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1. 发明授权

US4710227A Dispersion process for ceramic green body 失效
标题翻译：陶瓷绿体分散工艺
公开(公告)号：US4710227A
公开(公告)日：1987-12-01
申请号：US856879
申请日：1986-04-28
申请人： A. Dale Harley , Lawrence G. Duquette , Issam A. Khoury , Iwao Kohatsu
发明人： A. Dale Harley , Lawrence G. Duquette , Issam A. Khoury , Iwao Kohatsu
IPC分类号： C01B13/32 , C01G23/00 , C01G25/00 , C04B35/468 , C04B35/636 , C08L1/08 , C03C3/00 , C04B35/46
CPC分类号： B82Y30/00 , C01B13/32 , C01G23/006 , C01G25/00 , C04B35/4682 , C04B35/4684 , C04B35/6365 , C01P2002/60 , C01P2004/32 , C01P2004/50 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C01P2006/12
摘要： Preparation of a ceramic green body by hydrolyzing two groups of alkoxides to form a dispersion of their reaction product, concentrating the dispersion to a sediment without drying it, and admixing a binder solution, plasticizer and release agent with the sediment to make a ceramic slip formulation. The slip formulation is then cast as a ceramic green body. The proportions of alkoxides can be adjusted to produce a ceramic green body which is dielectric and useful for microcapacitors.
摘要翻译：通过水解两组醇盐形成其反应产物的分散体来制备陶瓷生坯，将分散体浓缩而不干燥沉淀物，并将粘合剂溶液，增塑剂和脱模剂与沉淀物混合以制备陶瓷滑移配方。然后将滑爽剂配制成陶瓷生坯。可以调节醇盐的比例以产生电介质并且可用于微电容器的陶瓷生坯体。

2. 发明授权

US4816072A Dispersion process for ceramic green body 失效
标题翻译：陶瓷绿体分散工艺
公开(公告)号：US4816072A
公开(公告)日：1989-03-28
申请号：US92025
申请日：1987-09-01
申请人： A. Dale Harley , Larwrence G. Duquette , Issam A. Khoury , Iwao Kohatsu
发明人： A. Dale Harley , Larwrence G. Duquette , Issam A. Khoury , Iwao Kohatsu
IPC分类号： C08J9/28 , A61L2/00 , A61L2/02 , A61M1/34 , B01D61/14 , B01D69/02 , B01D69/08 , B01D71/10 , C01B13/32 , C01G23/00 , C01G25/00 , C04B35/468 , C04B35/634 , C04B35/636 , D01D5/24 , D01F2/04 , D01F6/00 , C08L1/08 , C03C3/00
CPC分类号： A61L2/0017 , A61L2/022 , A61M1/34 , B01D69/02 , B01D69/08 , B82Y30/00 , C01B13/32 , C01G23/006 , C01G25/00 , C04B35/4682 , C04B35/4684 , C04B35/634 , C04B35/6365 , A61M2205/7509 , A61M2205/7554 , A61M2205/7581 , C01P2002/02 , C01P2002/34 , C01P2002/60 , C01P2004/32 , C01P2004/50 , C01P2004/61 , C01P2004/64 , C01P2006/12 , C01P2006/60
摘要： A process is described for the preparation of a ceramic green body by hydrolyzing at least one alkoxide selected from each of two specified groups to form a dispersion of their reaction product, concentrating the dispersion to a sediment without drying it, and admixing a binder and a plasticizer with the sediment to make a ceramic slip formulation. A release agent can optionally be admixed. The slip formulation is then cast as a ceramic green body. The proportions of alkoxides can be adjusted, as desired, to produce a ceramic green body which is dielectric and useful for microcapacitors or as a conductor.
摘要翻译：描述了通过水解选自两个特定基团中的每一个的至少一种醇盐以形成其反应产物的分散体来制备陶瓷生坯的方法，将分散体浓缩而不干燥沉淀物，并将粘合剂和增塑剂与沉淀物制成陶瓷滑移配方。可以任选地混合脱模剂。然后将滑爽剂配制成陶瓷生坯。可以根据需要调节醇盐的比例以产生电介质并且可用于微电容器或导体的陶瓷生坯体。

3. 发明授权

US5246903A Process and catalyst for the dehydrohalogenation of halogenated hydrocarbons or alkylene halohydrins 失效
标题翻译：用于卤代烃或亚烷基卤代醇的脱卤化氢的方法和催化剂
公开(公告)号：US5246903A
公开(公告)日：1993-09-21
申请号：US918997
申请日：1992-07-23
申请人： A. Dale Harley
发明人： A. Dale Harley
IPC分类号： C07C17/25
CPC分类号： B01J27/138 , C07C17/25 , B01J21/08 , B01J37/0201
摘要： An unsaturated halohydrocarbon such as vinylidene chloride is produced by the dehydrohalogenation of haloalkanes such as 1,1,1-trichloroethane or 1,1,2-trichloroethane, by contacting the haloalkane with a Group IA metal halide and a Group IIA or IIB metal oxide or metal hydroxide, together supported on a porous carrier material, under reaction conditions sufficient to form the corresponding unsaturated hydrocarbon and a Group IIA or IIB metal halide. The Group IIA or IIB metal oxide or metal hydroxide may be regenerated by contacting the Group IIA or IIB metal halide with an alkanol or water. In one embodiment, the process is initiated by contacting a novel catalyst comprising a Group IA metal cation such as Cs, a Group IIA or IIB metal cation such as Mg and a neutralizing number of halide anions such as chloride distributed on a support such as silica, with water or an alkanol under reaction conditions sufficient to form the Group IA metal halide and the Group IIA or IIB metal oxide or metal hydroxide supported on a porous carrier material. The process of the invention is also useful for the dehydrohalogenation of alkylene halohydrins to produce alkylene oxides. The process of the invention may be carried out in a riser reactor system, whereby the reactants are cycled in a continuous process.
摘要翻译：通过使卤代烷与IAA金属卤化物和IIA或IIB族金属氧化物接触，通过卤代烷烃如1,1,1-三氯乙烷或1,1,2-三氯乙烷的脱卤化氢来制备不饱和卤代烃或金属氢氧化物，一起负载在多孔载体材料上，在足以形成相应的不饱和烃和IIA或IIB族金属卤化物的反应条件下。 IIA族或IIB族金属氧化物或金属氢氧化物可以通过IIA或IIB族金属卤化物与链烷醇或水接触来再生。在一个实施方案中，通过使包含诸如Cs的第IA族金属阳离子如Mg，IIA族或IIB族金属阳离子如Mg的中和数量的卤化物阴离子（例如分布在载体上的氯化物如二氧化硅）在足以形成IA族金属卤化物的反应条件下的水或链烷醇，以及负载在多孔载体材料上的IIA或IIB族金属氧化物或金属氢氧化物。本发明的方法也可用于亚烷基卤代醇的脱卤化氢以产生环氧烷烃。本发明的方法可以在提升管反应器系统中进行，由此反应物以连续方式循环。

4. 发明授权

US5252771A Aluminum trifluoride catalyst for production of diaryl carbonates 失效
标题翻译：用于生产碳酸二芳基酯的三氟化铝催化剂
公开(公告)号：US5252771A
公开(公告)日：1993-10-12
申请号：US706426
申请日：1991-05-28
申请人： A. Dale Harley , Jose Puga
发明人： A. Dale Harley , Jose Puga
IPC分类号： B01J27/125 , C07B61/00 , C07C68/02 , C07C69/96
CPC分类号： C07C68/02
摘要： A process for the production of a diaryl carbonate useful in the preparation of polycarbonate molding resins comprising contacting an aromatic hydroxy compound and a carbonyl halide or aryl haloformate in the presence of a catalyst comprising aluminum trifluoride.

5. 发明授权

US5041406A Catalyst for hydrochlorination of hydrocarbons 失效
标题翻译：氢氯化烃的催化剂
公开(公告)号：US5041406A
公开(公告)日：1991-08-20
申请号：US486584
申请日：1990-02-28
申请人： A. Dale Harley , Michael T. Holbrook
发明人： A. Dale Harley , Michael T. Holbrook
IPC分类号： C07C17/16
CPC分类号： C07C17/16
摘要： Methyl chloride is produced by contacting methanol and hydrogen chloride in the vapor phase in the presence of KZnCl.sub.3 supported on silica. The process produces methyl chloride in good yield with minimal formation of dimethyl ether as a by-product.
摘要翻译：通过在负载在二氧化硅上的KZnCl 3存在下，使气相中的甲醇和氯化氢接触来制备甲基氯。该方法以最低的二甲醚形成作为副产物以良好的产率生产甲基氯。

6. 发明授权

US4935565A Process and catalyst for hydrochlorination of hydrocarbons 失效
标题翻译：碳氢化合物氢氯化过程和催化剂
公开(公告)号：US4935565A
公开(公告)日：1990-06-19
申请号：US235579
申请日：1988-08-24
申请人： A. Dale Harley , Michael T. Holbrook
发明人： A. Dale Harley , Michael T. Holbrook
IPC分类号： B01J27/138 , B01J29/035 , B01J35/10 , C07C17/16 , C07C19/01
CPC分类号： C07C17/16
摘要： Methyl chloride is produced by contacting methanol and hydrogen chloride in the vapor phase in the presence of KZnCl.sub.3 supported on silica. The process produces methyl chloride in good yield with minimal formation of dimethyl ether as a by-product.

7. 发明授权

US4604242A Preparation of dialiphatic, dialicyclic, or di(aryl-substituted aliphatic) carbonates 失效
标题翻译：脂肪族，二元脂环或二（芳基取代的脂肪族）碳酸酯的制备
公开(公告)号：US4604242A
公开(公告)日：1986-08-05
申请号：US590596
申请日：1984-03-19
申请人： A. Dale Harley , Jerald L. Curnutt , David T. Doughty
发明人： A. Dale Harley , Jerald L. Curnutt , David T. Doughty
IPC分类号： C07C68/00
CPC分类号： C07C68/005
摘要： This invention is a process for the preparation of a symmetrical or unsymmetrical dihydrocarbyl carbonate which comprises contacting an aliphatic, cycloaliphatic or di(aryl-substituted aliphatic) alcohol or mixtures thereof with carbon monoxide and oxygen in the presence of a catalytic amount of bis((2,4-pentanedianato)copper (II) methoxide) and a cocatalytic amount of a basic nitrogen-containing coordination compound under conditions such that a symmetrical or unsymmetrical dihydrocarbyl carbonate is prepared.
摘要翻译：本发明是一种制备对称或不对称二碳碳酸酯的方法，该方法包括在催化量的双（（（C 1 -C 6））存在下使脂族，脂环族或二（芳基取代的脂族醇）或其混合物与一氧化碳和氧气接触， 2,4-戊二胺）铜（II））和助催化量的碱性含氮配位化合物，在制备对称或不对称二碳碳酸酯的条件下。

8. 发明授权

US5430214A Hydrodehalogenation process and catalyst for use therein 失效
标题翻译：加氢脱卤方法和催化剂用于其中
公开(公告)号：US5430214A
公开(公告)日：1995-07-04
申请号：US153557
申请日：1993-11-16
申请人： David D. Smith , Michael T. Holbrook , A. Dale Harley , Larry N. Ito
发明人： David D. Smith , Michael T. Holbrook , A. Dale Harley , Larry N. Ito
IPC分类号： C07C1/26
CPC分类号： C07C1/26 , C07C2521/04 , C07C2523/46
摘要： A hydrodehalogenation process, comprising the step of reacting a saturated halohydrocarbon (e.g., 1,2-dichloropropane) with hydrogen or a hydrogen donor in the gas phase in the presence of a catalytically effective amount of ruthenium on a support, and at temperatures of at least about 100 degrees Celsius, to produce reaction products including a corresponding non-halogenated, unsaturated hydrocarbon (e.g., propylene).
摘要翻译：一种加氢脱卤方法，包括在催化有效量的钌存在下在载体上以及在载体的温度下使饱和卤代烃（例如1,2-二氯丙烷）与气相中的氢或氢供体反应的步骤至少约100摄氏度，以产生包括相应的非卤代不饱和烃（例如丙烯）的反应产物。

9. 发明授权

US4816609A Process and catalyst for the dehydrohalogenation of halogenated hydrocarbons 失效
标题翻译：卤代烃脱卤化氢的工艺和催化剂
公开(公告)号：US4816609A
公开(公告)日：1989-03-28
申请号：US53925
申请日：1987-05-26
申请人： A. Dale Harley
发明人： A. Dale Harley
IPC分类号： C07C17/25 , C07C17/34 , C07C21/06
CPC分类号： B01J27/138 , C07C17/25 , B01J21/08 , B01J37/0201
摘要： An unsaturated halohydrocarbon such as vinylidene chloride is produced by the dehydrohalogenation of haloalkanes such as 1,1,1-trichloroethane or 1,1,2-trichloroethane, in the presence of a novel mixed salt catalyst containing a Group IA metal cation such as Cs, a Group IIA metal cation such as Mg and a neutralizing number of counter anions such as chloride distributed on a support such as silica.
摘要翻译：在含有IA族金属阳离子如Cs的新型混合盐催化剂的存在下，通过卤代烷烃如1,1,1-三氯乙烷或1,1,2-三氯乙烷的脱卤化氢来制备不饱和卤代烃如偏二氯乙烯，IIA族金属阳离子如Mg和中和数量的抗衡阴离子如分配在诸如二氧化硅的载体上的氯化物。

10. 发明授权

US5476979A Processes for converting chlorinated alkenes to useful, less chlorinated alkenes 失效
标题翻译：将氯化烯烃转化为有用的较少氯化烯烃的方法
公开(公告)号：US5476979A
公开(公告)日：1995-12-19
申请号：US227806
申请日：1994-04-14
申请人： Larry N. Ito , Craig B. Murchison , Michael T. Holbrook , A. Dale Harley , David D. Smith
发明人： Larry N. Ito , Craig B. Murchison , Michael T. Holbrook , A. Dale Harley , David D. Smith
IPC分类号： B01J23/89 , B01J23/52 , B01J27/18 , C07B61/00 , C07C1/26 , C07C1/30 , C07C17/23 , C07C17/25 , C07C21/02 , C07C21/10 , C07C21/04
CPC分类号： B01J23/52 , B01J23/8926 , C07C1/26 , C07C1/30 , C07C17/23 , C07C17/25 , C07C2521/18 , C07C2523/14 , C07C2523/18 , C07C2523/42 , C07C2523/44 , C07C2523/46 , C07C2523/50 , C07C2523/52 , C07C2523/72 , C07C2523/89 , Y02P20/52
摘要： A process for converting a chlorinated alkene feedstock including two or more chlorines to reaction products including a less-chlorinated alkene in a commercially substantial proportion, comprising reacting the chlorinated alkene feedstock with hydrogen in the presence of a catalyst consisting essentially of a Group VIII metal other than rhodium, palladium or ruthenium and a Group IB metal on a support.
摘要翻译：一种将包含两种或多种氯的氯化烯烃原料转化成包括较低氯化烯烃在内的市售重要比例的反应产物的方法，包括使氯代烯烃原料与氢在催化剂存在下反应，所述催化剂基本上由VIII族金属比铑，钯或钌以及载体上的IB族金属。

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