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1. 发明授权

US07994090B2 Process for producing fine particles of solid solution 失效
标题翻译：生产固溶微细颗粒的方法
公开(公告)号：US07994090B2
公开(公告)日：2011-08-09
申请号：US12506415
申请日：2009-07-21
申请人： Yoshihisa Beppu , Kazuo Sunahara
发明人： Yoshihisa Beppu , Kazuo Sunahara
IPC分类号： B01J23/10 , B01J21/02
CPC分类号： C01G25/006 , B01J23/002 , B01J35/023 , B01J35/1014 , B01J37/08 , B01J2523/00 , B82Y30/00 , C01P2002/50 , C01P2004/10 , C01P2004/20 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C03C3/155 , C03C10/00 , C03C23/008 , H01M4/9016 , B01J2523/24 , B01J2523/25 , B01J2523/305 , B01J2523/3706 , B01J2523/3712 , B01J2523/48 , B01J2523/3787 , B01J2523/3725 , B01J2523/3718 , B01J2523/375 , B01J2523/36
摘要： Provided is a process for readily producing fine particles of a solid solution having a small particle size, comprising a solid solution of zirconia, ceria and a rare earth oxide in a desired composition, and being highly crystalline.The process for producing the fine particles of the solid solution comprises the following steps in the order named: obtaining a melt comprising, in terms of mol % on an oxide basis, from 5 to 50% ZrO2, CeO2 and RE2O3 (where RE is at least one member selected from rare earth elements other than Ce) in total, from 10 to 50% RO (where R is at least one member selected from the group consisting of Mg, Ca, Sr, Ba and Zn), and from 30 to 75% B2O3; quenching the melt to obtain an amorphous material; heating the amorphous material to obtain precipitates containing crystals of a solid solution with ZrO2, CeO2 and RE2O3; and separating the crystals of the solid solution from the precipitates to obtain fine particles of the solid solution.
摘要翻译：本发明提供容易制造具有小粒径的固溶体的细颗粒的方法，其包含氧化锆，二氧化铈和稀土氧化物的固溶体，并具有高结晶性。制造固溶体微粒的方法包括以下顺序的步骤：获得包含以氧化物为基准的摩尔％为5至50％的ZrO 2，CeO 2和RE 2 O 3（其中RE为至少一种选自Ce以外的稀土元素的组分），10至50％的RO（其中R是选自Mg，Ca，Sr，Ba和Zn中的至少一种），并且从30至 75％B2O3; 淬火熔体以获得无定形材料; 加热无定形材料，得到含有ZrO 2，CeO 2和RE 2 O 3的固溶体晶体的析出物; 并将固溶体的晶体与析出物分离，得到固溶微细颗粒。

2. 发明申请

US20100298127A1 CERIA-ZIRCONIA SOLID SOLUTION CRYSTAL FINE PARTICLES AND THEIR PRODUCTION PROCESS 失效
标题翻译： CERIA-ZIRCONIA固体溶液水晶微粒及其生产工艺
公开(公告)号：US20100298127A1
公开(公告)日：2010-11-25
申请号：US12796492
申请日：2010-06-08
申请人： Yoshihisa Beppu , Kazuo Sunahara
发明人： Yoshihisa Beppu , Kazuo Sunahara
IPC分类号： B01J21/02 , B01J23/10
CPC分类号： C01F17/0043 , B82Y30/00 , C01G25/00 , C01G25/02 , C01P2002/50 , C01P2002/72 , C01P2002/77 , C01P2004/10 , C01P2004/16 , C01P2004/20 , C01P2004/64 , C01P2006/12 , C01P2006/13
摘要： To provide a process for producing ceria-zirconia solid solution crystal fine particles having high crystallinity, being excellent in uniformity of composition and particle size, having a small particle size and a high specific surface area and being excellent in heat resistance, and such solid solution crystal fine particles.A process comprises a step of obtaining a melt containing, as represented by mol % based on oxides, from 5 to 50% of (ZrO2+CeO2), from 10 to 60% of RO (wherein R is at least one member selected from the group consisting of Mg, Ca, Sr and Ba) and from 25 to 70% of B2O3, a step of quenching the melt to obtain an amorphous material, a step of heating the amorphous material at a temperature of from 550 to 1000° C. to precipitate a ceria-zirconia solid solution crystal in the amorphous material, and a step of separating components other than the ceria-zirconia solid solution crystal from the obtained precipitates to obtain the ceria-zirconia solid solution crystal fine particles, in this order.
摘要翻译：为了提供具有高结晶度的二氧化铈 - 氧化锆固溶体结晶微粒的制造方法，组成和粒度均匀性优异，粒径小，比表面积小，耐热性优异的固溶体晶体细颗粒。一种方法包括以下步骤：获得含有以氧化物为基准的摩尔％为5〜50％的（ZrO 2 + CeO 2），10〜60％的RO（其中，R为至少1种选自由Mg，Ca，Sr和Ba组成的组）和25〜70％的B 2 O 3，使熔融物淬火以获得无定形材料的步骤，在550〜1000℃的温度下加热无定形材料的工序。在无定型材料中析出二氧化铈 - 氧化锆固溶体晶体，以及从得到的析出物中分离除二氧化铈 - 氧化锆固溶体结晶以外的成分的工序，得到氧化铈 - 氧化锆固溶体结晶微粒。

3. 发明申请

US20090113809A1 FINE PARTICLES OF OXIDE CRYSTAL AND SLURRY FOR POLISHING WHICH CONTAINS THE FINE PARTICLES 审中-公开
标题翻译：氧化物晶体和浆料的精细颗粒，用于含有细颗粒的抛光
公开(公告)号：US20090113809A1
公开(公告)日：2009-05-07
申请号：US12258106
申请日：2008-10-24
申请人： Tomohiro Sakai , Yoshihisa Beppu , Kazuo Sunahara
发明人： Tomohiro Sakai , Yoshihisa Beppu , Kazuo Sunahara
IPC分类号： C09K3/14 , B32B1/00 , C01F17/00
CPC分类号： H01L21/31053 , B82Y30/00 , C01F17/0043 , C01P2002/60 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2006/10 , C09K3/1409 , C09K3/1454 , H01L21/3212 , Y10T428/2982
摘要： To provide a slurry for polishing which is excellent in polishing properties, can suppress scratches and is appropriate for accurate polishing in semiconductor production steps, and fine particles of oxide crystal for it.Fine particles of oxide crystal, characterized in that the ratio of the crystallite size measured by X-ray diffraction method and calculated by Scherrer method to the average primary particle size equivalent to sphere from the specific surface area measured by BET is the crystallite size: the average primary particle size=1:0.8 to 1:2.5. A slurry for polishing, characterized in that the fine particles of oxide crystal are dispersed in a liquid medium, and from 0.1 to 40 mass % of the fine particles of oxide crystal are contained, per the total mass of the slurry for polishing.
摘要翻译：为了提供抛光性能优异的抛光用浆料，可以抑制划痕，适用于半导体制造工序中的精确研磨以及氧化物结晶用微粒。氧化物晶体的细颗粒，其特征在于，通过X射线衍射法测量并通过Scherrer方法计算的微晶尺寸与通过BET测量的比表面积相当于球体的平均一次粒径的比率为微晶尺寸：平均一次粒径= 1:0.8至1:2.5。一种用于抛光的浆料，其特征在于，将氧化物晶体的细颗粒分散在液体介质中，并且相对于用于抛光的浆料的总质量，含有0.1〜40质量％的氧化物结晶微粒。

4. 发明申请

US20060046320A1 Liquid composition for forming ferroelectric thin film and process for producing ferroelectric thin film 失效
标题翻译：用于形成铁电薄膜的液体组合物和用于制备铁电薄膜的方法
公开(公告)号：US20060046320A1
公开(公告)日：2006-03-02
申请号：US11260209
申请日：2005-10-28
申请人： Kazuo Sunahara , Hiroyuki Tomonaga , Yoshihisa Beppu
发明人： Kazuo Sunahara , Hiroyuki Tomonaga , Yoshihisa Beppu
IPC分类号： H01L21/00
CPC分类号： C01G49/0054 , B82Y30/00 , C01G23/003 , C01G23/005 , C01G23/006 , C01G25/00 , C01G33/00 , C01G35/00 , C01G49/0027 , C01G49/0036 , C01P2002/34 , C01P2004/54 , C01P2004/64 , C01P2006/40 , C23C18/1216 , C23C18/127 , H01L21/31691
摘要： It is an object to provide a liquid composition for forming a thin film, with which a ferroelectric thin film having excellent characteristics can be prepared even by baking at a low temperature, and a process for producing a ferroelectric thin film using it. The above object is achieved by use of a liquid composition for forming a ferroelectric thin film, characterized in that in a liquid medium, ferroelectric oxide particles being plate or needle crystals, which are represented by the formula ABO3 (wherein A is at least one member selected from the group consisting of Ba2+, Sr2+, Ca2+, Pb2+, La2+, K+ and Na+, and B is at least one member selected from the group consisting of Ti4+, Zr4+, Nb5+, Ta5+ and Fe3+) and have a Perovskite structure and which have an average primary particle size of at most 100 nm and an aspect ratio of at least 2, are dispersed, and a soluble metal compound which forms a ferroelectric oxide by heating, is dissolved.
摘要翻译：本发明的目的是提供一种用于形成薄膜的液体组合物，即使通过低温烘烤也可制备出具有优异特性的铁电薄膜，以及使用该薄膜制造铁电薄膜的工艺。上述目的通过使用用于形成铁电薄膜的液体组合物来实现，其特征在于，在液体介质中，由式ABO 3 3表示的板状或针状晶体的铁电氧化物颗粒（其中A是选自Ba 2+，Sr 2+，Ca 2+，Pb 2+中的至少一种。 > 2 + ，La 2+，K + +和Na + +，B是选自以下的至少一种：由Ti 4+，Zr 4+，Nb 5+，Ta 5+和Fe 4+组成， 3 +），并且具有钙钛矿结构，其平均初级粒径为至多100nm，纵横比为2以上，通过加热形成铁电氧化物的可溶性金属化合物，溶解

5. 发明申请

US20060001069A1 Composition for forming dielectric layer, MIM capacitor and process for its production 失效
标题翻译：用于形成介电层的组合物，MIM电容器及其制造方法
公开(公告)号：US20060001069A1
公开(公告)日：2006-01-05
申请号：US11150231
申请日：2005-06-13
申请人： Hiroyuki Tomonaga , Katsuaki Miyatani , Yoshihisa Beppu , Kumiko Takahashi , Kazuo Sunahara
发明人： Hiroyuki Tomonaga , Katsuaki Miyatani , Yoshihisa Beppu , Kumiko Takahashi , Kazuo Sunahara
IPC分类号： H01L21/8242 , H01L27/108
CPC分类号： H01L21/02197 , H01G4/1218 , H01G4/1236 , H01G4/1254 , H01L21/31691 , H01L28/55 , H01L28/65
摘要： To provide a composition for forming a dielectric layer excellent in dielectric constant and withstand voltage properties, a MIM capacitor and a process for its production. A composition for forming a dielectric layer, which comprises fine particles of perovskite type dielectric crystal, glass frit, and a hydrolysable silicon compound or its oligomer, and a MIM capacitor comprising a substrate, and a bottom electrode layer, a dielectric layer having a structure such that fine particles of perovskite type dielectric crystal are dispersed in a silicon oxide matrix containing glass-forming ions and a top electrode, formed on the substrate in this order.
摘要翻译：为了提供用于形成介电常数和耐电压性能优异的介电层的组合物，MIM电容器及其制造方法。一种用于形成电介质层的组合物，其包含钙钛矿型电介质晶体的微细颗粒，玻璃料和可水解硅化合物或其低聚物，以及包含基底的MIM电容器和底部电极层，具有结构使得细小颗粒的钙钛矿型电介质晶体分散在含有玻璃形成离子的氧化硅基体和顶部电极中，所述氧化硅基体依次形成在基板上。

6. 发明授权

US07857680B2 Method for producing glass substrate for magnetic disk, and magnetic disk 失效
标题翻译：用于制造用于磁盘的玻璃基板和磁盘的方法
公开(公告)号：US07857680B2
公开(公告)日：2010-12-28
申请号：US11739997
申请日：2007-04-25
申请人： Katsuaki Miyatani , Osamu Miyahara , Yuzuru Tanabe , Hiroshi Usui , Yoshihisa Beppu , Kazuo Sunahara , Mitsuru Horie , Satoshi Kashiwabara , Tomohiro Sakai , Yoshinori Kon , Iori Yoshida
发明人： Katsuaki Miyatani , Osamu Miyahara , Yuzuru Tanabe , Hiroshi Usui , Yoshihisa Beppu , Kazuo Sunahara , Mitsuru Horie , Satoshi Kashiwabara , Tomohiro Sakai , Yoshinori Kon , Iori Yoshida
IPC分类号： B24C3/00 , C01G1/00 , G11B5/706 , G11B5/64 , C03C21/00
CPC分类号： G11B5/8404 , C03C3/15 , C03C10/0054 , C03C19/00
摘要： A method for producing a glass substrate for a magnetic disk by polishing a circular glass plate, which comprises a step of polishing the principal plane of the circular glass plate by using a slurry containing a CeO2 crystal powder, the CeO2 crystal powder being obtained in such a manner that a melt containing CeO2 is quenched to obtain an amorphous material, and the amorphous material is subjected to heat treatment to obtain a CeO2 crystals-precipitated amorphous material, which is subjected to acid treatment to separate and extract the CeO2 crystal powder from the CeO2 crystals-precipitated amorphous material.
摘要翻译：通过研磨圆形玻璃板来制造用于磁盘的玻璃基板的方法，该方法包括通过使用含有CeO 2晶体粉末的浆料对圆形玻璃板的主平面进行研磨的步骤，所述CeO 2晶体粉末是这样获得的使含有CeO 2的熔体淬火以获得无定形材料的方式，并且对非晶材料进行热处理以获得CeO 2晶体沉淀的非晶态材料，其经过酸处理以从CeO 2晶体粉末中分离并提取CeO 2晶体粉末 CeO2晶体沉淀的非晶态材料。

7. 发明申请

US20100159246A1 PROCESS FOR PRODUCING OXIDE CRYSTAL FINE PARTICLES 审中-公开
标题翻译：生产氧化锆晶粒的方法
公开(公告)号：US20100159246A1
公开(公告)日：2010-06-24
申请号：US12717228
申请日：2010-03-04
申请人： Tomohiro Sakai , Yoshihisa Beppu , Hiroyuki Suzuki , Nobuo Inuzuka
发明人： Tomohiro Sakai , Yoshihisa Beppu , Hiroyuki Suzuki , Nobuo Inuzuka
IPC分类号： C01F17/00 , B32B5/16
CPC分类号： C09K3/1427 , B82Y30/00 , C01B13/14 , C01F17/0043 , C01G25/006 , C01P2002/50 , C01P2002/60 , C01P2004/04 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/10 , C01P2006/12 , C01P2006/22 , C09K3/1409 , Y10T428/2982
摘要： To provide a process for producing fine particles of crystalline oxide which have high crystallinity, are excellent in uniformity of the composition and particle diameter, and have a small particle diameter, and such fine particles of crystalline oxide.A process for producing fine particles of crystalline oxide, which comprises:a step of obtaining a melt containing an oxide of M (M is at least one member selected from the group consisting of Ce, Ti, Zr, Al, Fe, Zn, Mn, Cu, Co, Ni, Bi, Pb, In, Sn and rare earth elements (excluding Ce)) and B2O3,a step of rapidly cooling the melt to form an amorphous material,a step of pulverizing the amorphous material to obtain a pulverized material having a volume-based particle size distribution within a range of from 0.1 to 40 μm,a step of heating the pulverized material to precipitate an oxide crystal containing M in the pulverized particles, anda step of separating components other than the oxide crystal containing M from the crystal-precipitated particles to obtain fine particles of crystalline oxide containing M, in this order.
摘要翻译：为了提供具有高结晶度的结晶氧化物微粒的制造方法，组合物的均匀性和粒径优异，粒径小，结晶性氧化物微粒等。一种生产结晶氧化物微粒的方法，包括：获得含有M的氧化物的熔体的步骤（M是选自Ce，Ti，Zr，Al，Fe，Zn，Mn中的至少一种，Cu，Co，Ni，Bi，Pb，In，Sn和稀土元素（Ce除外））和B 2 O 3，将熔体快速冷却以形成非晶态材料的步骤，具有0.1〜40μm范围内的体积粒径分布的材料，在粉碎粒子中加热粉碎物质使含有M的氧化物晶体析出的工序，除了含有 M从结晶析出的颗粒中依次获得含有M的结晶氧化物的微粒。

8. 发明授权

US07381232B2 Process for producing CeO2 fine particles and polishing slurry containing such fine particles 失效
标题翻译：用于制备CeO 2微粒和含有这种细颗粒的抛光浆料的方法
公开(公告)号：US07381232B2
公开(公告)日：2008-06-03
申请号：US11745024
申请日：2007-05-07
申请人： Yoshihisa Beppu , Tomohiro Sakai , Satoshi Kashiwabara , Kazuo Sunahara
发明人： Yoshihisa Beppu , Tomohiro Sakai , Satoshi Kashiwabara , Kazuo Sunahara
IPC分类号： B24D3/02 , C09C1/68 , C09K3/14
CPC分类号： C09K3/1427 , B82Y30/00 , C01F17/0043 , C01P2002/60 , C01P2002/72 , C01P2004/62 , C01P2004/64 , C09G1/02 , C09K3/1463 , H01L21/31053
摘要： To provide a process for producing CeO2 fine particles having high crystallinity, being excellent in uniformity of composition and particle size and having a small particle size, and a polishing slurry containing such fine particles.A process for producing CeO2 fine particles, which comprises a step of obtaining a melt containing, as represented by mol % based on oxides, from 5 to 50% of CeO2, from 10 to 50% of RO (wherein R is at least one member selected from the group consisting of Mg, Ca, Sr and Ba) and from 30 to 75% of B2O3, a step of quenching the melt to obtain an amorphous material, a step of precipitating CeO2 crystals from the amorphous material, and a step of separating the CeO2 crystals from the obtained crystallized product, in this order. A polishing slurry containing from 0.1 to 20 mass % of such fine particles.
摘要翻译：为了提供一种制备具有高结晶度的CeO 2 细小颗粒的方法，组合物的均匀性和粒径均匀性以及粒径小的抛光浆料和含有这种细颗粒的研磨浆料。一种制备CeO 2 细颗粒的方法，其包括以下步骤：获得含有以氧化物的摩尔％表示的含有5至50％CeO 2的熔体的熔体，，RO为10〜50％（其中R为选自Mg，Ca，Sr和Ba中的至少1种）和30〜75％的B 2 O 2， 3，淬火熔体以获得无定形材料的步骤，从无定形材料中沉淀CeO 2结晶的步骤，以及分离CeO 2 / 从得到的结晶产物中按此顺序。含有0.1〜20质量％的这种微粒的研磨浆料。

9. 发明申请

US20070251270A1 METHOD FOR PRODUCING GLASS SUBSTRATE FOR MAGNETIC DISK, AND MAGNETIC DISK 失效
标题翻译：用于生产用于磁盘的玻璃基板的方法和磁盘
公开(公告)号：US20070251270A1
公开(公告)日：2007-11-01
申请号：US11739997
申请日：2007-04-25
申请人： Katsuaki Miyatani , Osamu Miyahara , Yuzuru Tanabe , Hiroshi Usui , Yoshihisa Beppu , Kazuo Sunahara , Mitsuru Horie , Satoshi Kashiwabara , Tomohiro Sakai , Yoshinori Kon , Iori Yoshida
发明人： Katsuaki Miyatani , Osamu Miyahara , Yuzuru Tanabe , Hiroshi Usui , Yoshihisa Beppu , Kazuo Sunahara , Mitsuru Horie , Satoshi Kashiwabara , Tomohiro Sakai , Yoshinori Kon , Iori Yoshida
IPC分类号： G11B5/706 , C03C21/00 , C03C10/00
CPC分类号： G11B5/8404 , C03C3/15 , C03C10/0054 , C03C19/00
摘要： A method for producing a glass substrate for a magnetic disk by polishing a circular glass plate, which comprises a step of polishing the principal plane of the circular glass plate by using a slurry containing a CeO2 crystal powder, the CeO2 crystal powder being obtained in such a manner that a melt containing CeO2 is quenched to obtain an amorphous material, and the amorphous material is subjected to heat treatment to obtain a CeO2 crystals-precipitated amorphous material, which is subjected to acid treatment to separate and extract the CeO2 crystal powder from the CeO2 crystals-precipitated amorphous material.
摘要翻译：一种通过研磨圆形玻璃板来制造用于磁盘的玻璃基板的方法，该方法包括通过使用含有CeO 2结晶粉末的浆料对圆形玻璃板的主平面进行抛光的步骤，以使含有CeO 2 H 2的熔体淬火获得无定形材料的方式获得CeO 2结晶粉末，并对非晶材料进行热处理以获得 CeO 2结晶沉淀的非晶态材料，其经过酸处理以从CeO 2结晶中分离并提取CeO 2/2结晶粉末 - 沉淀的无定形材料。

10. 发明申请

US20060124890A1 Liquid composition for forming ferroelectric thin film and process for producing ferroelectric thin film 审中-公开
标题翻译：用于形成铁电薄膜的液体组合物和用于制备铁电薄膜的方法
公开(公告)号：US20060124890A1
公开(公告)日：2006-06-15
申请号：US11340548
申请日：2006-01-27
申请人： Kazuo Sunahara , Hiroyuki Tomonaga , Yoshihisa Beppu
发明人： Kazuo Sunahara , Hiroyuki Tomonaga , Yoshihisa Beppu
IPC分类号： H01L41/18
CPC分类号： H01L21/02197 , B82Y30/00 , C01G23/003 , C01G29/00 , C01P2004/64 , C01P2006/40 , H01B1/22 , H01L21/02282 , H01L21/316 , H01L21/31691
摘要： The present invention provides a liquid composition for forming a thin film, with which a ferroelectric thin film having excellent characteristics can be prepared even by baking at a low temperature, and a process for producing a ferroelectric thin film using it. A liquid composition for forming a ferroelectric thin film is used, which is characterized by comprising a liquid medium, crystalline ferroelectric oxide particles represented by the formula (Bi2O2)2+(Bim-1TimO3.5m-0.5)2− (wherein m is an integer of from 1 to 5) or (Bi2O2)2+(Am-1TimO3.5m-0.5)2− (wherein A is Bi3+ or La3+, the La3+/Bi3+ ratio is from 0.05 to 0.5, and m is an integer of from 1 to 5) and having an average primary particle diameter of at most 100 nm, dispersed in the liquid medium, and a soluble metal compound capable of forming a ferroelectric oxide by heating, dissolved in the liquid medium.
摘要翻译：本发明提供了一种用于形成薄膜的液体组合物，即使通过低温烘烤也可制备出具有优异特性的铁电薄膜，以及使用该薄膜制造铁电薄膜的方法。使用用于形成铁电薄膜的液体组合物，其特征在于包括液体介质，由式（Bi 2 O 2 O 2）表示的结晶铁电氧化物颗粒，（2-m-1）Ti 3 O 3 3.5m-0.5 3）2 - / SUP >（其中m是1至5的整数）或（Bi 2 O 2 O 2）2 +（A m- 1 3 3 （其中A是Bi 3+ 或La 3+，La 3+ / Bi 3+比为0.05至0.5，m为1至 5），分散在液体介质中的平均一次粒径为100nm以下，溶解在液体介质中的能够通过加热形成铁电氧化物的可溶性金属化合物。

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