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1. 发明授权

US5115066A Polystyrene having high degree of expandability, and formulation having a highly-expandable polymer therein 失效
标题翻译：具有高扩展性的聚苯乙烯和其中具有高度可膨胀聚合物的制剂
公开(公告)号：US5115066A
公开(公告)日：1992-05-19
申请号：US777869
申请日：1991-10-15
申请人： Eugene K. Zimmermann , Bernhard Wagner , William E. Volz , William H. Harclerode , John V. Wiman , John C. Voss
发明人： Eugene K. Zimmermann , Bernhard Wagner , William E. Volz , William H. Harclerode , John V. Wiman , John C. Voss
IPC分类号： C08J9/06 , C08J9/12 , C08J9/14 , C08J9/16
CPC分类号： C08J9/16 , C08J9/06 , C08J9/12 , C08J9/141 , C08J2325/06 , Y10S264/07 , Y10S264/09 , Y10S264/10 , Y10S264/15
摘要： A polystyrene polymer as well as an expandable polystyrene formulation comprises a polystyrene polymer having a particular molecular weight distribution. The polymer itself exhibits a polydispersity of from about 1 to less tha 2.0, a weight average molecular weight of greater than about 200,000 to about 300,000, and an M.sub.z :M.sub.n of from about 2 to less than about 3.0. Furthermore, the polystyrene polymer is branched to from 0 to less than 5 weight percent.The expandable polystyrene formulation comprises a polystyrene polymer exhibiting a polydispersity of from about 1.0 to less than 2.5, a weight average molecular weight of from greater than about 180,000 to about 300,000, an M.sub.z :M.sub.n of from about 2 to about 4.5. The polystyrene polymer is present in an amount of from about 94.5 weight percent to about 98 weight percent, based on the total weight of the formulation, and the polystyrene polymer is branched to from 0 to less than 5 weight percent. The formulation further comprises a blowing agent, wherein the blowing agent is present in an amount of from about 2 weight percent to less than 5.5 weight percent, wherein the blowing agent is a hydrocarbon which is gaseous or liquid at standard temperature and pressure, does not dissolve the styrene polymer, and boils below the softening point of the polymer.
摘要翻译：聚苯乙烯聚合物以及可发性聚苯乙烯制剂包含具有特定分子量分布的聚苯乙烯聚合物。聚合物本身表现出多分散性为约1至小于2.0，重均分子量大于约200,000至约300,000，Mz：Mn为约2至小于约3.0。此外，聚苯乙烯聚合物分支至0至小于5重量％。可发性聚苯乙烯制剂包含显示约1.0至小于2.5的多分散性，大于约180,000至约300,000的重均分子量，约2至约4.5的Mz：Mn的聚苯乙烯聚合物。基于制剂的总重量，聚苯乙烯聚合物的存在量为约94.5重量％至约98重量％，并且聚苯乙烯聚合物分支至0至小于5重量％。制剂还包含发泡剂，其中发泡剂的存在量为约2重量％至小于5.5重量％，其中发泡剂是在标准温度和压力下为气态或液体的烃，不是溶解苯乙烯聚合物，并且沸点低于聚合物的软化点。

2. 发明授权

US5112875A Polystyrene having high degree of expandability, and formulation having a highly-expandable polymer therein 失效
标题翻译：具有高扩展性的聚苯乙烯和其中具有高度可膨胀聚合物的制剂
公开(公告)号：US5112875A
公开(公告)日：1992-05-12
申请号：US617711
申请日：1990-11-26
申请人： Eugene K. Zimmermann , Bernhard Wagner , William E. Volz , William H. Harclerode , John V. Wiman , John C. Voss
发明人： Eugene K. Zimmermann , Bernhard Wagner , William E. Volz , William H. Harclerode , John V. Wiman , John C. Voss
IPC分类号： C08J9/06 , C08J9/12 , C08J9/14 , C08J9/16 , C08K5/00 , C08K5/01 , C08L25/06
CPC分类号： C08J9/16 , C08J9/06 , C08J9/12 , C08J9/141 , C08J2325/06 , Y10S264/09 , Y10S521/907
摘要： A polystyrene polymer as well as an expandable polystyrene formulation comprises a polystyrene polymer having a particular molecular weight distribution. The polymer itself exhibits a polydispersity of from about 1 to less than 2.0, a weight average molecular weight of greater than about 200,000 to about 300,000, and an M.sub.z :M.sub.n of from about 2 to less than about 3.0. Furthermore, the polystyrene polymer is branched to from 0 to less than 5 weight percent.The expandable polystyrene formulation comprises a polystyrene polymer exhibiting a polydispersity of from about 1.0 to less than 2.5, a weight average molecular weight of from greater than about 180,000 to about 300,000, an M.sub.z :M.sub.n of from about 2 to about 4.5. The polystyrene polymer is present in an amount of from about 94.5 weight percent to about 98 weight percent, based on the total weight of the formulation, and the polystyrene polymer is branched to from 0 to less than 5 weight percent. The formulation further comprises a blowing agent, wherein the blowing agent is present in an amount of from about 2 weight percent to less than 5.5 weight percent, wherein the blowing agent is a hydrocarbon which is gaseous or liquid at standard temperature and pressure, does not dissolve the styrene polymer, and boils below the softening point of the polymer.
摘要翻译：聚苯乙烯聚合物以及可发性聚苯乙烯制剂包含具有特定分子量分布的聚苯乙烯聚合物。聚合物本身表现出约1至小于2.0的多分散性，重均分子量大于约200,000至约300,000，Mz：Mn为约2至小于约3.0。此外，聚苯乙烯聚合物分支至0至小于5重量％。可发性聚苯乙烯制剂包含显示约1.0至小于2.5的多分散性，大于约180,000至约300,000的重均分子量，约2至约4.5的Mz：Mn的聚苯乙烯聚合物。基于制剂的总重量，聚苯乙烯聚合物的存在量为约94.5重量％至约98重量％，并且聚苯乙烯聚合物分支至0至小于5重量％。制剂还包含发泡剂，其中发泡剂的存在量为约2重量％至小于5.5重量％，其中发泡剂是在标准温度和压力下为气态或液体的烃，不是溶解苯乙烯聚合物，并且沸点低于聚合物的软化点。

3. 发明授权

US4465638A Process for using sediments developed during storage of pure MDI 失效
标题翻译：在纯MDI储存过程中开发沉淀物的工艺
公开(公告)号：US4465638A
公开(公告)日：1984-08-14
申请号：US459463
申请日：1983-01-20
申请人： Peter T. Kan , Robert L. Schaaf , Lewis N. Medaugh , William E. Volz
发明人： Peter T. Kan , Robert L. Schaaf , Lewis N. Medaugh , William E. Volz
IPC分类号： C07C265/12 , C07D229/00 , C08G18/76 , C07C119/048
CPC分类号： C07C265/12 , C07D229/00 , C08G18/7671
摘要： This invention relates to a process for utilizing the sediments in pure MDI which comprises(a) heating the sediments at temperatures of 180.degree. C. to 250.degree. C. for 0.25 hour to 6 hours in the presence of crude MDI; and(b) cooling the product to a temperature of 60.degree. C. or less within 5 minutes.The sediment-free crude MDI which results can then be used for the preparation of polyurethane products.
摘要翻译：本发明涉及一种在纯MDI中利用沉淀物的方法，其包括（a）在粗MDI存在下，在180℃至250℃的温度下加热沉淀物0.25小时至6小时; 和（b）在5分钟内将产品冷却至60℃或更低的温度。得到的无沉淀的粗MDI可用于制备聚氨酯产品。

4. 发明授权

US5110837A Process for making molded polymeric product with multipass expansion of polymer bead with low blowing agent content 失效
标题翻译：用于制备具有低发泡剂含量的聚合物珠的多次膨胀的模制聚合物产品的方法
公开(公告)号：US5110837A
公开(公告)日：1992-05-05
申请号：US618359
申请日：1990-11-26
申请人： William H. Harclerode , William E. Volz , John V. Wiman , John C. Voss , Barry J. Pekich , John C. Knutsen
发明人： William H. Harclerode , William E. Volz , John V. Wiman , John C. Voss , Barry J. Pekich , John C. Knutsen
IPC分类号： C08J9/228
CPC分类号： C08J9/228 , C08J2325/06 , Y10S264/07 , Y10S264/09 , Y10S264/10 , Y10S264/15
摘要： A method for making low density (0.8-1.1 lb/cu.ft.) expanded polymeric products uses blowing agent in an amount of only from 2 to 4.4 weight percent. The process uses 2 to 5 expansion steps together with a polymer having a particular polydispersity, weight average molecular weight and M.sub.z :M.sub.n, this polymer having a greater expandability than conventional polymers. The process requires only about half of the amount of blowing agent currently being used in commercially viable processes for making expanded polystyrene products. The process can be used with or without a molding step.
摘要翻译：制造低密度（0.8-1.1磅/立方英尺）膨胀聚合物的方法使用的发泡剂的用量仅为2至4.4重量％。该方法与具有特定多分散性，重均分子量和Mz：Mn的聚合物一起使用2至5个膨胀步骤，该聚合物具有比常规聚合物更大的膨胀性。该方法仅需要用于制造发泡聚苯乙烯产品的商业上可行的方法中的一半量的发泡剂。该方法可以在成型步骤中或不使用成型步骤的情况下使用。

5. 发明授权

US06849665B2 Absorbent compositions 有权
标题翻译：吸收剂组合物
公开(公告)号：US06849665B2
公开(公告)日：2005-02-01
申请号：US10028908
申请日：2001-12-28
申请人： Volker Frenz , Norbert Herfert , Ulrich Riegel , William E. Volz , Thomas H. Majette , James Hill
发明人： Volker Frenz , Norbert Herfert , Ulrich Riegel , William E. Volz , Thomas H. Majette , James Hill
IPC分类号： A61F13/53 , A61F13/00 , A61F13/15 , A61F13/49 , A61L15/60 , B01J20/26 , C08L101/14 , C08J9/28
CPC分类号： A61L15/60 , B01J20/26 , Y10T428/249953 , Y10T428/2991 , Y10T428/2998 , Y10T428/31971 , Y10T428/31975 , Y10T428/31978
摘要： Described is a water-absorbent composition containing from 30 to 100% by weight, based on the water-absorbent composition, of water-insoluble water-swellable hydrogels characterized by the following features: Centrifuge Retention Capacity (CRC) of at least 24 g/g, Saline Flow Conductivity (SFC) of at least 80×10−7 cm3 s/g and Free Swell Rate (FSR) of at least 0.15 g/g s and/or Vortex Time of not more than 160 s.
摘要翻译：描述了基于吸水性组合物含有30-100重量％的水不溶性水溶胀性水凝胶的吸水性组合物，其特征在于以下特征：离心保留容量（CRC）为至少24g / g，至少80×10 -7 cm 3 / s的盐水流动电导率（SFC）和至少0.15g / gs和/或不超过160s的涡旋时间的无膨胀速率（FSR）。

6. 发明授权

US5110524A Process for making molded polymeric product with multipass expansion of polymer bead with low blowing agent content 失效
标题翻译：用于制备具有低发泡剂含量的聚合物珠的多次膨胀的模制聚合物产品的方法
公开(公告)号：US5110524A
公开(公告)日：1992-05-05
申请号：US776956
申请日：1991-10-15
申请人： William H. Harclerode , William E. Volz , John V. Wiman , John C. Voss , Barry J. Pekich , John C. Knutsen
发明人： William H. Harclerode , William E. Volz , John V. Wiman , John C. Voss , Barry J. Pekich , John C. Knutsen
IPC分类号： C08J9/228
CPC分类号： C08J9/228 , C08J2325/06 , Y10S264/07 , Y10S264/09 , Y10S264/10 , Y10S264/15
摘要： A method for making low density (0.8-1.1 lb/cu. ft.) expanded polymeric products uses blowing agent in an amount of only from 2 to 4.4 weight percent. The process uses 2 to 5 expansion steps together with a polymer having a particular polydispersity, weight average molecular weight and M.sub.z :M.sub.n, this polymer having a greater expandability than conventional polymers. The process requires only about half of the amount of blowing agent currently being used in commercially viable processes for making expanded polystyrene products. The process can be used with or without a molding step.
摘要翻译：制造低密度（0.8-1.1磅/立方英尺）膨胀聚合物的方法使用的发泡剂的量仅为2至4.4重量％。该方法与具有特定多分散性，重均分子量和Mz：Mn的聚合物一起使用2至5个膨胀步骤，该聚合物具有比常规聚合物更大的膨胀性。该方法仅需要用于制造发泡聚苯乙烯产品的商业上可行的方法中的一半量的发泡剂。该方法可以在成型步骤中或不使用成型步骤的情况下使用。

7. 发明授权

US4384052A Polyurethanes produced from an adduct of an organic polyisocyanate and certain amines 失效
标题翻译：由有机多异氰酸酯和某些胺的加合物生产的聚氨酯
公开(公告)号：US4384052A
公开(公告)日：1983-05-17
申请号：US271807
申请日：1981-06-08
申请人： Robert L. McBrayer , John G. Demou , Peter T. Kan , William E. Volz
发明人： Robert L. McBrayer , John G. Demou , Peter T. Kan , William E. Volz
IPC分类号： C08G18/80 , C08G18/14 , C08G18/77
CPC分类号： C08G18/8038 , Y10S521/904
摘要： Reaction products of an organic polyisocyanate with a reactive diamine such as bis(4-aminocyclohexyl)methane and isophorone diamine, prepared at a temperature of between 135.degree. C. and 200.degree. C., are used to prepare polyurethanes useful for comfort cushioning applications such as automotive seating, furniture, mattresses, and large automotive body panels.
摘要翻译：使用有机多异氰酸酯与反应性二胺如双（4-氨基环己基）甲烷和异佛尔酮二胺的反应产物，其温度为135℃至200℃，制备用于舒适缓冲应用的聚氨酯，作为汽车座椅，家具，床垫和大型汽车车身面板。

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