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    • 3. 发明授权
    • Fractionation of multicomponent dimethylnaphthelenes feeds by selective
crystallization
    • 通过选择性结晶分馏多组分二甲基萘并饲料
    • US3996031A
    • 1976-12-07
    • US495752
    • 1974-08-08
    • Victor M. Chong
    • Victor M. Chong
    • B01D9/00B01D9/02C07C7/14
    • B01D9/0013
    • A process and system for separating a preferentially crystallizable component A from a feed, wherein a series of zones are used between which mother liquor can flow without passage of crystallized material. Liquid feed is introduced to a zone other than the end zone from which effluent rich in component A is withdrawn. During one stage gradating crystallization temperature pattern is established throughout the series ranging from relatively low to relatively high, causing component A to crystallize in each zone; and mother liquor is caused to flow toward the low temperature end, while a portion of previously withdrawn effluent rich in component A is returned to the higher temperature end and effluent lean in component A is removed from the lower temperature end. In another stage a higher temperature pattern is established throughout the series whereby at least a portion of crystallized material melts in each zone, and mother liquor is caused to flow in the opposite direction while an equivalent amount of effluent rich in component A is withdrawn from said end zone.
    • 一种用于将优先结晶的组分A与进料分离的方法和系统,其中使用一系列区域,母液可以在其间流动而不通过结晶材料。 将液体进料引入除了从其中排出富含组分A的流出物的末端区域以外的区域。 在一个阶段中,渐变结晶温度模式在整个系列范围内从相对较低到相对较高,使组分A在每个区域中结晶; 使母液流向低温端,而富含组分A的一部分先前取出的流出物返回到较高温度的末端,并且从低温端除去组分A中的贫的流出物。 在另一个阶段,在整个系列中建立了更高的温度模式,其中至少一部分结晶的材料在每个区域中熔化,并使母液沿相反的方向流动,同时将等量的富含组分A的流出物从所述 结束区域。