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    • 3. 发明申请
    • Fine nickel powder and process for producing the same
    • 细镍粉及其制造方法
    • US20070101822A1
    • 2007-05-10
    • US11266495
    • 2005-11-04
    • Yasumasa HattoriEgon Matijevic
    • Yasumasa HattoriEgon Matijevic
    • B22F9/22
    • B22F9/22B22F1/0018B22F2001/0033B22F2998/00B82Y30/00B22F1/0055B22F2201/013B22F2201/02
    • An efficient process for producing fine nickel powder, capable of metallizing the powder at low temperature to prevent its sintering, and fine nickel powder produced by the process, composed of particles having a flat shape, diameter of limited variations and uniform thickness, and suitable for internal electrodes for laminate ceramic capacitors of high electric capacity. The process comprises a step for forming a nickel compound coated with gelatin by adsorbing gelatin on preformed nickel compound particles with different size and shape (Step (A)), and another step for converting said nickel compound coated with gelatin into fine particles containing metallic nickel and nickel oxide by heating the nickel compound coated with gelatin produced in Step (A) in an inert gas atmosphere (Step (B)). It may include an additional step (Step (C)), subsequent to Step (B), for completely reducing nickel oxide in said fine particles by heating at temperature lower than that for Step (B) in a reducing gas atmosphere.
    • 制造能够在低温下金属化粉末以防止其烧结的细镍粉的有效方法,以及由具有平坦形状,有限变化直径和均匀厚度的颗粒形成的由该方法生产的细镍粉,并且适用于 用于层压陶瓷电容器的高电容的内部电极。 该方法包括通过将明胶吸附到具有不同尺寸和形状的预形成的镍化合物颗粒上形成涂有明胶的镍化合物的步骤(步骤(A)),以及将用明胶涂布的镍化合物转化为含有金属镍的细颗粒的另一步骤 和氧化镍,通过在惰性气体气氛中加热在步骤(A)中制备的用明胶制备的镍化合物(步骤(B))。 在步骤(B)之后,还可以包括在还原气体气氛中通过在低于步骤(B)的温度下进行加热来完全还原所述细颗粒中的氧化镍的附加步骤(步骤(C))。
    • 5. 发明授权
    • Fine nickel powder and process for producing the same
    • 细镍粉及其制造方法
    • US07604679B2
    • 2009-10-20
    • US11266495
    • 2005-11-04
    • Yasumasa HattoriEgon Matijevic
    • Yasumasa HattoriEgon Matijevic
    • B22F1/00B22F9/00C21B15/04C22B5/20C22C1/04B22F1/02C22C1/05
    • B22F9/22B22F1/0018B22F2001/0033B22F2998/00B82Y30/00B22F1/0055B22F2201/013B22F2201/02
    • An efficient process for producing fine nickel powder, capable of metallizing the powder at low temperature to prevent its sintering, and fine nickel powder produced by the process, composed of particles having a flat shape, diameter of limited variations and uniform thickness, and suitable for internal electrodes for laminate ceramic capacitors of high electric capacity. The process comprises a step for forming a nickel compound coated with gelatin by adsorbing gelatin on preformed nickel compound particles with different size and shape (Step (A)), and another step for converting said nickel compound coated with gelatin into fine particles containing metallic nickel and nickel oxide by heating the nickel compound coated with gelatin produced in Step (A) in an inert gas atmosphere (Step (B)). It may include an additional step (Step (C)), subsequent to Step (B), for completely reducing nickel oxide in said fine particles by heating at temperature lower than that for Step (B) in a reducing gas atmosphere.
    • 制造能够在低温下金属化粉末以防止其烧结的细镍粉的有效方法,以及由具有平坦形状,有限变化直径和均匀厚度的颗粒形成的由该方法生产的细镍粉,并且适用于 用于层压陶瓷电容器的高电容的内部电极。 该方法包括通过将明胶吸附到具有不同尺寸和形状的预形成的镍化合物颗粒上形成涂有明胶的镍化合物的步骤(步骤(A)),以及将用明胶涂布的镍化合物转化为含有金属镍的细颗粒的另一步骤 和氧化镍,通过在惰性气体气氛中加热在步骤(A)中制备的用明胶制备的镍化合物(步骤(B))。 在步骤(B)之后,还可以包括在还原气体气氛中通过在低于步骤(B)的温度下进行加热来完全还原所述细颗粒中的氧化镍的附加步骤(步骤(C))。