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1. 发明公开

KR1020050093781A 헥사플루오로프로필렌 옥사이드와 퍼플루오로아실플루오리드의 선택 반응 无效
标题翻译：十六烷基氧化物与全氟代氟化物的选择性反应
公开(公告)号：KR1020050093781A
公开(公告)日：2005-09-23
申请号：KR1020057011074
申请日：2003-10-23
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 구에라,미구엘,에이.
IPC分类号： C07C51/58 , C07C51/64
CPC分类号： C07C303/22 , C07C51/58 , Y02P20/582 , C07C59/135 , C07C59/315 , C07C309/82
摘要： A method is provided for reacting hexafluoropropylene oxide (HFPO) with a perfluoroacyl fluorides according to the formula X-Rf-COF (II) to selectively produce a monoaddition product according to the formula X- Rf- CF2-O-CF(CF3)COF (I), wherein selectivity for the monoaddition product over the biaddition product is 90% or greater or more typically 95% or greater. A continuous or repeated- batch process is provided comprising the steps of: a) providing a mixture of X-Rf-COF (II), a fluoride salt, and a polar solvent; b) adding hexafluoropropylene oxide (HFPO) in an amount such that X-R f-COF remains in molar excess of HFPO by at least 10% and reacting X- Rf-COF with HFPO; c) separating unreacted X-Rf-COF from a mixture of addition products of hexafluoropropylene oxide (HFPO) and X- Rf-COF; and d) repeating step a) using unreacted X-Rf- COF separated in step c).
摘要翻译：提供了一种用于使六氟环氧丙烷（HFPO）与根据式X-Rf-COF（II）的全氟酰基氟化物反应的方法，以选择性地制备根据式X- Rf-CF 2 -O-CF（CF 3）COF的单加成产物（I），其中加成产物相对于加合产物的选择性为90％或更大或更通常为95％或更高。提供连续或重复分批的方法，包括以下步骤：a）提供X-Rf-COF（II），氟化物盐和极性溶剂的混合物; b）加入六氟环氧丙烷（HFPO），其量使得X-R f-COF保持摩尔过量的HFPO至少10％，并使X- Rf-COF与HFPO反应; c）从六氟环氧丙烷（HFPO）和X-Rf-COF的加成产物的混合物中分离未反应的X-Rf-COF; 和d）重复步骤a）使用在步骤c）中分离的未反应的X-Rf-COF。

2. 发明公开

KR1020060117949A 강화된 중합체 전해질 막 无效
标题翻译：增强聚合物电解质膜
公开(公告)号：KR1020060117949A
公开(公告)日：2006-11-17
申请号：KR1020067009327
申请日：2004-10-13
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 구에라,미구엘,에이. , 얀드라시츠,마이클,에이.
IPC分类号： C08J5/22 , C08F8/30 , C08F8/00
CPC分类号： C08J5/2281 , C08J2379/06 , H01M8/1004 , H01M8/1023 , H01M8/103 , H01M8/1039 , H01M8/1072 , Y02P70/56
摘要： A method is provided for making a reinforced polymer electrolyte membrane, such as may be used in electrolytic cells such as fuel cells, by mixing a sulfonate- or sulfonyl halide-functional polymer with a bisamidine compound and subsequently trimerizing the amidine groups of the bisamidine compound to form triazine linkages. The sulfonyl halide or sulfonate groups may then be converted to sulfonic acid groups, yielding a polymer electrolyte reinforced with a polytriazine.
摘要翻译：提供了用于制造增强聚合物电解质膜的方法，例如可以用于诸如燃料电池的电解池中，通过将磺酸盐或磺酰卤官能聚合物与双脒化合物混合，随后将双脒化合物的脒基团三聚以形成三嗪键。然后将磺酰卤或磺酸酯基团转化为磺酸基团，产生用聚三嗪增强的聚合物电解质。

3. 发明公开

KR1020070008544A 직접 플루오르화에 의해 가교결합된 폴리머 전해질 막 无效
标题翻译：通过直接荧光交联的聚合物电解质膜
公开(公告)号：KR1020070008544A
公开(公告)日：2007-01-17
申请号：KR1020067014164
申请日：2004-11-19
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 구에라,미구엘,에이.
IPC分类号： C08F8/18 , C08F8/20 , C08J5/22 , C08J3/24
CPC分类号： H01M8/106 , C08F8/20 , C08J3/24 , C08J5/2237 , C08J5/2281 , C08J2327/18 , H01M8/1023 , H01M8/1039 , H01M8/1072 , H01M8/1088 , H01M2300/0082 , Y02P70/56
摘要： A method is provided for making a crosslinked polymer by direct fluorination of a non-perfluorinated polymer comprising first pendent groups which comprise sulfonyl halide groups or by direct fluorination of a polymer mixture of a first polymer which is a non-perfluorinated polymer and a second polymer which comprises first pendent groups which comprise sulfonyl halide groups. Such crosslinked polymers or polymer mixtures may be used to make polymer electrolyte membranes (PEM's) that may be used in electrolytic cells such as fuel cells and which should demonstrate increased durability in fuel cell use. ® KIPO & WIPO 2007
摘要翻译：提供了一种通过直接氟化非全氟化聚合物制备交联聚合物的方法，所述非全氟化聚合物包括包含磺酰卤基团的第一侧基，或直接氟化作为非全氟化聚合物的第一聚合物和第二聚合物的聚合物混合物其包括包含磺酰卤基团的第一侧基。这种交联聚合物或聚合物混合物可用于制备可用于电解池如燃料电池的聚合物电解质膜（PEM），并且应证明燃料电池使用中的耐久性提高。 ®KIPO＆WIPO 2007

4. 发明公开

KR1020050016482A 규소 물품을 위한 플루오로화합물 처리 无效
标题翻译：硅制品的氟化学处理
公开(公告)号：KR1020050016482A
公开(公告)日：2005-02-21
申请号：KR1020047019446
申请日：2003-04-01
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 둔바,티모티,디. , 자쩨라,로렌스,에이. , 펠레라이트,마크,제이. , 보드맨,래리,디. , 무어,조지쥐.,아이. , 구에라,미구엘,에이. , 엘스번드,체릴,엘.,에스.
IPC分类号： B81B3/00
摘要： Si-H 결합을 갖는 규소 기판은 하기 화학식의 플루오르화 올레핀을 이용하여 화학적으로 개질된다:

상기 식에서,
m은 1 이상의 정수이고,
n은 0 이상의 정수이고,
Z는 2가 연결기이고,
R
f 는 고도로 플루오르화된 유기기이다.

5. 发明公开

KR1020040034695A 일렉트릿의 제조 방법 无效
标题翻译：驻极体的制造方法
公开(公告)号：KR1020040034695A
公开(公告)日：2004-04-28
申请号：KR1020047003305
申请日：2002-08-12
申请人： 쓰리엠 이노베이티브 프로퍼티즈 컴파니
发明人： 초우,시흐-훙 , 우,티엔,충 , 메이,베티,지. , 샤베르그,마크,에스. , 부세라토,지나,엠. , 엘스베른드,셰릴,엘.,에스. , 구에라,미구엘,에이.
IPC分类号： H01G7/02
CPC分类号： D06M23/10 , B01D39/1623 , D04H1/56 , D06M11/05 , D06M23/06 , D06M23/105 , H01G7/023 , Y10T442/2418 , Y10T442/68
摘要： 중합체를 포함한 다공성 기판을, 중합체를 팽윤시킬 수 있는 용매를 포함한 조성물과 접촉시키고, 기판으로부터 용매를 제거하고, 기판에 일렉트릿 하전을 부여하기에 충분한 방식으로 기판을 물과 접촉시키는 것을 포함하는, 일렉트릿의 제조 방법.

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