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1. 发明申请

WO2004011510A1 ULTRACLEAN FLUOROELASTOMER SUITABLE FOR USE IN THE MANUFACTURING OF ELECTRONIC COMPONENTS 审中-公开
标题翻译： ULTRACLEAN FLOROELASTOMER适用于制造电子元器件
公开(公告)号：WO2004011510A1
公开(公告)日：2004-02-05
申请号：PCT/US2003/023530
申请日：2003-07-25
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner M., A. , HINTZER, Klaus , HIRSCH, Bernhard , KASPAR, Harald , KOLB, Robert, E. , LOHR, Gernot , SCHWERTFEGER, Werner
IPC分类号： C08F214/18
CPC分类号： C08F214/18 , C08F214/184
摘要： A curable fluoroelastomer composition for preparing a perfluoroelastomer. The composition includes; (1) a perfluoropolymer having one or more cure-sites selected from a halogen capable of participating in peroxide cure reaction and/or nitrile groups; (2) an organic peroxide and/or a compound capable of effecting curing of the perfluoropolymer through said nitrile groups; and (3) optionally a polyunsaturated coagent. The perfluoropolymer in the composition is essentially free of ionic end groups and the total amount of metal cations in the composition is not more than 10µg/g perfluoropolymer. The perfluoroelastomers may be obtained from curing the composition in a sufficiently low amount of metal cations so as to make the fluoroelastomer suitable for use in the semi-conductor industry.
摘要翻译：一种用于制备全氟弹性体的可固化的含氟弹性体组合物。组合物包括：（1）具有一个或多个选自能够参与过氧化物固化反应的卤素和/或腈基的固化位点的全氟聚合物; （2）能够通过所述腈基实现全氟聚合物固化的有机过氧化物和/或化合物; 和（3）任选的多不饱和助剂。组合物中的全氟聚合物基本上不含离子端基，组合物中金属阳离子的总量不超过10μg/ g全氟聚合物。全氟弹性体可以通过以足够低量的金属阳离子固化组合物获得，以使得氟弹性体适用于半导体工业。

2. 发明申请

WO2002083755A1 FLUOROPOLYMERS HAVING PENDANT IMIDATE STRUCTURES 审中-公开
标题翻译：具有辅助剂结构的氟聚合物
公开(公告)号：WO2002083755A1
公开(公告)日：2002-10-24
申请号：PCT/US2002/011602
申请日：2002-04-12
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： HINTZER, Klaus , GROOTAERT, Werner, M., A. , KOLB, Robert, E. , MAERZ, Franz , SCHWERTFEGER, Werner
IPC分类号： C08F214/18
CPC分类号： C08F16/24 , C08F214/18 , C08F214/262 , C08J5/18
摘要： A composition comprising (a) a fluoropolymer having pendant imidate groups, which imidate groups have the formula: -C=NH(OR) wherein R is a C 1 -C 10 aliphatic group which aliphatic group may have F or Cl substituents; and optionally, (b) a perfluorovinyl ether of the formula CF 2 =CFO(R' f O) a (R" f O) b R f wherein R' f and R" f are the same or are different C 1 -C 6 linear or branched perfluoroalkylene groups; a and b are, independently, 0 or an integer from 1 to 10; and R f is a C 1 -C 8 perfluoroalkyl group or a C 1 -C 15 perfluoroalkoxy group. Also provided are a method of making a fluoropolymer composition and curable and cured articles comprising a fluoropolymer composition.
摘要翻译：一种组合物，其包含（a）具有亚酰氨基侧基的含氟聚合物，所述亚胺基具有下式：-C = NH（OR），其中R是C1-C10脂族基团，该脂族基团可以具有F或Cl取代基; 任选地，（b）式CF 2 = CFO（R'fO）a（R“fO）b R f的全氟乙烯基醚，其中R'f和R”f相同或不同的是C1-C6直链或支链全氟亚烷基; a和b独立地为0或1〜10的整数; Rf为C1-C8全氟烷基或C1-C15全氟烷氧基。还提供了制备包含含氟聚合物组合物的含氟聚合物组合物和可固化和固化的制品的方法。

3. 发明申请

WO2002088248A1 PEROXIDE CURABLE FLUORELASTOMER COMPOSITIONS 审中-公开
标题翻译：过氧化物可固化FLUORELASTOMER组合物
公开(公告)号：WO2002088248A1
公开(公告)日：2002-11-07
申请号：PCT/US2002/003590
申请日：2002-02-07
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner, M., A. , COGGIO, William, D. , HINTZER, Klaus , KOLB, Robert, E. , LOHR, Gernot
IPC分类号： C08L27/12
CPC分类号： C08K5/14 , C08F4/34 , C08F6/22 , C08F14/18 , C08K5/00 , C08K5/17 , C08K5/36 , C08K5/49 , C08K5/50 , C08L27/12 , C08L27/18 , C08L2205/02 , C09D127/18 , C09K3/1009 , C08L2666/04 , C08F2/16
摘要： Curable fluoroelastomer compositions having improved compression set after curing are provided, as well as compositions that are of relatively high purity. These compositions include a hydrogen-containing fluoroelastomer having interpolymerized units derived from a cure-site monomer, a curative (optionally with a co-agent), and an organo-onium. When the fluoroelastomer contains units derived from vinylidene fluoride, the composition is essentially free from an inorganic acid acceptor. Methods of improving the compression of cured fluoroelastomer and cured fluoroelastomers having improved compression set are also provided.
摘要翻译：提供了固化后具有改进的压缩永久变形的可固化含氟弹性体组合物，以及具有相对高纯度的组合物。这些组合物包括具有衍生自固化部位单体，固化剂（任选与助剂）和有机鎓的共聚单元的含氢弹性体。当含氟弹性体含有衍生自偏二氟乙烯的单元时，组合物基本上不含无机酸受体。还提供了改进压缩永久变形的固化的含氟弹性体和固化的含氟弹性体的压缩方法。

4. 发明申请

WO2002083756A1 FLUOROPOLYMER COMPOSITIONS 审中-公开
标题翻译：氟聚合物组合物
公开(公告)号：WO2002083756A1
公开(公告)日：2002-10-24
申请号：PCT/US2002/011601
申请日：2002-04-12
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner, M., A. , KOLB, Robert, E. , HINTZER, Klaus
IPC分类号： C08F214/26
CPC分类号： C08K5/0025 , C08K5/50 , C08L27/12 , C08L27/18
摘要： A composition of (a) a fluoropolymer having interpolymerized units derived from a nitrogen-containing cure site monomer; and (b) a nonfluorinated catalyst composition that includes a compound having the general formula: {RA} (-) {QR' k } (+) or in certain cases the precursors thereof, wherein R is hydrogen, an alkyl, alkenyl, cycloalkyl, cycloalkenyl, aryl or aralkyl, A is an acid- or acid-derivative anion, Q is phosphorous, sulfur, nitrogen, arsenic, or antimony, and each R' is hydrogen or an alkyl, aryl, aralkyl, or alkenyl group, k is the valence of Q; and optionally (c) an alcohol of the formula R 2 -OH, wherein R 2 is an alkyl group which can be partially fluorinated. Also provided are a method of making a fluoropolymer, a method of increasing induction time, and fluoropolymer articles containing curable or cured fluoropolymer compositions.
摘要翻译：（a）具有衍生自含氮固化位点单体的共聚单元的含氟聚合物的组合物; （b）非氟化催化剂组合物，其包含具有以下通式的化合物：{RA}（（ - ）> {Q'k}（（+））或在某些情况下为其前体，其中R为氢，烷基，烯基，环烷基，环烯基，芳基或芳烷基，A是酸或酸衍生的阴离子，Q是磷，硫，氮，砷或锑，并且每个R'是氢或烷基，芳基，芳烷基或烯基，k是Q的化合价; 和任选地（c）式R 2 -OH的醇，其中R 2是可部分氟化的烷基。还提供了制备含氟聚合物的方法，增加诱导时间的方法和含有可固化或固化的含氟聚合物组合物的含氟聚合物制品。

5. 发明申请

WO2004033546A1 FLUOROPOLYMER COMPOSITIONS 审中-公开
标题翻译：氟聚合物组合物
公开(公告)号：WO2004033546A1
公开(公告)日：2004-04-22
申请号：PCT/US2003/029570
申请日：2003-09-23
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner, M., A. , KOLB, Robert, E.
IPC分类号： C08K5/00
CPC分类号： C08K5/29 , C08F8/30 , C08F2800/10 , C08L27/12 , C08F214/262
摘要： Compositions comprising a fluoropolymer having interpolymerized units derived from a nitrogen-containing cure site monomer and an amidine-containing curative are provided. Also provided are a method of making a fluoropolymer and fluoropolymer articles containing curable or cured fluoropolymer compositions.
摘要翻译：提供了包含具有衍生自含氮固化位点单体和含脒固化剂的共聚单元的含氟聚合物的组合物。还提供了制备含有可固化或固化的含氟聚合物组合物的含氟聚合物和含氟聚合物制品的方法。

6. 发明申请

WO2004011508A1 PROCESS FOR MAKING A FLUOROELASTOMER 审中-公开
标题翻译：制备荧光体的方法
公开(公告)号：WO2004011508A1
公开(公告)日：2004-02-05
申请号：PCT/US2003/023498
申请日：2003-07-25
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner, M., A. , HINTZER, Klaus , HIRSCH, Bernhard , KASPAR, Harald , KOLB, Robert, E. , LOHR, Gernot , SCHWERTFEGER, Werner
IPC分类号： C08F16/28
CPC分类号： C08F214/18 , C08F14/18
摘要： Aqueous microemulsions obtained from a perfluorinated alkane sulphonic or carboxylic acid or salt thereof, a liquid fluorinated monomer comprising a cure-site and optionally an inert liquid and highly fluorinated hydrocarbon compound. The aqueous microemulsion may be formed by mixing together water, a perfluorinated alkane sulphonic or carboxylic acid or salt thereof, optionally an inert liquid and highly fluorinated hydrocarbon compound and a liquid fluorinated monomer having a cure-site.
摘要翻译：由全氟化烷烃磺酸或其羧酸或其盐获得的水性微乳液，包含固化部位和任选的惰性液体和高度氟化烃化合物的液体氟化单体。水性微乳液可以通过将水，全氟化烷烃磺酸或其羧酸或其盐，任选的惰性液体和高度氟化的烃化合物和具有固化位点的液体氟化单体混合在一起而形成。

7. 发明申请

WO2002088228A1 FLUOROPOLYMER CURING SYSTEM 审中-公开
标题翻译：氟聚合物固化体系
公开(公告)号：WO2002088228A1
公开(公告)日：2002-11-07
申请号：PCT/US2002/013687
申请日：2002-04-30
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner, M. A. , KOLB, Robert, E. , HINTZER, Klaus
IPC分类号： C08J3/24
CPC分类号： C08K5/19 , C08L27/18 , C08L2205/02 , C08L27/12 , C08L2666/04
摘要： A composition of a fluoropolymer comprising interpolymerized units of nitrogen-containing cure site monomer and a catalyst comprising a compound having the formula (I), wherein HA is an acid, each R 1 , R 2 , and R 3 is independently a C 1 -C 20 alkyl group, which may be cyclic or heterocyclic, or R f (CH 2 ) x - wherein R f is a C 1 -C 8 linear or branched and at least partially fluorinated, and x is 1 to 4, and one R group may be a bond to another R group such that the nitrogen is bonded to or part of an alkenyl, cycloalkenyl, or aromatic group. This may further comprise a catalyst composition comprising a compound of the formula R 1 C(OR 2 )=NH, and salts thereof, where each R 1 and R 2 is, independently, a substituted or unsubstituted alkyl, aryl, aralkyl, alkenyl, cycloalkyl, or cycloalkenyl. Also provided are a method of making a fluoropolymer composition and articles prepared from the compositions.
摘要翻译：含有含氮固化位点单体的共聚单元的含氟聚合物的组合物和包含具有式（I）的化合物的催化剂，其中HA为酸，每个R 1，R 2和R 3独立地为C 1 -C 20烷基，其可以是环状或杂环的，或Rf（CH 2）x - ，其中R f是直链或支链并且至少部分氟化的C 1 -C 8，并且x是1至4，并且一个R基团可以是与另一R基团的键氮键合或链烯基，环烯基或芳基的一部分。这可以进一步包括催化剂组合物，其包含式R 1 C（OR 2）= NH的化合物及其盐，其中每个R 1和R 2独立地是取代或未取代的烷基，芳基，芳烷基，烯基，环烷基或环烯基。还提供了制备含氟聚合物组合物和由组合物制备的制品的方法。

8. 发明申请

WO2004060944A1 FLUOROPLASTIC POLYMERS HAVING NITROGEN-CONTAINING CURE SITES 审中-公开
标题翻译：具有含氮固化场的氟聚合物
公开(公告)号：WO2004060944A1
公开(公告)日：2004-07-22
申请号：PCT/US2003/038104
申请日：2003-12-01
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： GROOTAERT, Werner, M., A. , HINTZER, Klaus , KOLB, Robert, E. , ZIPPLIES, Tilman
IPC分类号： C08F259/08
CPC分类号： C08F214/182 , C08F214/265 , C08F259/08
摘要： Provided is a fluoroplastic or latex comprising a nitrogen-containing cure site and units derived from a fluorinated monomer. Also provided is a curable blend comprising a fluoroplastic and a fluoroleastomer gum, wherein said fluoroplastic comprises a nitrogen-containing cure site and units derived from a fluorinated monomer. Also provided are cured, shaped articles, latex blends, and a process for preparing a fluoroplastic comprising: (a) introducing at least 60 weight percent of a first polymerizable composition comprising a fluorinated monomer into a polymerization reactor; (b) polymerizing said composition in said reactor; (c) introducing at least 70 weight percent of a second polymerizable composition comprising a nitrogen-containing cure site monomer into said reactor following addition of at least 80% by weight of said first polymerizable composition; and (d) copolymerizing said nitrogen-containing cure site monomer with said fluorinated monomer to form a fluoroplastic.
摘要翻译：本发明提供含有含氮固化部位的氟塑料或胶乳和衍生自氟化单体的单元。还提供了包含氟塑料和氟橡胶胶的可固化共混物，其中所述氟塑料包含含氮固化部位和衍生自氟化单体的单元。还提供了固化，成型制品，胶乳混合物和制备氟塑料的方法，包括：（a）将至少60重量％的包含氟化单体的第一可聚合组合物引入聚合反应器中; （b）在所述反应器中聚合所述组合物; （c）在加入至少80重量％的所述第一可聚合组合物之后，将至少70重量％的包含含氮固化部位单体的可聚合组合物引入所述反应器中; 和（d）使所述含氮固化位点单体与所述氟化单体共聚以形成氟塑料。

9. 发明申请

WO2002060969A1 FLUOROPOLYMER COMPOSITIONS 审中-公开
标题翻译：氟聚合物组合物
公开(公告)号：WO2002060969A1
公开(公告)日：2002-08-08
申请号：PCT/US2002/003099
申请日：2002-01-31
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： KOLB, Robert, E. , GROOTAERT, Werner, M., A. , HINTZER, Klaus
IPC分类号： C08F214/26
CPC分类号： C08K5/0025 , C08K5/50 , C08L27/12 , C08L27/18
摘要： Compositions comprising a fluoropolymer having interpolymerized units derived from a nitrogen-containing cure site monomer and a catalyst composition are provided. The catalyst composition includes a compound having the general formula:{RA}¿(-)?{QR'¿k?}¿(+)? or the precursors thereof, wherein R is a nonfluorinated, partially fluorinated, or perfluorinated alkyl, alkenyl, cycloalkyl, cycloalkenyl, aryl or aralkyl, A is an acid- or acid-derivative anion, Q is phosphorous, sulfur, nitrogen, arsenic, or antimony, and each R' is hydrogen or an alkyl, aryl, aralkyl, or alkenyl group, k is the valence of Q; and optionally (c) an alcohol of the formula R?2¿-OH, wherein R?2¿ is an alkyl group which can be fluorinated.Also provided are a method of making a fluoropolymer, a method of increasing induction time, and fluoropolymer articles containing curable or cured fluoropolymer compositions.
摘要翻译：提供包含含有衍生自含氮固化位点单体的共聚单元的含氟聚合物和催化剂组合物的组合物。催化剂组合物包括具有以下通式的化合物：{RA}（ - ）{QR'k}（+）或其前体，其中R是非氟化，部分氟化或全氟化的烷基，烯基，环烷基，环烯基，芳基或芳烷基，A是酸或酸衍生的阴离子，Q是磷，硫，氮，砷或锑，并且每个R'是氢或烷基，芳基，芳烷基或烯基，k是 Q; 和任选地（c）式R 2 -OH的醇，其中R 2是可被氟化的烷基。还提供了制备含氟聚合物的方法，增加诱导时间的方法和含氟聚合物含有可固化或固化的含氟聚合物组合物的制品。

10. 发明公开

EP1549705A1 FLUOROPOLYMER COMPOSITIONS 有权
标题翻译： FLUORPOLYMERZUSAMMENSETZUNGEN
公开(公告)号：EP1549705A1
公开(公告)日：2005-07-06
申请号：EP03749774.0
申请日：2003-09-23
申请人： 3M Innovative Properties Company
发明人： GROOTAERT, Werner, M., A. , KOLB, Robert, E.
IPC分类号： C08K5/00 , C08K5/29
CPC分类号： C08K5/29 , C08F8/30 , C08F2800/10 , C08L27/12 , C08F214/262
摘要： Compositions comprising a fluoropolymer having interpolymerized units derived from a nitrogen-containing cure site monomer and an amidine-containing curative are provided. Also provided are a method of making a fluoropolymer and fluoropolymer articles containing curable or cured fluoropolymer compositions.

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