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1. 发明专利

JP2014214091A 有機官能基含有オルガノポリシロキサンの製造方法有权
标题翻译：用于生产有机官能团的含有机硅氧烷的方法
公开(公告)号：JP2014214091A
公开(公告)日：2014-11-17
申请号：JP2013090159
申请日：2013-04-23
申请人：信越化学工業株式会社 , Shin Etsu Chem Co Ltd
发明人： HIROKAMI MUNENAO , TSUCHIDA KAZUHIRO , KUDO MUNEO
IPC分类号： C07F7/10 , C08G77/18 , C08G77/28 , C08G77/48
CPC分类号： C07F7/10 , C08G77/18 , C08G77/28 , C08G77/48
摘要：【解決手段】スルフィド基含有二価の有機基及び/又はメルカプト基含有有機基と加水分解性基とを含有する化合物を加水分解・縮合して、式(1)(A)a(B)b(C)c(D)dSiO(4-2a-b-c-d)/2(1)(Aはスルフィド基含有二価の有機基、Bはメルカプト基含有有機基、Cは加水分解性基、Dはアルキル基、アリール基、アルケニル基、エポキシ基含有有機基、(メタ)アクリロイル基含有有機基、ハロアルキル基からなる群から選ばれる有機基で、0≦2a
摘要翻译：待解决的问题：提供一种含有含硫基的有机基团和含有巯基的有机基团中的至少一种的有机聚硅氧烷和可水解基团的方法。解决方案：提供一种由式（1），（A）（B）（C）（D）SiO（1）（式中，A是含有硫醚基的二价有机基团; B是含有巯基的有机基团; C是可水解的基团; D是选自烷基，芳基，烯基，含环氧基的有机基团，（甲基）丙烯酰基的有机基团和卤代烷基基团中的有机基团; 0 当2a = 0,0

2. 发明专利

JP2008174430A Hydrophobic spherical silica fine particle, its manufacturing method and toner external additive for electrostatic charge image development 审中-公开
标题翻译：疏水性硅胶微粒，其静电荷图像发展的制造方法和调色剂外用添加剂
公开(公告)号：JP2008174430A
公开(公告)日：2008-07-31
申请号：JP2007011227
申请日：2007-01-22
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： KUDO MUNEO
IPC分类号： C01B33/18 , G03G9/08
摘要： PROBLEM TO BE SOLVED: To provide a hydrophobic spherical silica fine particle by which the fluidity of a toner can be improved and its manufacturing method.
SOLUTION: The hydrophobic spherical silica fine particle is obtained by hydrophobic treatment containing such steps that an R
4 SiO
3/2 unit (wherein, R
4 is a 1-20C substituted or nonsubstituted univalent hydrocarbon group) is introduced into the surface of a hydrophilic spherical silica fine particle consisting of an SiO
2 unit which is obtained by hydrolyzing and condensing at least one kind of compounds selected from the group consisting of a tetrahydrocarbyloxysilane compound whose general formula (1) is denoted as Si(OR
1 )
4 (wherein, R
1 s are same or different and each is a 1-6C univalent hydrocarbon group) and its partially hydrolyzed and condensed product and subsequently an R
6
3 SiO
1/2 unit (wherein, R
6 s are same or different and each is a 1-20C substituted or nonsubstituted univalent hydrocarbon group) is introduced. The hydrophobic spherical silica fine particle contains a hydrocarbyloxy group of 1,000 ppm or less and has a particle diameter of 0.01-5 μm.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供调色剂的流动性可以提高的疏水性球状二氧化硅细颗粒及其制造方法。解决方案：通过疏水处理获得疏水性球形二氧化硅细颗粒，其包括以下步骤：R 4 SP 3 SiO 3 SB 2单元（其中，R 4 = 是1-20C取代或未取代的一价烃基）引入到由SiO 2 SBS单元组成的亲水性球状二氧化硅细颗粒的表面中，所述亲水性球形二氧化硅细颗粒通过至少水解和缩合而获得一种选自由通式（1）表示为Si（OR SP）1的四羧基氧硅烷化合物组合的化合物（其中，R 1 相同或不同，并且各自为1-6C一价烃基）及其部分水解和缩合产物，随后是R 6 SP 3 > 1/2 单元（其中R 6相同或不同，分别为1-20C取代或未取代的一价烃基）。疏水性球状二氧化硅微粒含有1000ppm以下的烃氧基，粒径为0.01〜5μm。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2006154474A Toner external additive for electrostatic image development and toner 有权
标题翻译：用于静电图像发展和调色剂的调色剂外部添加剂
公开(公告)号：JP2006154474A
公开(公告)日：2006-06-15
申请号：JP2004346779
申请日：2004-11-30
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： KUDO MUNEO
IPC分类号： G03G9/08
摘要： PROBLEM TO BE SOLVED: To provide an external additive for toner which does not react or interact with an organic photoreceptor, causes neither deterioration nor cracking of the photoreceptor because it is softer than conventional inorganic fine particles, causes no toner adhesion to the photoreceptor because of good fluidity, and has charging property independent of the environmental condition, and to provide toner with the external additive added.
SOLUTION: The toner external additive for electrostatic image development comprises spherical hydrophilized silica fine particles having an average particle diameter of primary particles of 0.01-5 μm obtained by mixing (A) a spherical hydrophilic silica fine particle dispersion prepared by cohydrolysis and condensation reaction of a tetraalkoxysilane and/or a partial hydrolytic condensation product thereof with (B) a compound having a hydrolyzable silyl group and a hydrophilic group, reacting the spherical hydrophilic silica fine particles, and reacting the silica fine particles after the reaction with (C) a silazane compound and/or a silane compound. The toner with the external additive added is also provided.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：为了提供不与有机感光体反应或相互作用的调色剂的外部添加剂，因为它比常规的无机细颗粒更软，所以不会导致感光体的劣化或破裂，不会使调色剂粘附到感光体，因为具有良好的流动性，并且具有独立于环境条件的带电特性，并为添加了外部添加剂的调色剂提供色调。解决方案：用于静电图像显影的调色剂外用添加剂包括通过混合（A）通过共水解和缩合制备的球形亲水性二氧化硅细颗粒分散体获得的平均粒径为0.01-5μm的球形亲水化二氧化硅细颗粒四烷氧基硅烷和/或其部分水解缩合产物与（B）具有可水解甲硅烷基和亲水基团的化合物的反应，使球形亲水性二氧化硅细颗粒反应，并使反应后的二氧化硅细颗粒与（C）硅氮烷化合物和/或硅烷化合物。还提供添加了外部添加剂的调色剂。版权所有（C）2006，JPO＆NCIPI

4. 发明专利

JP2006152190A Thermoplastic synthetic resin film 有权
标题翻译：热塑性合成树脂膜
公开(公告)号：JP2006152190A
公开(公告)日：2006-06-15
申请号：JP2004348013
申请日：2004-12-01
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： IGUCHI YOSHINORI , KUDO MUNEO
IPC分类号： C08L101/00 , C08K9/06
摘要： PROBLEM TO BE SOLVED: To provide a thermoplastic synthetic resin film wherein injury by abrasion of films is hardly formed, and excellent in transparency, anti-blocking, processability upon molding and practical handling such as easy opening when it is used as a bag.
SOLUTION: The thermoplastic synthetic resin film is produced by molding into a film a composition comprising (A) a thermoplastic synthetic resin and (B) hydrophobic silica spherical particulates having an average primary particle size of 0.01-20 μm, which is obtained by a treatment for giving hydrophobic property, including a process of introducing an R
1
3 SiO
1/2 unit (wherein R
1 is the same or different and a substituted or non-substituted 1-6C monovalent hydrocarbon group) into the surface of hydrophilic silica particulates consisting substantially of SiO
2 units, followed by curing the film composition.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种热塑性合成树脂膜，其中几乎不形成由于磨损造成的损伤，并且在成型时的透明性，防粘连性，加工性以及实际的操作（例如当将其作为袋。解决方案：热塑性合成树脂膜通过将包含（A）热塑性合成树脂的组合物和（B）平均一次粒径为0.01〜20μm的疏水性二氧化硅球形微粒组合成膜而制造，得到通过用于提供疏水性的处理，包括引入R 1 SP 3 SiO 1/2 单元（其中R 1 相同或不同，取代或未取代的1-6C单价烃基）进入到基本上由SiO 2 单元组成的亲水性二氧化硅颗粒的表面中，然后固化膜组合物。版权所有（C）2006，JPO＆NCIPI

5. 发明专利

JP2006151764A Spherical silica fine particle, toner external additive for electrostatic charge image development and toner 有权
标题翻译：静电二氧化硅微粒，用于静电电荷图像开发和调色剂的调色剂外用添加剂
公开(公告)号：JP2006151764A
公开(公告)日：2006-06-15
申请号：JP2004346755
申请日：2004-11-30
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： KUDO MUNEO
IPC分类号： C01B33/18 , G03G9/08
摘要： PROBLEM TO BE SOLVED: To provide a toner external additive which hardly causes deterioration or crack of an organic photoreceptor because it does not react or interact with the photoreceptor and is softer than a conventional inorganic fine particle, prevent sticking of a toner onto the photoreceptor because it has good flowability, and has electrizability not affected by the environmental state, and to provide a toner that is obtained by externally adding the toner external additive, and a silica fine particle useful for their manufacturing.
SOLUTION: The spherical silica fine particle is obtained by reacting (1) a hydrophilic group-containing spherical silica fine particle, that is obtained by performing the cohydrolysis and condensation reactions of (A) a tetraalkoxy silane and/or its partially hydrolyzed and condensed material and (B) a compound having a hydrolyzable silyl group and a hydrophilic group, and (2) a silazane compound and/or a silane compound, has an average particle size of the primary particles of 0.01-5 μm, and has a hydrophobic surface and a hydrophilic group-containing nucleus. There are provided the toner external additive composed of the spherical silica fine particle, and the toner that is obtained by externally adding the toner external additive.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供一种调色剂外部添加剂，其不会导致有机感光体的劣化或裂纹，因为它不与感光体反应或相互作用并且比常规的无机细颗粒更软，防止调色剂粘附到感光体，因为其具有良好的流动性，并且具有不受环境状态影响的电气性，并且提供通过外部添加调色剂外添剂获得的调色剂和可用于其制造的二氧化硅微粒。＆lt; P＆gt;解决方案：通过使（A）含有亲水基团的球状二氧化硅细颗粒与（A）四烷氧基硅烷和/或其部分水解的共水解和缩合反应和（B）具有水解性甲硅烷基和亲水基团的化合物，和（2）硅氮烷化合物和/或硅烷化合物，所述一次粒子的平均粒径为0.01-5μm，并且具有疏水表面和含亲水基团的核。提供由球形二氧化硅细颗粒组成的调色剂外部添加剂和通过外部添加调色剂外添剂获得的调色剂。版权所有（C）2006，JPO＆NCIPI

6. 发明专利

JP2005015251A Hydrophobic spherical silica minute particle, its manufacturing method, and toner additive therewith for electrostatic charge image development 有权
标题翻译：疏水性二氧化硅颗粒，其制造方法和用于静电电荷图像发展的调色剂添加剂
公开(公告)号：JP2005015251A
公开(公告)日：2005-01-20
申请号：JP2003179692
申请日：2003-06-24
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： KUDO MUNEO
IPC分类号： G03G9/08 , C01B33/159
摘要： PROBLEM TO BE SOLVED: To provide an additive for a toner comprising a hydrophobic spherical silica minute particle capable of giving required electric charge to the toner, a hydrophobic spherical silica minute particle useful for manufacturing the additive, and its manufacturing method.
SOLUTION: This hydrophobic spherical silica minute particle has a frictional charge quantity with iron of -100-(-300) μC/g, a bulk density of 0.2-0.4 g/mL, and a particle diameter of 0.01-5 μm, and its manufacturing method and a toner additive for electrostatic charge image development with the particle are also presented.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种用于调色剂的添加剂，其包括能够向调色剂提供所需电荷的疏水性球形二氧化硅微粒，用于制造添加剂的疏水性球形二氧化硅微粒及其制造方法。解决方案：该疏水性球形二氧化硅微粒具有铁的摩擦带电量为-100-（ - 300）μC/ g，堆积密度为0.2-0.4g / mL，粒径为0.01-5μm 并且还提出了其制造方法和用于与颗粒进行静电荷图像显影的调色剂添加剂。版权所有（C）2005，JPO＆NCIPI

7. 发明专利

JP2004315712A Coating material composition for forming protective coating film, coated article, and multilayer laminate product 有权
公开(公告)号：JP2004315712A
公开(公告)日：2004-11-11
申请号：JP2003113737
申请日：2003-04-18
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： YAMATANI MASAAKI , SATO KAZUHARU , KUDO MUNEO
IPC分类号： B32B27/00 , C09D4/00 , C09D5/00 , C09D183/08 , C09D183/14
CPC分类号： C09D183/14 , C09D4/00 , Y10T428/3154 , Y10T428/31612 , Y10T428/31663 , C08G77/24
摘要： PROBLEM TO BE SOLVED: To provide a coating material composition superior in chemical resistance and scratch resistance and effective as a protective coating film for a plastic base material and the like, to provide a coated article having its hardened film, and to provide a multilayer laminate product. SOLUTION: The coating material composition for forming a protective coating film contains as the main component a disilane compound represented by the formula: X m R 1 3-m Si-Y-SiR 1 3-m X m or a (partial) hydrolysate thereof. In the formula R 1 is a 1-6C monovalent hydrocarbon group, Y is a divalent organic group containing one or more fluorine atoms, X is a hydrolyzable group, and m is 1, 2 or 3. COPYRIGHT: (C)2005,JPO&NCIPI

8. 发明专利

JP2014028797A Organopolysiloxane and production method therefor 有权
标题翻译：有机硅氧烷及其生产方法
公开(公告)号：JP2014028797A
公开(公告)日：2014-02-13
申请号：JP2013130097
申请日：2013-06-21
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： HIROKAMI MUNENAO , TSUCHIDA KAZUHIRO , KUDO MUNEO
IPC分类号： C07F7/18 , C08G77/28
CPC分类号： C07F7/0834 , C08G77/28 , C08K5/548
摘要： PROBLEM TO BE SOLVED: To provide a novel organopolysiloxane containing a sulfide group-containing organic group, a long chain alkyl group, and a hydrolyzable group, and to provide production method therefor.SOLUTION: A organopolysiloxane represented by the average composition formula (1), containing an organic group having at least sulfide group, a long chain alkyl group, and a hydrolyzable group. (A)(B)(C)(D)(R)SiO(1), where A is a divalent organic group containing sulfide group, B is an alkyl group having 5 to 10 carbon atoms, C is a hydrolyzable group and/or a hydroxyl group, D is a mercapto group-containing organic group, Ris an alkyl group having 1 to 4 carbon atoms or an aryl group having 6 to 10 carbon atoms, 0
摘要翻译：要解决的问题：提供含有含硫醚基的有机基团，长链烷基和可水解基团的新型有机聚硅氧烷，并提供其制备方法。解决方案：由平均组成式（1）表示的有机聚硅氧烷，，含有至少具有硫醚基的有机基团，长链烷基和可水解基团。（A）（B）（C）（D）（R）SiO（1），其中A是含有硫醚基的二价有机基团，B是具有5-10个碳原子的烷基，C是可水解基团和/ 或羟基，D是含巯基的有机基团，R是具有1至4个碳原子的烷基或具有6至10个碳原子的芳基，0 <2a <1,0

9. 发明专利

JP2007099582A Highly hydrophobic spherical sol-gel silica fine particle, method for producing the same, toner external additive for electrostatic charge image development composed of the fine particle, and developer using the toner external additive 有权
标题翻译：高亲水性溶胶凝胶二氧化硅微粒，其制造方法，用于微细颗粒组合的静电电荷图像发展的调色剂外用添加剂，以及使用调色剂外部添加剂的开发商
公开(公告)号：JP2007099582A
公开(公告)日：2007-04-19
申请号：JP2005294280
申请日：2005-10-07
申请人： Shin Etsu Chem Co Ltd , 信越化学工業株式会社
发明人： KUDO MUNEO
IPC分类号： C01B33/159 , G03G9/08
摘要： PROBLEM TO BE SOLVED: To provide highly hydrophobic spherical sol-gel silica fine particles; a method for producing the same; a toner external additive for electrostatic charge image development, which is excellent in flowability of a toner, caking resistance, fixability, cleaning property, environmental stability of the electrified charge amount, or the like and useful for an electrophotographic method, and to provide a developer containing the toner additive.
SOLUTION: The method for producing the highly hydrophobic spherical sol-gel silica fine particles having a hydrophobicity of ≥50 and comprising primary particles having an average particle diameter of 0.01-5 μm includes: a process for obtaining heat treated spherical sol-gel silica fine particles having a hydrophobicity of
摘要翻译：要解决的问题：提供高度疏水的球形溶胶 - 凝胶二氧化硅细颗粒; 其制造方法; 用于静电荷图像显影的调色剂外用添加剂，调色剂的流动性优异，耐结块性，定影性，清洁性，充电电荷量的环境稳定性等，并且可用于电子照相方法，并提供显影剂含有调色剂添加剂。解决方案：具有疏水性≥50的高疏水性球状溶胶凝胶二氧化硅微粒的制造方法，其包含平均粒径为0.01〜5μm的一次粒子，包括：获得热处理球状溶胶 - 凝胶二氧化硅微粒的方法，通过热处理疏水性为≥50的疏水性球状溶胶 - 凝胶状二氧化硅微粒而具有疏水性<50的凝胶状二氧化硅微粒，其包含平均粒径为0.01〜5μm的一次粒子，其通过使亲水性球状溶胶凝胶二氧化硅细颗粒，通过烃氧基硅烷的水解缩合得到疏水性; 以及使热处理的球状溶胶 - 凝胶二氧化硅细粒疏水的方法。还提供了通过该方法得到的二氧化硅微粒。调色剂外部添加剂包括二氧化硅细颗粒，显影剂含有调色剂外部添加剂。版权所有（C）2007，JPO＆INPIT

10. 发明专利

JP2007034156A Microcapsule, method for manufacturing the same, and electrophotographic toner composition 有权
标题翻译：微生物，其制备方法和电摄影色调剂组合物
公开(公告)号：JP2007034156A
公开(公告)日：2007-02-08
申请号：JP2005220638
申请日：2005-07-29
申请人： Nisshin Chem Ind Co Ltd , Shin Etsu Chem Co Ltd , 信越化学工業株式会社 , 日信化学工業株式会社
发明人： OKUDA HARUKAZU , SHIRASAWA KEIICHI , KUDO MUNEO , TANAKA MASAKI
IPC分类号： G03G9/08 , G03G9/087
摘要： PROBLEM TO BE SOLVED: To provide microcapsules or the like for obtaining electrophotographic toner composition that can be fixed while preventing offset in a heat roll fixing system and shows excellent blocking resistance with time.
SOLUTION: The microcapsules are composed of a shell resin comprising a vinyl resin or a polyester resin, and a core substance containing silicone oil. The microcapsules containing silicone oil as the core substance are compounded into toner so that the silicone oil is kept as a finely dispersed state in the toner. The silicone oil is prevented from bleeding out to the toner surface by the effect of the shell resin of the microcapsules. The microcapsules having silicone oil as the core substance can not release the inner silicone oil until the shell is broken by heating and pressurizing in fixing. As a result, offset resistance and blocking resistance can be improved.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供用于获得电子照相调色剂组合物的微胶囊等，其可以在防止热辊定影系统中的偏移的同时被固定并且随时间显示出优异的耐粘连性。解决方案：微胶囊由包含乙烯基树脂或聚酯树脂的壳树脂和含硅油的核心物质组成。将含有硅油作为核心物质的微胶囊复合到调色剂中，使得硅油保持为调色剂中的细分散状态。通过微胶囊的壳树脂的作用，防止硅油渗出到调色剂表面。具有硅油作为核心物质的微胶囊不能释放内部硅油，直到外壳在固定时通过加热和加压而破裂。结果，可以提高抗粘连性和抗粘连性。版权所有（C）2007，JPO＆INPIT

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