an acid based on the amount of aspartic or glutamic acid.
摘要翻译：本发明涉及氰化物与氨基酸和醛的反应的方法，其特征在于氰化物是氰化物盐，氨基酸是酸性形式的天冬氨酸和/或谷氨酸，该方法通过加入基于天冬氨酸或谷氨酸的量的0至1当量的酸在酸性pH下进行。

4. 发明申请

WO2003020689A1 CHELATING AGENTS AND THEIR METAL CHELATES 审中-公开
标题翻译：焊接剂及其金属螯合物
公开(公告)号：WO2003020689A1
公开(公告)日：2003-03-13
申请号：PCT/EP2002/009353
申请日：2002-08-20
申请人： AKZO NOBEL N.V. , KLEIJER, Arnold, Johan , HEUS, Martin , REICHWEIN, Adrianus, Maria
发明人： KLEIJER, Arnold, Johan , HEUS, Martin , REICHWEIN, Adrianus, Maria
IPC分类号： C07C251/24
CPC分类号： C07C251/24 , C05D9/02 , C07C2601/14
摘要： The invention pertains to a chelating agent of the formula: (I) wherein Z is cyclohexylene or (CR 2 ) n wherein R is independently H or C1-4 alkyl, and n is an integer of 2-4; X is (CR' 2 ) m COO - M + wherein R' is independently H or CH 3, m is an integer of 0-3, and M is selected from H, Na, K, and NH 4 ; and Y is independently selected from H, oh, COOOH, SO 3 H, PO 3 H 2 , C1-4 alkyl, halogen, CN, and NO 2 . The invention further pertains to this chelating agent and a metal ion, preferably manganese ion, preferably to combat manganese ion deficiency in plant cultivation.
摘要翻译：本发明涉及式（I）的螯合剂，其中Z是亚环己基或（CR 2）n，其中R独立地是H或C 1-4烷基，n是2-4的整数; X是（CR'2）mCOO - ，其中R'独立地是H或CH3，m是0-3的整数，M选自H，Na，K和NH4; Y独立地选自H，OH，COOOH，SO 3 H，PO 3 H 2，C 1-4烷基，卤素，CN和NO 2。本发明还涉及该螯合剂和金属离子，优选锰离子，优选用于抵抗植物培养中的锰离子缺乏。

5. 发明申请

WO2009016235A2 CHELATING AGENT BASED IONIC LIQUIDS, A PROCESS TO PREPARE THEM, AND THEIR USE 审中-公开
标题翻译：基于代理的离子液体，制备方法及其使用
公开(公告)号：WO2009016235A2
公开(公告)日：2009-02-05
申请号：PCT/EP2008/060066
申请日：2008-07-31
申请人： Akzo Nobel N.V. , DE WOLF, Cornelia Adriana , KUZMANOVIC, Boris , BEMELAAR, Johanna Hendrika , VAN STRIEN, Cornelis Johannes Govardus , HEUS, Martin , TEN KATE, Antoon
发明人： DE WOLF, Cornelia Adriana , KUZMANOVIC, Boris , BEMELAAR, Johanna Hendrika , VAN STRIEN, Cornelis Johannes Govardus , HEUS, Martin , TEN KATE, Antoon
IPC分类号： C07C211/63 , C07C215/40 , C07C229/16 , C07C229/76 , C07F9/54
CPC分类号： C07C229/16 , C07C211/63 , C07C215/40 , C07C229/76 , C07F9/5407
摘要： The present invention relates to ionic liquids of the formula: (M m+ ) x H + y nN + R 1 R 2 R 3 R 4 Z-N(-CHXCOO - ) p Y 2-p or (M m+ ) x H + y nP + R 1 R 2 R 3 R 4 Z-N(-CHXCOO - ) p Y 2-p wherein any one of R 1 to R 4 independently represents a hydrogen, alkyl, cycloalkyl, aryl or aralkyl group that may be unsubstituted or substituted with one or more groups selected from OH, Cl, Br, F, I, phenyl, NH 2 , CN, NO 2, an ether group, COOR 5 , CHO, COR 5 or OR 5 , wherein R 5 is an alkyl or cycloalkyl group, and wherein two of the groups R 1 to R 4 together with the N atom may form a heteroaromatic or heterocyclic group such as a pyridinium, pyrrolidinium or imidazolium group; the Z-N(-CHXCOO - )pY 2-p is the anion derived from a chelating agent, wherein Z is a group selected from hydrogen, alkyl, an alkyl group optionally substituted with one or more carboxylate groups, hydroxyl groups and/or optionally containing one or more ether functionalities, or Z is a group of the formula -CH 2 -CHR 6 -R 7 -N-(CH 2 COO - ) 2 , R 6 is hydrogen or a C 1 -C 3 alkyl group, R 7 is a single bond, a C 1 -C 3 alkylene group or one or more groups of the formula -N(CH 2 COO - )-CH 2 -CHR 6 -R 8 -, R 8 is a single bond or a C 1 -C 3 alkylene group, p is 2 or 1, X is H, an aryl group that may be unsubstituted or substituted with an OH and/or CH 3 substituent, or CH 2 COO - , and when p is 1, Y is H, a benzyl group that may be unsubstituted or substituted with an OH and/or CH 3 group, or a phenyl group that may be unsubstituted or substituted with an OH and/or CH 3 substituent, M m+ is a m-valent metal cation, n is 1 or higher, x is from 0 to 5, y is from 0 to 3, the total positive charge of (M m+ ) x , H + y ,and nN + R 1 R 2 R 3 R 4 or nP + R 1 R 2 R 3 R 4 equals the negative charge of the Z-N(-CHXCOO - ) p Y 2-p anion, wherein at least one of the following conditions is fulfilled: i) the chelating agent has a connectivity index 1 X/ 3 X of below 2.17, ii) at least two different cations are present in the salt, whereby a proton cation does not count as one of the at least two, iii) at least one cation is a bivalent, trivalent, tetravalent or pentavalent cation, and having a melting point below 120°C. The invention further relates to a process to prepare them and their use.
摘要翻译：本发明涉及下式的离子液体：（Mm +）xH + y nN + R1R2R3R4ZN（-CHXCOO-）pY2-p或（Mm +）xH + ynP + R1R2R3R4Z-N（-CHXCOO-）pY2-p其中任何 R 1至R 4中的一个独立地表示氢，烷基，环烷基，芳基或芳烷基，其可以是未取代的或被一个或多个选自OH，Cl，Br，F，I，苯基，NH 2，CN，NO 2，醚基，COOR 5，CHO，COR 5或OR 5，其中R 5是烷基或环烷基，并且其中R 1至R 4中的两个与N原子一起可以形成杂芳族或杂环基，例如吡啶鎓，吡咯烷鎓或咪唑鎓基团 ; ZN（-CHXCOO-）pY2-p是衍生自螯合剂的阴离子，其中Z是选自氢，烷基，任选被一个或多个羧酸酯基团取代的烷基，羟基和/或任选地含有一个或更多的醚官能团，或Z是式-CH2-CHR6-R7-N-（CH2COO-）2的基团，R6是氢或C1-C3烷基，R7是单键，C1-C3亚烷基基团或一个或多个式-N（CH 2 COO - ） - CH 2 - CHR 6 -R 8 - 的基团，R 8是单键或C 1 -C 3亚烷基，p是2或1，X是H，可以是未被取代的或被OH和/或CH 3取代基或CH 2 COO-取代的，当p是1时，Y是H，可以是未取代的或被OH和/或CH 3基团取代的苄基或苯基其可以是未取代的或被OH和/或CH 3取代基取代，M m +是m价金属阳离子，n为1或更高，x为0至5，y为0至3，（ Mm +）x，H + y和nN + R1R2R3R4或 nP + R1R2R3R4等于ZN（-CHXCOO-）pY2-p阴离子的负电荷，其中满足以下条件中的至少一个：i）螯合剂具有低于2.17的连续性指数1 X / 3 X，ii ）盐中存在至少两种不同的阳离子，其中质子阳离子不计为至少两种，iii）至少一种阳离子之一是二价，三价，四价或五价阳离子，并且具有低于 120℃。本发明还涉及制备它们及其用途的方法。

6. 发明申请

WO2008065109A1 PROCESS TO PREPARE AMINO ACID-N, N-DIACETIC ACID COMPOUNDS 审中-公开
标题翻译：制备氨基酸-N，N-二酸化合物的方法
公开(公告)号：WO2008065109A1
公开(公告)日：2008-06-05
申请号：PCT/EP2007/062881
申请日：2007-11-27
申请人： Akzo Nobel N.V. , HEUS, Martin , LAMMERS, Hans , VOLMER, Arie
发明人： HEUS, Martin , LAMMERS, Hans , VOLMER, Arie
IPC分类号： C07C227/40 , C07C229/16 , C07C229/24 , B01D61/44
CPC分类号： C07C227/40 , B01D61/44 , C07C229/16 , C07C229/24
摘要： The invention relates to a process for the production of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups or its salt with less than an equivalent of alkaline metal based on the number of carboxyl groups, said process comprising reducing alkali metal ions from an aqueous solution of an alkali metal salt of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups and acidifying the amino carboxylate starting material by first performing a chemical acidification step using an organic or inorganic acid to get a compound in which at least one of the groups is protonated, and in a subsequent step further acidifying the amino carboxylate starting material and reducing alkali metal ions from an aqueous solution of the partially acidified alkali metal salt of the amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups by electrodialysis, wherein the electrodialysis is performed using a hydrogen ion permselective membrane on the anode side and a cation-permeable membrane on the cathode side.
摘要翻译：本发明涉及一种制备具有至少一个仲氨基或叔氨基和三个或更多个羧基的氨基酸的方法或其盐，其基于羧基数目少于等于碱当量，所述方法包括从具有至少一个仲或叔氨基和三个或多个羧基的氨基酸的碱金属盐的水溶液中还原碱金属离子，并且通过首先使用有机或不饱和羧酸盐进行化学酸化步骤酸化氨基羧酸盐原料无机酸，得到其中至少一个基团被质子化的化合物，并且在随后的步骤中，进一步酸化氨基羧酸酯起始原料并从部分酸化的氨基酸的碱金属盐的水溶液中还原碱金属离子，其具有至少一个仲或叔氨基和三个或更多个羧基通过电渗析，其中选择使用阳极侧的氢离子选择性膜和阴极侧的阳离子透过膜进行透析。

7. 发明申请

WO2010076291A1 COATED PARTICLES OF A CHELATING AGENT 审中-公开
标题翻译：螯合剂的涂层颗粒
公开(公告)号：WO2010076291A1
公开(公告)日：2010-07-08
申请号：PCT/EP2009/067913
申请日：2009-12-24
申请人： AKZO NOBEL N.V. , SEETZ, Johannes Wilhelmus Franciscus Lucas , MERCANTON, Jérôme , FERM, Paul Michael , HEUS, Martin , SZILÁGYI, Zoltán , VAN LARE, Cornelis Elizabeth Johannus
发明人： SEETZ, Johannes Wilhelmus Franciscus Lucas , MERCANTON, Jérôme , FERM, Paul Michael , HEUS, Martin , SZILÁGYI, Zoltán , VAN LARE, Cornelis Elizabeth Johannus
IPC分类号： B01J2/00 , C09K8/536 , C08J3/20 , C11D3/33 , C11D3/37 , C11D7/32 , C11D17/00
CPC分类号： C09K8/536 , C11D3/33 , C11D17/0039
摘要： The present invention relates to a coated particle including a particle including at least one chelating agent of the formula COOH-CHX-N-(CH 2 -COOH) 2 , wherein X stands for carboxyalkyl, alkyl, hydroxyalkyl or aminoalkyl, and alkyl is a C1-C4 alkyl group, and the coating on the particle includes at least one scale- inhibiting additive, a process to prepare such particle, and to the use thereof in detergents, in oil field applications, in agriculture and in water treatment.
摘要翻译：本发明涉及包含至少一种式COOH-CHX-N-（CH2-COOH）2螯合剂的颗粒的涂覆颗粒，其中X代表羧基烷基，烷基，羟基烷基或氨基烷基，烷基是C1 -C4烷基，并且颗粒上的涂层包括至少一种防垢添加剂，制备这种颗粒的方法，以及其在洗涤剂，油田应用，农业和水处理中的用途。

8. 发明申请

WO2005014527A1 ANAQUEOUS SOLUTION OF A SODIUM SALT OF HEDTA 审中-公开
标题翻译： HEDTA钠盐的无效解决方案
公开(公告)号：WO2005014527A1
公开(公告)日：2005-02-17
申请号：PCT/EP2004/007841
申请日：2004-07-13
申请人： AKZO NOBEL N.V. , HEUS, Martin , LAMMERS, Hans , LEPAGE, Jim
发明人： HEUS, Martin , LAMMERS, Hans , LEPAGE, Jim
IPC分类号： C07C229/26
CPC分类号： B01D61/445 , C02F1/683 , C02F2101/203
摘要： The invention pertains to an aqueous solution of a sodium salt xNa + yH + of the chelating compound of formula (I): wherein x = 2.1 - 2.7, y = 0.9 - 0.3, and x + y = 3. The invention further pertains to a container comprising at least 0.5 kg of said aqueous solution and to a method of preparing an aqueous solution comprising at least 45wt% of the sodium salt xNa + yH + of the chelating compound of formula (I) from Na 3 -HEDTA, comprising the steps of electrodialysing an aqueous solution containing less than 42 wt% of Na 3 -HEDTA using a bipolar membrane, thereby converting the trisodium salt solution to the solution of the sodium salt of formula (I) with x = 2.1 - 2.7, y = 0.9 - 0.3, and x + y = 3.
摘要翻译：本发明涉及式（I）螯合化合物的钠盐x Na + yH +的水溶液：其中x = 2.1-2.7，y = 0.9-0.3，x + y = 3。本发明还涉及包含至少0.5kg所述水溶液的容器和制备包含至少45wt％的式（I）螯合化合物的钠盐x Na + yH +的水溶液的方法，包括以下步骤：使用双极膜电渗析含有少于42重量％的Na 3 -HEDTA的水溶液，由此将三钠盐溶液转化为式（I）的钠盐溶液，其中x = 2.1 -2.7，y = 0.9-0.3，x + y = 3。

9. 发明申请

WO2012000914A1 PARTICLES COATED WITH VINYL ALCOHOL (CO) POLYMER AND POLYSACCHARIDE 审中-公开
标题翻译：用乙烯醇（CO）聚合物和多糖包覆的颗粒
公开(公告)号：WO2012000914A1
公开(公告)日：2012-01-05
申请号：PCT/EP2011/060671
申请日：2011-06-27
申请人： AKZO NOBEL CHEMICALS INTERNATIONAL B.V. , VAN LARE, Cornelis, Elizabeth, Johannus , HEUS, Martin
发明人： VAN LARE, Cornelis, Elizabeth, Johannus , HEUS, Martin
IPC分类号： C11D3/33 , C11D3/37 , C11D7/32 , C11D17/00 , B01J2/00 , C09K8/536 , C11D3/22 , C08J3/12
CPC分类号： C11D3/33 , C09K8/536 , C09K2208/26 , C11D3/222 , C11D3/225 , C11D3/3753 , C11D17/0039
摘要： The present invention relates to a coated particle containing a particle and a coating, wherein the particle contains glutamic acid Ν,Ν-diacetic acid or a partial salt thereof of the formula HnYm-GLDA, wherein Y is a cation selected from the group of sodium, potassium, and mixtures thereof, n+m = 4, and wherein the coating contains at least one vinyl alcohol (co)polymer and at least one polysaccharide, to a process to make such particle, and to the use thereof. In addition, the invention provides a method to reduce the hygroscopicity and water uptake and/or to improve the stability and flow properties of materials.
摘要翻译：本发明涉及含有颗粒和涂层的涂覆颗粒，其中所述颗粒含有式HnYm-GLDA的谷氨酸α，β-二乙酸或其部分盐，其中Y是选自钠，钾及其混合物，n + m = 4，并且其中所述涂层含有至少一种乙烯醇（共）聚合物和至少一种多糖，制备这种颗粒的方法及其用途。此外，本发明提供了减少吸湿性和吸水性和/或改善材料的稳定性和流动性质的方法。

10. 发明授权

EP2086923B1 PROCESS TO PREPARE AMINO ACID-N, N-DIACETIC ACID COMPOUNDS 有权转让
标题翻译：用于生产氨基-N，N-DIESSIGSÄUREVERBINDUNGEN
公开(公告)号：EP2086923B1
公开(公告)日：2012-08-15
申请号：EP07847408.7
申请日：2007-11-27
申请人： Akzo Nobel N.V.
发明人： HEUS, Martin , LAMMERS, Hans , VOLMER, Arie
IPC分类号： C07C227/40 , C07C229/16 , C07C229/24 , B01D61/44
CPC分类号： C07C227/40 , B01D61/44 , C07C229/16 , C07C229/24
摘要： The invention relates to a process for the production of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups or its salt with less than an equivalent of alkaline metal based on the number of carboxyl groups, said process comprising reducing alkali metal ions from an aqueous solution of an alkali metal salt of an amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups and acidifying the amino carboxylate starting material by first performing a chemical acidification step using an organic or inorganic acid to get a compound in which at least one of the groups is protonated, and in a subsequent step further acidifying the amino carboxylate starting material and reducing alkali metal ions from an aqueous solution of the partially acidified alkali metal salt of the amino acid having at least one secondary or tertiary amino group and three or more carboxyl groups by electrodialysis, wherein the electrodialysis is performed using a hydrogen ion permselective membrane on the anode side and a cation-permeable membrane on the cathode side.

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