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1. 发明专利

JPH1097863A SECONDARY BATTERY TYPE STORAGE BATTERY 失效
公开(公告)号：JPH1097863A
公开(公告)日：1998-04-14
申请号：JP25058996
申请日：1996-09-20
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , NEGISHI AKIRA , KATO TAKESHI , TSUDA IZUMI , TAKAHATA MASAATSU , NAKAMURA YUKIO , HAMAMOTO OSAMU
IPC分类号： B22F5/00 , B22F3/11 , H01M4/02 , H01M4/38 , H01M4/66 , H01M8/18 , H01M10/04 , H01M10/24 , H01M10/38 , H01M10/36
摘要： PROBLEM TO BE SOLVED: To provide a smaller, shockproof secondary battery type storage battery with a higher arrangement latitude, durability against overcharge and a longer cycle life. SOLUTION: A secondary battery type storage battery includes a positive electrode body and a negative electrode body both impregnated with or carrying battery active materials at their electrodes constituted of porous electric conductors, which are respectively housed in independent electrode chambers separated by a diaphragm. The apparent volume resistivity of the porous electric conductor measured by the DC four-terminal method is set to 10 Ω.cm or below, the porosity thereof obtained from the difference between the apparent specific gravity and the true specific gravity is set between 30 and 60%, the volume of the electrode chamber is made larger than the apparent volume of the electrode body by 20 to 200%, and the electrode chamber is filled at its void with electrolyte.

2. 发明专利

JPH06118056A MEASURING METHOD FOR MOISTURE 失效
公开(公告)号：JPH06118056A
公开(公告)日：1994-04-28
申请号：JP26607792
申请日：1992-10-05
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , KANEKO HIROKO , NEGISHI AKIRA , HAMAMOTO OSAMU , WATANABE KEIICHI
IPC分类号： G01N21/78 , G01N27/416 , G01N31/00 , G01N33/18
摘要： PURPOSE:To provide a measuring method for moisture capable of easily performing stable moisture measurement without having no limitation on measurement such as electrolytic condition at measuring the moisture of a high water content sample. CONSTITUTION:In a measuring method for moisture, the correlation between the water content in a high water content sample and the dissolved oxygen quantity of the sample laid in the equilibrated state to oxygen in the atmosphere is preliminarily determined at measuring the water content of the sample, the dissolved oxygen quantity of the moisture in the sample laid in the equilibrated state to oxygen in the atmosphere is measured, and the water content corresponding to the dissolved oxygen quantity is determined from the correlation. Since the water content can be determined from the dissolved oxygen quantity of the moisture in the sample, the moisture of a high water content sample which was difficult to measure in the past can be easily measured.

3. 发明专利

JPH06116772A ELECTROLYTIC METHOD AND ELECTROLYTIC DEVICE 失效
公开(公告)号：JPH06116772A
公开(公告)日：1994-04-26
申请号：JP26607592
申请日：1992-10-05
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , KANEKO HIROKO , NEGISHI AKIRA , HAMAMOTO OSAMU
IPC分类号： C25B1/00 , C25B3/02 , C25B9/00 , C25B11/03 , C25B15/08
摘要： PURPOSE:To provide the electrolytic method and electrolytic device capable of effecting org. or inorg. electrolytic synthesis with the inexpensive device and high efficiency and having excellent economy. CONSTITUTION:This electrolytic method consists in clamping or depositing a material 2 to be electrolyzed hardly soluble or insoluble in an electrolyte 4 in or on conductive porous body electrodes 1 and electrolyzing this material 2 in an electrolyte. This electrolytic device has the above-mentioned electrolyte and electrodes. Working electrodes 1 of the above-mentioned electrode are the conductive porous body electrodes formed by clamping or depositing the material 2 hardly soluble or insoluble in the above-mentioned electrolyte 4. An electrolytic cell which houses the electrolyte 4, plural double polar partition plates which partition this electrolyte cell 10 to plural electrolytic chambers, the plural conductive porous body electrodes which clamp or hold the material to be electrolyzed hardly soluble or insoluble in the electrolyte 4 and are installed in respective electrolytic chambers and means for electrically conducting these electrodes and the above-mentioned double polar partition plates are provided.

4. 发明专利

JPH05346418A 失效
公开(公告)号：JPH05346418A
公开(公告)日：1993-12-27
申请号：JP30206891
申请日：1991-11-18
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NEGISHI AKIRA , KANEKO HIROKO , NOZAKI TAKESHI , HAMAMOTO OSAMU
IPC分类号： G01N27/42 , G01N27/416
摘要： PURPOSE:To measure water content from micro concentration to relatively high concentration conveniently with high accuracy by bringing a fluid sample containing water into contact with water soluble electrolyte thereby electrolyzing the sample and then measuring current value or quantity of electricity. CONSTITUTION:Fluid sample stored in a bottle 1 is introduced into an electrolyte column 2 where the sample is brought into contact with sodium sulfate thus dissolving sodium sulfate into the water of the sample. The sample-containing water dissolved with sodium sulfate is then brought into contact with a sensor 3, onto which DC voltage of 2.5V is applied from a constant voltage supply 4 to electrolyze water in the sample and the value of generated current is recorded on a recorder 5. Water content of the sample is then measured based on a previously prepared working curve. This method realizes highly accurate and convenient measurement of water content of organic solvent and the like from micro concentration upto relatively high concentration.

5. 发明专利

JPH05326022A ORGANIC ELECTROLYTIC SECONDARY BATTERY 失效
公开(公告)号：JPH05326022A
公开(公告)日：1993-12-10
申请号：JP13383192
申请日：1992-05-26
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , NEGISHI AKIRA , KANEKO HIROKO , HAMAMOTO OSAMU , WATANABE KEIICHI
IPC分类号： H01M4/04 , H01M10/05 , H01M10/40
摘要： PURPOSE:To provide an organic electrolytic secondary battery for preventing the occurrence of short circuit while allowing the reduction of electric resistance inside the battery, being excellent in the safety and the life of the battery, and being capable of having a larger capacity and a higher density. CONSTITUTION:A conductive porous body holding electrolyte and supporting negative electrode active material whose charge-discharge body is insoluble or slightly soluble in the electrolyte, a diaphragm having 0.5mm thickness or less, and the conductive porous body holding the electrolyte and holding or supporting a positive active material, are arranged in order.

6. 发明专利

JPH05326012A SECONDARY BATTERY 失效
公开(公告)号：JPH05326012A
公开(公告)日：1993-12-10
申请号：JP13388492
申请日：1992-05-26
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , KANEKO HIROKO , NEGISHI AKIRA , HAMAMOTO OSAMU , WATANABE KEIICHI
IPC分类号： H01M10/10 , H01M10/12
摘要： PURPOSE:To provide a high performance secondary battery whose inner electric resistance is low, short circuit of which is prevented, and which is durable to deep discharge and has a long charge-discharge cycle life. CONSTITUTION:A conductive porous body 5, a conductive spacer 3, a diaphragm 4 with 1mm or less thickness, and a conductive porous body 6 are successively arranged wherein the porous body 5 retains an electrolytic solution and supports a negative pole active material whose charge and discharge states are insoluble or hard to be dissolved in the electrolytic solution and the porous body 6 retains the electrolytic solution and retains or supports a positive pole active material.

7. 发明专利

JPH05126794A MEASURING METHOD FOR ACIDITY AND ALKALINITY 失效
公开(公告)号：JPH05126794A
公开(公告)日：1993-05-21
申请号：JP28888391
申请日：1991-11-05
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , HAMAMOTO OSAMU
IPC分类号： G01N27/44 , G01N27/28
摘要： PURPOSE:To obtain the measurement method capable of easily and highly precisely measuring by means of a coulometric titration method. CONSTITUTION:The measurement method of acidity and alkalinity shows that a multipole partition plate 2A composed of Pd or Pd alloy is set in an electrolytic cell 1, with specimen electrolytic solution 6 put in one hand cell 1A of seriately-connected multipole electrolytic cells and with acid solution, alkali solution or pH buffer solution 6A put in the other hand cell 1B thereof, electrolysis is performed and a hydrogen ion in the specimen electrolytic solution or, the acid solution, the alkali solution or the pH buffer solution is moved between both the electrolytic cells through said multipole partition plate to perform coulometric titration. As usual, with titration reagent solution precisely prepared, simple measurement is possible without any need of filling it. In addition, because the number of parts is few, the low cost and compactness of the device can be contrived. Furthermore measurement precision is improved because any interference component in the specimen solution is not influenced.

8. 发明专利

JPH05126782A ELECTRODE FOR MEASUREMENT AND MANUFACTURING THEREOF 失效
公开(公告)号：JPH05126782A
公开(公告)日：1993-05-21
申请号：JP28888491
申请日：1991-11-05
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NEGISHI AKIRA , KANEKO HIROKO , NOZAKI TAKESHI , HAMAMOTO OSAMU
IPC分类号： G01N27/30
摘要： PURPOSE:To obtain an electrode for measurement that enables getting a tiny electrode of less than 50mum of interelectrode distance through rather simple manufacturing processes, and the manufacturing method thereof. CONSTITUTION:An electrode for measurement consists of a center electrode 1 made of metallic material, outer electrodes 2 made of metallic material and provided in the vicinity of the center electrode putting an electrically insulating resin layer 3 in between, and reinforcing insulation layer 4 formed at circumference of the outer electrodes. Gap distance among the center electrode and the outer electrodes is less than 50mum and end tip of each electrode is exposed out. As for manufacturing method of the electrodes for measurement, the method is to coat a metallic wire or a metallic band with an electrically insulating resin layer 3 and to form a metallic layer at circumference or on front/back sides of the coated layer by a surface metallization method, and thereafter to form a reinforcing insulation layer 4 at circumference of the metallic layer and then to expose the metal wire or the metallic band and the metallic layer at the end parts thereof.

9. 发明专利

JPH06118057A COULOMETRIC DETECTOR AND CONCENTRATION MEASURING METHOD 失效
公开(公告)号：JPH06118057A
公开(公告)日：1994-04-28
申请号：JP26607692
申请日：1992-10-05
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , KANEKO HIROKO , NEGISHI AKIRA , HAMAMOTO OSAMU , WATANABE KEIICHI
IPC分类号： G01N27/42
摘要： PURPOSE:To provide an easily usable coulometric detector capable of quick measurement and easy to maintain, and a concentration measuring method using this. CONSTITUTION:A coulometric detector has a positive electrode plate 1B and negative electrode plate 1A connected to a power source and a measuring instrument, respectively, with an electrode space less than 2mm, and a means 2 for holding a sample between both the electrode plates. A concentration measuring method comprises electrolyzing a material to be electrolyzed in the sample held between the electrode plates 1A, 1B of the coulometric detector, determining the extrapolation value of the quantity of electricity from the current and quantity of electricity at that time or the plot of the logarithm of current and the time, and calculating the absolute quantity of the material to be electrolyzed in the sample. The absolute determination of the material to be electrolyzed in the sample can be quickly measured from the extrapolation value of the quantity of electricity, and since no carbon felt electrode is used, the maintenance of the detector is facilitated.

10. 发明专利

JPH05126791A MEASURING METHOD FOR CONCENTRATION 失效
公开(公告)号：JPH05126791A
公开(公告)日：1993-05-21
申请号：JP28888291
申请日：1991-11-05
申请人： AGENCY IND SCIENCE TECHN , MITSUI SHIPBUILDING ENG
发明人： NOZAKI TAKESHI , HAMAMOTO OSAMU
IPC分类号： G01N27/28 , G01N27/416
摘要： PURPOSE:To obtain the method capable of contriving the simplification of a device and measuring at high precision. CONSTITUTION:With pH of a solution containing a substance to be measured iondissociating in the solution and having steam pressure at a non-dissociation condition regulated, the concentration of the substance to be measured therein is continuously measured by the use of a gas electrode with a diaphragm 1. At the time the pH regulation of the solution is performed by continuously bringing the solution into contact with an acid solution, the solution into contact with an alkali solution or a pH buffer solution through an ion exchange membrane 2. A cylinder pump, an agitator and the like for pH regulation are not needed and the simplification, light weight and low cost of a device can be contrived. The ion exchange membrane 2 and a detection electrode are easy to wash and the maintenance and inspection thereof become easy, so that its time can be reduced. High sensitivity can be easily achieved in the measurement of CO2, NH3 and the like, furthermore the compensation of temperature is unnecessary if a pH regulation vessel 3 is made a thermostatic chamber and measurement precision is improved.

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