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1. 发明授权

US06982308B2 PTFE-based formulation for the insulation of integrated circuits 失效
标题翻译：用于集成电路绝缘的PTFE基配方
公开(公告)号：US06982308B2
公开(公告)日：2006-01-03
申请号：US10970009
申请日：2004-10-22
申请人： Valery Kapeliouchko , Enrico Marchese , Tatiana Temtchenko
发明人： Valery Kapeliouchko , Enrico Marchese , Tatiana Temtchenko
IPC分类号： C08F214/26
CPC分类号： C08J3/03 , C08J2327/18 , C08K5/03 , C08K5/04 , C08K5/098 , H01B3/445 , C08L27/18
摘要： A formulation based on the PTFE, homopolymer or modified, comprising: 1) latex of said PTFE having a particle diameter between 5 and 100 nm, comprising an anionic fluorinated surfactant in an amount in the range 2–25% by weight based on the PTFE; 2) a non ionic fluorinated surfactant added to the PTFE latex in an amount in the range 18–60% by weight based on the PTFE.
摘要翻译：基于PTFE，均聚物或改性的制剂，其包含：1）具有5至100nm粒径的所述PTFE的胶乳，其包含基于PTFE的2-25重量％范围内的量的阴离子氟化表面活性剂 ; 2）添加到PTFE胶乳中的非离子氟化表面活性剂，其量为基于PTFE的18-60重量％。

2. 发明申请

US20050261454A1 PTFE-BASED FORMULATION FOR THE INSULATION OF INTEGRATED CIRCUITS 失效
标题翻译：用于绝缘电路绝缘的PTFE基配方
公开(公告)号：US20050261454A1
公开(公告)日：2005-11-24
申请号：US10970009
申请日：2004-10-22
申请人： Valery Kapeliouchko , Enrico Marchese , Tatiana Temtchenko
发明人： Valery Kapeliouchko , Enrico Marchese , Tatiana Temtchenko
IPC分类号： C08L27/18 , C08F214/26 , C08J3/03 , C08K5/03 , C08K5/04 , C08K5/06 , C08K5/09 , C08K5/098 , C08K5/42 , C08L71/02 , H01B3/44 , C08F214/18
CPC分类号： C08J3/03 , C08J2327/18 , C08K5/03 , C08K5/04 , C08K5/098 , H01B3/445 , C08L27/18
摘要： A formulation based on the PTFE, homopolymer or modified, comprising: 1) latex of said PTFE having a particle diameter between 5 and 100 nm, comprising an anionic fluorinated surfactant in an amount in the range 2-25% by weight based on the PTFE; 2) non ionic fluorinated surfactant added to the PTFE latex in an amount in the range 18-60% by weight based on the PTFE.
摘要翻译：基于PTFE，均聚物或改性的制剂，其包含：1）具有5至100nm粒径的所述PTFE的胶乳，其包含基于PTFE的2-25重量％范围内的量的阴离子氟化表面活性剂 ; 2）加入到PTFE胶乳中的非离子氟化表面活性剂，其量为基于PTFE的18-60重量％。

3. 发明授权

US06479591B2 Fine powders of polytetrafluoroethylene 有权
标题翻译：聚四氟乙烯细粉
公开(公告)号：US06479591B2
公开(公告)日：2002-11-12
申请号：US09907821
申请日：2001-07-19
申请人： Valery Kapeliouchko , Enrico Marchese
发明人： Valery Kapeliouchko , Enrico Marchese
IPC分类号： C08L2712
CPC分类号： C08F259/08
摘要： Fine powders of modified PTFE having a “core-shell” structure; the fine powder being formed by: a “core” of tetrafluoroethylene (TFE) modified by one or more monomers selected from: a) dioxoles; b) one or more perfluorinated monomers which cyclize during the polymerization; a “shell” of TFE modified by perfluoropropene (PFP); the amount, referred to the total core+shell particle, of comonomers 1) in the “core” being in the range 0.01-0.06% by weight; the amount, referred to the total core+shell particle, of perfluoropropene 2) in the “shell” being in the range 0.002-0.06% by weight; the thermal instability index (TII) of the fine powder being equal to or lower than 5, determined according to ASTM D4895.
摘要翻译：具有“核 - 壳”结构的改性PTFE的细粉末; 该细粉末由以下一种或多种单体改性的四氟乙烯（TFE）的“芯”形成：a）二氧杂环戊烯; b）在聚合过程中环化的一种或多种全氟化单体;由TFE改性的TFE的“壳” 全氟丙烯（PFP）; “芯”中的共聚单体1）的总核心+壳粒子的量在0.01-0.06重量％的范围内; “壳”中的全氟丙烯2的总核+壳粒子的量，在0.002-0.06重量％范围内;细粉末的热不稳定指数（TII）等于或小于5 ，根据ASTM D4895测定。

4. 发明申请

US20050197426A1 PTFE-based polymers 审中-公开
标题翻译： PTFE基聚合物
公开(公告)号：US20050197426A1
公开(公告)日：2005-09-08
申请号：US10832246
申请日：2004-04-27
申请人： Giovanna Palamone , Valery Kapeliouchko , Michele Laus
发明人： Giovanna Palamone , Valery Kapeliouchko , Michele Laus
IPC分类号： C08L25/04 , C08F2/22 , C08F2/44 , C08F259/08 , C08L51/00 , C08L55/02 , C08L83/00
CPC分类号： C08L51/003 , C08F259/08 , C08L55/02 , Y10S525/902 , C08L2666/02
摘要： Compositions containing core-shell particles having a core polytetrafluoroethylene-based polymers (PTFE) and shell styrene-based polymers (PS), wherein the particles contain an amount by weight of PTFE from 3 to 50%, preferably from 5 to 30% by weight, wherein the core PTFE particles have an average diameter from 5 to 100 nm, preferably from 10 to 70 nm, the core-shell particles having an average diameter from 10 to 170 nm, preferably from 20 to 100 nm.
摘要翻译：含有核聚四氟乙烯基聚合物（PTFE）和壳苯乙烯基聚合物（PS）的核 - 壳颗粒的组合物，其中颗粒含有3至50重量％，优选5至30重量％其中，核心PTFE粒子的平均直径为5〜100nm，优选为10〜70nm，核 - 壳粒子的平均直径为10〜170nm，优选为20〜100nm。

5. 发明授权

US06790932B2 Process for obtaining non thermoprocessable fine powders of homopolymer or modified PTFE 失效
标题翻译：获得均聚物或改性PTFE的非热可加工细粉末的方法
公开(公告)号：US06790932B2
公开(公告)日：2004-09-14
申请号：US10202852
申请日：2002-07-26
申请人： Valery Kapeliouchko , Hua Wu , Giovanna Palamone
发明人： Valery Kapeliouchko , Hua Wu , Giovanna Palamone
IPC分类号： C08F21418
CPC分类号： C08J3/16 , C08J2327/18
摘要： A process for obtaining non thermoprocessable fine powders of homopolymer or modified PTFE, comprising the following steps: A) obtaining of the polymer latex under the gel form; B) washing of the polymer gel with acid aqueous solutions or neutral aqueous solutions; C) granulation of the gel washed by mechanical stirring, at a specific power in the range 1.5-10 kW/m3, until flotation of the PTFE fine powder, and separation of the floated fine powder; D) drying in an aerated oven of the floated fine powder at a drying temperature in the range 90° C.-160° C.
摘要翻译：获得均聚物或改性PTFE的非热可加工细粉末的方法，包括以下步骤：A）以凝胶形式获得聚合物胶乳; B）用酸性水溶液或中性水溶液洗涤聚合物凝胶; C）造粒通过机械搅拌洗涤的凝胶，以1.5-10kW / m 3的比功率，直至浮选PTFE细粉末，并分离漂浮的细粉; D）在充气烘箱中干燥在干燥温度为90°C-160°C时漂浮细粉

6. 发明授权

US06262209B1 Process for preparing modified PTFE 失效
标题翻译：改性PTFE的制备方法
公开(公告)号：US06262209B1
公开(公告)日：2001-07-17
申请号：US09235407
申请日：1999-01-22
申请人： Valery Kapeliouchko , Enrico Marchese
发明人： Valery Kapeliouchko , Enrico Marchese
IPC分类号： C08F21426
CPC分类号： C08F214/262
摘要： Method for preparing modified PTFE by suspension, wherein as comonomers perfluoroalkylvinylethers in which the alkyl has from 1 to 5 carbon atoms, and/or a perfluorodioxole are used, characterized by the following conditions: a part of the comonomer, from 15 to 90% by weight of the total amount is to be fed at the beginning of the reaction; the remaining part of the comonomer is to be distributed during the reaction so as to obtain a constant speed of the comonomer incorporation in the polymer chain; a perfluorinated surfactant and a buffering salt are used; a persulphate with a reducing agent is used as initiator in such a ratio as to generate a part of the radicals from the redox reaction and another one from the persulphate thermal decomposition; one operates with a polymerization pressure from 15 to 30 bar.
摘要翻译：通过悬浮液制备改性PTFE的方法，其中使用其中烷基具有1至5个碳原子的共聚单体全氟烷基乙烯基醚和/或全氟二恶烷，其特征在于以下条件：一部分共聚单体为15〜90％总量的重量在反应开始时进料; 共聚单体的剩余部分将在反应期间分布，以获得聚合物链中共聚单体引入的恒定速度;使用全氟化表面活性剂和缓冲盐;将具有还原剂的过硫酸盐用作引发剂这种比例从氧化还原反应产生一部分自由基，另一种来自过硫酸盐热分解;一种以15至30巴的聚合压力进行操作。

7. 发明授权

US06825304B2 PTFE-based formulation for the insulation of integrated circuits 失效
标题翻译：用于集成电路绝缘的PTFE基配方
公开(公告)号：US06825304B2
公开(公告)日：2004-11-30
申请号：US09931756
申请日：2001-08-20
申请人： Valery Kapeliouchko , Enrico Marchese , Tatiana Temtchenko
发明人： Valery Kapeliouchko , Enrico Marchese , Tatiana Temtchenko
IPC分类号： C08F21426
CPC分类号： C08J3/03 , C08J2327/18 , C08K5/03 , C08K5/04 , C08K5/098 , H01B3/445 , C08L27/18
摘要： A formulation based on the PTFE, homopolymer or modified, comprising: 1) latex of said PTFE having a particle diameter between 5 and 100 nm, comprising an anionic fluorinated surfactant in an amount in the range 2-25% by weight based on the PTFE; 2) non ionic fluorinated surfactant added to the PTFE latex in an amount in the range 18-60% by weight based on the PTFE.
摘要翻译：基于PTFE，均聚物或改性的制剂，其包含：1）具有5至100nm粒径的所述PTFE的胶乳，其包含基于PTFE的2-25重量％范围内的量的阴离子氟化表面活性剂 ; 2）添加到PTFE胶乳中的非离子氟化表面活性剂，其量为基于PTFE的18-60重量％。

8. 发明授权

US06780363B2 PTFE-based polymers 失效
标题翻译： PTFE基聚合物
公开(公告)号：US06780363B2
公开(公告)日：2004-08-24
申请号：US10097622
申请日：2002-03-15
申请人： Giovanna Palamone , Valery Kapeliouchko , Michele Laus
发明人： Giovanna Palamone , Valery Kapeliouchko , Michele Laus
IPC分类号： C08J500
CPC分类号： C08L51/003 , C08F259/08 , C08L55/02 , Y10S525/902 , C08L2666/02
摘要： Compositions containing core-shell particles having a core polytetrafluoroethylene-based polymers (PTFE) and shell styrene-based polymers (PS), wherein the particles contain an amount by weight of PTFE from 3 to 50%, preferably from 5 to 30% by weight, wherein the core PTFE particles have an average diameter from 5 to 100 nm, preferably from 10 to 70 nm, the core-shell particles having an average diameter from 10 to 170 nm, preferably from 20 to 100 nm.
摘要翻译：含有核心聚四氟乙烯基聚合物（PTFE）和壳苯乙烯基聚合物（PS）的核 - 壳颗粒的组合物，其中颗粒含有3至50重量％，优选5至30重量％其中，核心PTFE粒子的平均直径为5〜100nm，优选为10〜70nm，核 - 壳粒子的平均直径为10〜170nm，优选为20〜100nm。

9. 发明授权

US06576703B2 Process for the preparation of aqueous dispersions of fluoropolymers 失效
标题翻译：制备含氟聚合物水分散体的方法
公开(公告)号：US06576703B2
公开(公告)日：2003-06-10
申请号：US09789728
申请日：2001-02-22
申请人： Valery Kapeliouchko , Enrico Marchese
发明人： Valery Kapeliouchko , Enrico Marchese
IPC分类号： C08L2712
CPC分类号： C08F259/08 , C08F2/26 , C08F14/26 , C08F2/16
摘要： Process for the preparation of a dispersion based on homopolymers/copolymers of tetrafluoroethylene (TFE), said dispersion having a bimodal or multimodal distribution of the particle diameters, wherein the fraction of small particles is in the range 1.5-35% by weight calculated on the dry product; the ratio between the average diameter of the small particles with respect to the average diameter of the dispersion obtained from the polymerization being in the range 0.02-0.6; said process comprising the following essential steps: (a) preparation of an aqueous microemulsion comprising fluorinated surfactants and (per)fluoropolyether oils (PFPE); (b) feeding of the microemulsion into the polymerization reactor; (c) feeding of at least one fluorinated surfactant.
摘要翻译：用于制备基于四氟乙烯（TFE）的均聚物/共聚物的分散体的方法，所述分散体具有粒径的双峰或多峰分布，其中小颗粒的分数为1.5〜35重量％干燥产品; 小颗粒的平均直径相对于由聚合得到的分散体的平均直径的比在0.02-0.6的范围内; 所述方法包括以下必要步骤：（a）制备包含氟化表面活性剂和（全）氟聚醚油（PFPE）的水性微乳液;（b）将微乳液进料到聚合反应器中;（c）进料至少一种氟化表面活性剂。

10. 发明授权

US06297334B1 TFE polymerization process 有权
标题翻译： TFE聚合工艺
公开(公告)号：US06297334B1
公开(公告)日：2001-10-02
申请号：US09343237
申请日：1999-06-30
申请人： Enrico Marchese , Valery Kapeliouchko , Pasqua Colaianna
发明人： Enrico Marchese , Valery Kapeliouchko , Pasqua Colaianna
IPC分类号： C08F1426
CPC分类号： C08F14/26 , C08F283/06 , Y10S526/909 , Y10S526/911 , C08F2/16 , C08F214/26
摘要： Process for the preparation of tetrafluoroethylene (TFE) polymer-based dispersions having diameter average sizes in the range 0.005-0.06 &mgr;m, which comprises: a) preparation of an aqueous perfluoropolyether (PFPE) microemulsion; b) microemulsion feeding into the polymerization reactor, in such amounts so that the microemulsion perfluoropolyetheral oil phase is present in a concentration higher than 2 ml for liter of reaction medium; c) reaction medium feeding in the gaseous TFE polymerization reactor, optional addition of surfactants, stabilizers, comonomers, transfer agents; d) addition of the initiator, stabilizers, comonomers and transfer agents; e) discharge from the reactor of the polymeric latex.
摘要翻译：制备直径平均尺寸在0.005-0.06μm的四氟乙烯（TFE）聚合物基分散体的方法，其包括：a）制备全氟聚醚（PFPE）微乳液; b）将微乳液进料到聚合反应器中，这样的量使得微乳液全氟聚醚油相以升于1升反应介质中的浓度高于2ml; c）在气态TFE聚合反应器中进料的反应介质，任选加入表面活性剂，稳定剂，共聚单体，转移剂; d）加入引发剂，稳定剂，共聚单体和转移剂; e）从聚合物胶乳的反应器中排出。

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