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    • 3. 发明授权
    • Inlet distributor for fixed bed catalytic reactor
    • 固定床催化反应器入口分配器
    • US4788040A
    • 1988-11-29
    • US883848
    • 1986-07-10
    • Joseph F. CampagnoloTai-Sheng ChouWilliam F. HeaneyJohn D. Ruggles
    • Joseph F. CampagnoloTai-Sheng ChouWilliam F. HeaneyJohn D. Ruggles
    • B01J8/02C10G49/00B01D47/00B01J8/04
    • C10G49/002B01J8/0278
    • An inlet distributor system for a fixed bed catalyst reactor which includes an inlet deflector cone positioned to deflect liquid in cooperation with a splash plate onto a liquid distributor trough positioned therebelow. An upper tray is positioned beneath the distributor trough to receive liquid therefrom. The upper distributor tray has a series of risers in spaced position thereon and extending above and below the upper distributor tray. The risers are hollow and open above and below the upper distributor tray to permit vapor to pass through the tray and each riser has a plurality of weir slots cut into its outer surface through which liquid can pass through the tray. A lower distributor tray is positioned beneath the upper distributor tray to receive liquid passing through the weir slots of the risers. The lower distributor tray has a series of risers and downpipes thereon arranged in a predetermined pattern. Each of the risers and downpipes in said pattern extend above and below the lower distributor tray and have openings above and below the lower distributor tray to form a through passageway for liquid to pass through the tray when received from the upper distributor tray. The passageway in the downpipes is formed by an axial bore therethrough and the passageway in the risers is formed by its hollow tubular configuration open at the bottom and having a side opening therein above the upper surface of the lower distributor tray each riser includes another upper opening above the lower distributor tray to permit vapor to pass through the tray. The pattern of risers and downpipes provide an advantageous arrangement of passageways for liquid to be distributed to the catalytic bed therebelow.
    • 一种用于固定床催化剂反应器的入口分配器系统,其包括入口偏转器锥体,其定位成将与溅射板协作的液体偏转到位于其下方的液体分配器槽。 上托盘位于分配器槽下方以从其接收液体。 上部分配器托盘具有一系列在隔板位置上的提升器,并且在上部分配器托盘的上方和下方延伸。 上升管是中空的,并且在上部分配器托盘的上方和下方敞开,以允许蒸汽通过托盘,并且每个提升管具有切割到其外表面中的多个堰槽,液体可以通过该外部表面通过托盘。 下部分配器托盘位于上部分配器托盘下方以接收通过提升管的堰槽的液体。 下分配器托盘在其上以预定图案布置有一系列立管和落管。 所述图案中的每个立管和下水管都在下部分配器托盘的上方和下方延伸,并且在下部分配器托盘的上方和下方具有开口,以形成通道,用于在从上部分配器托盘接收时液体通过托盘。 下水管中的通道由穿过其中的轴向孔形成,并且提升管中的通道由其在底部开放的中空管状构造形成,并且在下分配器托盘的上表面上方具有侧开口,每个立管包括另一上部开口 在下分配器托盘上方,以允许蒸汽通过托盘。 提升管和水管的图案提供了用于液体分配到其下方的催化床的通道的有利布置。
    • 4. 发明授权
    • Lubricating oil dewaxing using membrane separation of cold solvent from
dewaxed oil and recycle of cold solvent to filter feed
    • 润滑油脱蜡使用冷脱溶剂与脱蜡油进行膜分离,并将冷溶剂再循环至过滤进料
    • US5360530A
    • 1994-11-01
    • US52327
    • 1993-04-23
    • Ronald M. GouldWilliam F. HeaneyAlbert R. NitschHoward E. Spencer
    • Ronald M. GouldWilliam F. HeaneyAlbert R. NitschHoward E. Spencer
    • C10G73/04C10G73/06C10G73/32B01D39/00C07C7/144
    • C10G73/06
    • A process for solvent dewaxing a waxy oil feed to obtain petroleum oil lubricating stock comprising the steps of contacting a warm waxy oil feed by indirect heat exchange first with cold filtrate, then with refrigerant to crystallize and precipitate the wax in the oil feed to form an oil/solvent/wax mixture. The oil/solvent/wax mixture is diluted with cold solvent to adjust the viscosity of the mixture and the mixture is fed to a filter which filters and removes the wax from the cold oil/solvent/wax mixture. A cold wax cake is recovered and a cold oil/solvent filtrate stream is recovered. The cold oil/solvent filtrate stream is fed, at the filtration temperature, to a selective permeable membrane. The membrane selectively separates the cold filtrate into a cold solvent permeate stream and a cold filtrate stream which contains the dewaxed oil and the remaining solvent. The cold solvent permeate stream at the filtration temperature is recycled to the filter feed stream. The cold filtrate stream is then contacted with the warm waxy oil feed by indirect heat exchange. After heat exchange with the warm waxy oil feed, the filtrate is sent to an oil/solvent separation operation in which the remaining solvent is removed from the dewaxed oil and recycled to the dewaxing process and the wax free lubricating oil stock product is recovered.
    • 一种用于对蜡状油进料进行溶剂脱蜡以获得石油润滑油料的方法,包括以下步骤:首先通过间接热交换将冷的蜡状油进料与冷滤液接触,然后用制冷剂使蜡在油进料中结晶和沉淀,形成 油/溶剂/蜡混合物。 用冷溶剂稀释油/溶剂/蜡混合物以调节混合物的粘度,并将混合物进料到过滤器中,该过滤器从冷油/溶剂/蜡混合物中过滤和除去蜡。 回收冷蜡饼,回收冷油/溶剂滤液流。 将冷的油/溶剂滤液流在过滤温度下进料至选择性渗透膜。 膜将冷滤液选择性地分离成冷溶剂渗透物流和含有脱蜡油和剩余溶剂的冷滤液流。 将过滤温度下的冷溶剂渗透物流再循环至过滤器进料流。 然后通过间接热交换将冷的滤液流与温暖的蜡状油进料接触。 与暖蜡进料进行热交换后,将滤液送至油/溶剂分离操作,其中将剩余的溶剂从脱蜡油中除去并再循环至脱蜡过程,并回收无蜡的润滑油原料。