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1. 发明公开

EP1124857A1 VERFAHREN ZUR HERSTELLUNG VON DEFINIERTEN SCHICHTEN ODER SCHICHTSYSTEMEN 有权
标题翻译：用于生产定义的层或者层系统
公开(公告)号：EP1124857A1
公开(公告)日：2001-08-22
申请号：EP99945985.2
申请日：1999-08-17
申请人： Böttcher, Henrik , Hallensleben, Manfred Ludwig, Prof.Dr.rer.nat. , Wurm, Hellmuth
发明人： Böttcher, Henrik , Hallensleben, Manfred Ludwig, Prof.Dr.rer.nat. , Wurm, Hellmuth
IPC分类号： C08F4/00 , C08F292/00 , C08F4/40
CPC分类号： C08F2/00 , Y10T428/2987 , Y10T428/2998 , Y10T428/31504 , Y10T428/31536 , Y10T428/31786 , Y10T428/31794 , Y10T428/31797 , Y10T428/31841 , Y10T428/31855 , Y10T428/31909
摘要： The invention relates to a method for producing defined layers or layer systems made of polymers or oligomers on any solid surface and with a controlled structure, according to which the layers are chemically deposited on the solid surface by means of live/controlled free-radical polymerization. Said method comprises the following steps: a) bonding the compounds of the general formula (1) A-L-I to the solid surface via the active group A, where A represents an active group, I is the initiating group for ATRP polymerization and L is the binding link between A and I; b) carrying out live/controlled free-radical polymerization by reacting the initiator group I with monomers, macromonomers or mixtures able to undergo free-radical polymerization, which produces the polymer layer on the solid surface. The invention also relates to solid surfaces with oligomer or polymer layers and initiators for carrying out the method.

2. 发明授权

EP1124857B1 VERFAHREN ZUR HERSTELLUNG VON DEFINIERTEN SCHICHTEN ODER SCHICHTSYSTEMEN 有权
标题翻译：用于生产定义的层或者层系统
公开(公告)号：EP1124857B1
公开(公告)日：2003-04-09
申请号：EP99945985.2
申请日：1999-08-17
申请人： Böttcher, Henrik , Hallensleben, Manfred Ludwig, Prof.Dr.rer.nat. , Wurm, Hellmuth
发明人： Böttcher, Henrik , Hallensleben, Manfred Ludwig, Prof.Dr.rer.nat. , Wurm, Hellmuth
IPC分类号： C08F4/00 , C08F292/00 , C08F4/40
CPC分类号： C08F2/00 , Y10T428/2987 , Y10T428/2998 , Y10T428/31504 , Y10T428/31536 , Y10T428/31786 , Y10T428/31794 , Y10T428/31797 , Y10T428/31841 , Y10T428/31855 , Y10T428/31909

3. 发明专利

CA2341387C METHOD FOR PRODUCING DEFINED LAYERS OR LAYER SYSTEMS 未知
公开(公告)号：CA2341387C
公开(公告)日：2007-04-17
申请号：CA2341387
申请日：1999-08-17
申请人： WURM HELLMUTH , BOTTCHER HENRIK , HALLENSLEBEN MANFRED L
发明人： WURM HELLMUTH , BOTTCHER HENRIK , HALLENSLEBEN MANFRED L
IPC分类号： C08F4/00 , B05D7/26 , B32B9/04 , C08F2/00 , C08F2/38 , C08F4/06 , C08F4/40 , C08F292/00
摘要： The invention relates to a method for producing defined layers or layer systems made of polymers or oligomers on any solid surface and with a controlled structure, according to which the layers are chemically deposited on the solid surface by means of live/controlled free-radical polymerization. Said method comprises the following steps: a)bonding the compounds of the general formula (a) A-L-I to the solid surfac e via the active group A, where A represents an active group, I is the initiating grou p for ATRP polymerization and L is the binding link between A and I; b) carrying out live/controlled free-radical polymerization by reacting the initiator group I with monomers, macromonomers or mixtures able to andergo free- radical polymerization, whic h produces the polymer layer on the solid surface. The invention also relates to solid surfaces with oligomer or polymer layers and initiators for carrying out the method.

4. 发明专利

DE19981629D2 未知
公开(公告)号：DE19981629D2
公开(公告)日：2002-01-24
申请号：DE19981629
申请日：1999-08-17
申请人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG , WURM HELLMUTH
发明人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG , WURM HELLMUTH
IPC分类号： B05D7/26 , B32B9/04 , C08F2/00 , C08F4/00 , C08F4/06 , C08F4/40 , C08F292/00

5. 发明专利

DE10052646A1 Production of functional polymers, e.g. for modification of products such as dyes and polymer additives, involves living polymerisation or post-polymerisation modification using species with specific functional properties 未知
公开(公告)号：DE10052646A1
公开(公告)日：2002-05-16
申请号：DE10052646
申请日：2000-10-24
申请人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG , WURM HELLMUTH
IPC分类号： C08F2/00 , C08F8/00 , C08F293/00 , C08F290/00
摘要： Functional polymers or oligomers are produced as such (or as layer systems on solid surfaces) by living/controlled radical polymerisation of functional polymerizable species with other comonomers and/or by post-polymerisation modification of polymers with functional species obtained by living polymerisation.. A method for the production of functional polymers or oligomers by living/controlled radical polymerisation involves the following alternative stages or combinations of these: (a) living/controlled radical polymerisation of polymerizable species with certain specific functional properties which also appear in the resulting products which may be homopolymers, statistical copolymers, gradient copolymers, block copolymer or graft copolymers with conventional (co)monomers or macromonomers as used to make polymer materials or with (co)monomers or macromonomers which give the products additional specific functional properties and (b) modification of the polymer (without changing the degree of polymerisation) by attaching chemical species with specific functional properties at reactive centers in the polymer chain or at the chain ends, using oligomers or polymers (of the types as listed in a) obtained by living/controlled radical polymerisation (i.e. post-polymerisation modification), and also a similar method for the production of layers or layer systems of functional polymers or oligomers which are attached to any solid surface by main valency bonds using stages (c) and/or (d) corresponding to stages (a) and/or (b) above. Functional polymers in this context comprise polymers having chemical species with a specific functional property in the main chain, at the chain ends or as lateral groups. Specific functional properties are shown by chemically homo- or hetero-geneous species (functional materials), inorganic/organic hybrids and micro- or nano-particles which are used, e.g. as dyes, optical brighteners, pigments, piezoelectric materials, electrical conductors, semiconductors or insulators, antistatics, permeation modifiers, additives for improving material properties (hardness, wear resistance etc.), soil-repellent materials, radiopaque materials, light stabilisers, fire retardants, pharmaceutical vehicles etc. (50 applications listed). Independent claims are also included for (i) solid surfaces with layers of functional oligomer or polymer, obtained by the above method; (ii) materials produced by using functional oligomers or polymers (or layers/layer systems thereof), obtained by this method; (iii) polymer materials as described in (ii) above.

6. 发明专利

CA2341387A1 METHOD FOR PRODUCING DEFINED LAYERS OR LAYER SYSTEMS 未知
公开(公告)号：CA2341387A1
公开(公告)日：2000-03-02
申请号：CA2341387
申请日：1999-08-17
申请人： HALLENSLEBEN MANFRED L , BOTTCHER HENRIK , WURM HELLMUTH
发明人： HALLENSLEBEN MANFRED L , BOTTCHER HENRIK , WURM HELLMUTH
IPC分类号： B05D7/26 , B32B9/04 , C08F2/00 , C08F4/00 , C08F4/06 , C08F4/40 , C08F292/00
摘要： The invention relates to a method for producing defined layers or layer systems made of polymers or oligomers on any solid surface and with a controlled structure, according to which the layers are chemically deposited on the solid surface by means of live/controlled free-radical polymerization . Said method comprises the following steps: a) bonding the compounds of the general formula (1) A-L-I to the solid surface via the active group A, where A represents an active group, I is the initiating group for ATRP polymerizatio n and L is the binding link between A and I; b) carrying out live/controlled free-radical polymerization by reacting the initiator group I with monomers, macromonomers or mixtures able to undergo free-radical polymerization, which produces the polymer layer on the solid surface. The invention also relates to solid surfaces with oligomer or polymer layers and initiators for carrying o ut the method.

7. 发明专利

ES2195610T3 未知
公开(公告)号：ES2195610T3
公开(公告)日：2003-12-01
申请号：ES99945985
申请日：1999-08-17
申请人： BOTTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG PR , WURM HELLMUTH DR RER NAT
发明人： BOTTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG PR , WURM HELLMUTH DR RER NAT
IPC分类号： B05D7/26 , B32B9/04 , C08F2/00 , C08F4/00 , C08F4/06 , C08F4/40 , C08F292/00

8. 发明专利

AT236936T 未知
公开(公告)号：AT236936T
公开(公告)日：2003-04-15
申请号：AT99945985
申请日：1999-08-17
申请人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG PR , WURM HELLMUTH
发明人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG PR , WURM HELLMUTH
IPC分类号： B05D7/26 , B32B9/04 , C08F2/00 , C08F4/00 , C08F4/06 , C08F4/40 , C08F292/00

9. 发明专利

DE19838241A1 Modification of solid surfaces, useful for the control of adhesion and surface reactivity comprises a living/controlled radical polymerization initiated by compounds bound to the solid surface. 未知
公开(公告)号：DE19838241A1
公开(公告)日：2000-02-24
申请号：DE19838241
申请日：1998-08-22
申请人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG , WURM HELLMUTH
发明人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG , WURM HELLMUTH
IPC分类号： B05D7/26 , B32B9/04 , C08F2/00 , C08F4/00 , C08F4/06 , C08F4/40 , C08F292/00
摘要： Process for the modification of solid surfaces comprises a living/controlled radical polymerization initiated by compounds bound to the solid surface. A process for performing a living/controlled radical polymerization comprises controlled growth of defined oligomeric or polymeric layers or layer systems on the surfaces of a solid body which are chemically bonded to the surface whereby: (A) functional groups of primary valence are bound to the surface of the solid body to initiate polymerization; (B) carrying out a living/controlled radical polymerization of monomers and/or macromonomers in a second step; (C) further living/controlled radical polymerization to form a second and/or further polymer layers of different monomers and/or macromonomer species; (D) modification of the polymer layers following steps (B) or (C) by means of appropriate reactants to chemically convert oligomeric and/or polymeric functional groups with retention of the degree of polymerization; and (E) the resulting solid-polymer layer system may be bound into a three dimensional polymer matrix by cross-linking reactions.

10. 发明专利

DE59904996D1 未知
公开(公告)号：DE59904996D1
公开(公告)日：2003-05-15
申请号：DE59904996
申请日：1999-08-17
申请人： BOETTCHER HENRIK , HALLENSLEBEN MANFRED LUDWIG , WURM HELLMUTH
发明人： BOETTCHER HENRIK , HALLENSLEBEN PROF DR RER NAT , WURM HELLMUTH
IPC分类号： B05D7/26 , B32B9/04 , C08F2/00 , C08F4/00 , C08F4/06 , C08F4/40 , C08F292/00

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