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1. 发明专利

SG102618A1 CONSTRUCTION METHOD OF AN ELEVATED CONCRETE SLAB USING PRECAST CONCRETE PANELS AND TEMPORARY ELEVATED SUPPORTING MEANS 未知
公开(公告)号：SG102618A1
公开(公告)日：2004-03-26
申请号：SG200101938
申请日：2001-03-27
申请人： ISHIDA MINORU , KENICHI NAKAJIMA , YUKIO TAKEI
发明人： ISHIDA MINORU , NAKAJIMA KENICHI , TAKEI YUKIO
IPC分类号： E04B5/18 , E04G11/48 , E04G17/14

2. 发明授权

US4350813A Process for producing 7-alkoxycarbonyl-6,8-dimethyl-4-hydroxymethyl-1-phthalazone and its intermediates 失效
标题翻译： 7-烷氧基羰基-6,8-二甲基-4-羟甲基-1-酞嗪酮及其中间体的制备方法
公开(公告)号：US4350813A
公开(公告)日：1982-09-21
申请号：US171363
申请日：1980-07-23
申请人： Yukio Takei , Masao Yoshida , Rinzo Nishizawa
发明人： Yukio Takei , Masao Yoshida , Rinzo Nishizawa
IPC分类号： C07D237/32 , C07D307/88
CPC分类号： C07D307/88 , C07D237/32
摘要： A novel process for producing 7-alkoxycarbonyl-6,8-dimethyl-4-hydroxymethyl-1-phthalazone, and its intermediates. 7-Alkoxycarbonyl-6,8-dimethyl-4-hydroxymethyl-1-phthalazone can be obtained by reacting substituted methylenetriphenylphosphorane with 3,5-dimethyl-4-alkoxycarbonylphthalic anhydride to obtain 6-alkoxycarbonyl-5,7-dimethyl-.DELTA..sup.3,.alpha. -substituted methylenephthalide, reacting the latter with hydrazine to obtain a phthalazone derivative, hydrolyzing the latter, halogenating the hydrolyzate to obtain 7-alkoxycarbonyl-6,8-dimethyl-4-(.alpha.-halogeno-.alpha.-substituted methyl)-1-phthalazone and then directly hydrolyzing and decarboxylating the latter or, when said 7-alkoxycarbonyl-6,8-dimethyl-4-(.alpha.-halogeno-.alpha.-substituted methyl)-1-phthalazone is 7-alkoxycarbonyl-6,8-dimethyl-1-phthalazone-4-.alpha.-halogenoacetic acid, reacting it with a carboxylic acid salt such as sodium acetate and simultaneously decarboxylating the acyloxylated compound and then hydrolyzing the decarboxylated product or firstly decarboxylating the 1-phthalazone-4-.alpha.-halogenoacetic acid derivative, reacting the decarboxylated product with said carboxylic acid salt and then hydrolyzing the reaction product or when said 7-alkoxycarbonyl-6,8-dimethyl-4-(.alpha.-halogeno-.alpha.-substituted methyl)-1-phthalazone is 7-alkoxycarbonyl-4-(.alpha.-carbamoyl-.alpha.-halogenomethyl)-6,8-dimethyl-1-phthalazone, reacting it with said carboxylic acid salt and then hydrolyzing and decarboxylating the acyloxylated compound simultaneously.
摘要翻译： 7-烷氧基羰基-6,8-二甲基-4-羟甲基-1-酞嗪酮及其中间体的新方法。 7-烷氧基羰基-6,8-二甲基-4-羟甲基-1-酞嗪酮可以通过使取代的亚甲基三苯基正膦与3,5-二甲基-4-烷氧基羰基邻苯二甲酸酐反应得到6-烷氧基羰基-5,7-二甲基-D-三唑， α-取代的亚甲基对苯二甲酸盐，使后者与肼反应得到酞嗪衍生物，水解后者，卤化水解产物得到7-烷氧基羰基-6,8-二甲基-4-（α-卤素-α-取代的甲基）-1- 然后直接水解和脱羧后者，或当所述7-烷氧基羰基-6,8-二甲基-4-（α-卤素-α-取代的甲基）-1-酞嗪酮为7-烷氧基羰基-6,8-二甲基 - 1-酞嗪-4-α-卤代乙酸，使其与羧酸盐如乙酸钠反应，同时使酰氧基化化合物脱羧，然后水解脱羧产物，或首先使1-酞嗪-4--α-卤代乙酸衍生物脱羧使脱羧产物与所述羧酸盐反应，然后水解反应产物，或当所述7-烷氧基羰基-6,8-二甲基-4-（α-卤代-α-取代的甲基）-1-酞嗪酮为7-烷氧羰基 - 将4-（α-氨基甲酰基-α-卤代甲基）-6,8-二甲基-1-酞嗪酮与所述羧酸盐反应，然后同时水解和脱羧酰氧化化合物。

3. 发明授权

US4464532A Intermediates of 7-alkoxycarbonyl-6,8-dimethyl-4-hydroxymethyl-1-phthalazone 失效
标题翻译： 7-烷氧基羰基-6,8-二甲基-4-羟甲基-1-酞嗪酮的中间体
公开(公告)号：US4464532A
公开(公告)日：1984-08-07
申请号：US386001
申请日：1982-06-07
申请人： Yukio Takei , Masao Yoshida , Rinzo Nishizawa
发明人： Yukio Takei , Masao Yoshida , Rinzo Nishizawa
IPC分类号： C07D237/32 , C07D307/88
CPC分类号： C07D307/88 , C07D237/32
摘要： A novel process for producing 7-alkoxycarbonyl-6,8-dimethyl-4-hydroxymethyl-1-phthalazone, and its intermediates. 7-Alkoxycarbonyl-6,8-dimethyl-4-hydroxymethyl-1-phthalazone can be obtained by reacting substituted methylenetriphenylphosphorane with 3,5-dimethyl-4-alkoxycarbonylphthalic anhydride to obtain 6-alkoxycarbonyl-5,7-dimethyl-.DELTA..sup.3,.alpha. -substituted methylenephthalide, reacting the latter with hydrazine to obtain a phthalazone derivative, hydrolyzing the latter, halogenating the hydrolyzate to obtain 7-alkoxycarbonyl-6,8-dimethyl-4-(.alpha.-halogeno-.alpha.-substituted methyl)-1-phthalazone and then directly hydrolyzing and decarboxylating the latter or, when said 7-alkoxycarbonyl-6,8-dimethyl-4-(.alpha.-halogeno-.alpha.-substituted methyl)-1-phthalazone is 7-alkoxycarbonyl-6,8-dimethyl-1-phthalazone-4-.alpha.-halogenoacetic acid, reacting it with a carboxylic acid salt such as sodium acetate and simultaneously decarboxylating the acyloxylated compound and then hydrolyzing the decarboxylated product or firstly decarboxylating the 1-phthalazone-4-.alpha.-halogenoacetic acid derivative, reacting the decarboxylated product with said carboxylic acid salt and then hydrolyzing the reaction product or when said 7-alkoxycarbonyl-6,8-dimethyl-4-(.alpha.-halogeno-.alpha.-substituted methyl)-1-phthalazone is 7-alkoxycarbonyl-4-(.alpha.-carbamoyl-.alpha.-halogenomethyl-6,8-dimethyl-1-phthalazone, reacting it with said carboxylic acid salt and then hydrolyzing and decarboxylating the acyloxylated compound simultaneously.
摘要翻译： 7-烷氧基羰基-6,8-二甲基-4-羟甲基-1-酞嗪酮及其中间体的新方法。 7-烷氧基羰基-6,8-二甲基-4-羟甲基-1-酞嗪酮可以通过使取代的亚甲基三苯基正膦与3,5-二甲基-4-烷氧基羰基邻苯二甲酸酐反应得到6-烷氧基羰基-5,7-二甲基-D-三唑， α-取代的亚甲基对苯二甲酸盐，使后者与肼反应得到酞嗪衍生物，水解后者，卤化水解产物得到7-烷氧基羰基-6,8-二甲基-4-（α-卤素-α-取代的甲基）-1- 然后直接水解和脱羧后者，或当所述7-烷氧基羰基-6,8-二甲基-4-（α-卤素-α-取代的甲基）-1-酞嗪酮为7-烷氧基羰基-6,8-二甲基 - 1-酞嗪-4-α-卤代乙酸，使其与羧酸盐如乙酸钠反应，同时使酰氧基化化合物脱羧，然后水解脱羧产物，或首先使1-酞嗪-4--α-卤代乙酸衍生物脱羧使脱羧产物与所述羧酸盐反应，然后水解反应产物，或当所述7-烷氧基羰基-6,8-二甲基-4-（α-卤代-α-取代的甲基）-1-酞嗪酮为7-烷氧羰基 - 4-（α-氨基甲酰基-α-卤代甲基-6,8-二甲基-1-酞嗪酮）与所述羧酸盐反应，然后同时水解和脱羧酰氧基化化合物。

4. 发明授权

US3951728A Method of treating semiconductor wafers 失效
标题翻译：处理半导体晶片的方法
公开(公告)号：US3951728A
公开(公告)日：1976-04-20
申请号：US493106
申请日：1974-07-30
申请人： Etsuo Egashira , Shinichiro Miyoshi , Yukio Takei , Masato Fujita
发明人： Etsuo Egashira , Shinichiro Miyoshi , Yukio Takei , Masato Fujita
IPC分类号： C30B33/00 , H01L21/00 , H01L21/308 , H01L21/465 , H01L21/467 , H01L29/00 , H01L21/20 , H01L21/302
CPC分类号： H01L21/00 , C30B33/00 , H01L21/308 , H01L21/465 , H01L21/467 , H01L29/00 , Y10S148/054
摘要： A method of treating wafers, wherein a plurality of wafers are stacked and immersed in an etchant, to work, i.e., etch, the peripheral surfaces of the wafers. Sliced semiconductor wafers or metallic or ceramic wafers can be chemically chamfered in this manner.
摘要翻译：一种处理晶片的方法，其中多个晶片被堆叠并浸没在蚀刻剂中，以工作，即蚀刻晶片的外围表面。切片半导体晶片或金属或陶瓷晶片可以以这种方式进行化学倒角。

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