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1. 发明申请

US20140121321A1 METHOD FOR POLYMERIZNG VINYLIDENE FLUORIDE 有权
标题翻译：聚乙烯酰氟的方法
公开(公告)号：US20140121321A1
公开(公告)日：2014-05-01
申请号：US14125940
申请日：2012-06-15
申请人： Bradley Lane Kent , Valeriy Kapelyushko , Giulio Brinati , Alessandro Veneroni
发明人： Bradley Lane Kent , Valeriy Kapelyushko , Giulio Brinati , Alessandro Veneroni
IPC分类号： C08K5/42
CPC分类号： C08K5/42 , C08F14/22 , C08F214/22 , C08F2/16
摘要： A process for manufacturing a dispersion of a vinylidene fluoride (VDF) thermoplastic polymer [polymer (F)], said process comprising polymerizing VDF in an aqueous phase comprising from 0.5 to 1.5 g/l of at least one surfactant of formula F—(CF2CF2)3—CH2CH2—SO3Xa, wherein Xa is H, a alkali metal or a NRH4 group, with RH being H or a C1-C6 hydrocarbon group [surfactant (T)] and an organic oxidizing agent [agent (O)] as polymerization initiator.
摘要翻译：一种制备偏二氟乙烯（VDF）热塑性聚合物[聚合物（F）]的分散体的方法，所述方法包括在包含0.5至1.5g / l的至少一种式F-（CF 2 CF 2）的表面活性剂的水相中聚合VDF ）3-CH 2 CH 2 -SO 3 Xa，其中Xa为H，碱金属或NRH4基，RH为H或C1-C6烃基[表面活性剂（T）]和有机氧化剂[试剂（O）]为聚合发起人

2. 发明授权

US10030087B2 Method for manufacturing fluoroelastomers 有权
公开(公告)号：US10030087B2
公开(公告)日：2018-07-24
申请号：US14114799
申请日：2012-05-02
申请人： Liubov Chernysheva , Bradley Lane Kent , Giovanni Comino , Valeriy Kapelyushko
发明人： Liubov Chernysheva , Bradley Lane Kent , Giovanni Comino , Valeriy Kapelyushko
IPC分类号： C08F214/28 , C08F214/22
摘要： The invention pertains to a process for manufacturing a fluoroelastomer [fluoroelastomer (A)] having a heat of fusion of less than 5 J/g as measured by ASTM D-3418-08, said method comprising emulsion polymerizing vinylidene fluoride (VDF) in the presence of at least one additional fluorinated monomer, in an aqueous polymerization medium, said method comprising polymerizing VDF and said additional fluorinated monomer(s) in the presence of a redox radical initiator system comprising: —at least one organic oxidizing agent [agent (O)]; —at least one organic reducing agent [agent (R)]; wherein agent (O) is fed to said polymerization medium separately from agent (R), so that agent (O) comes in contact with agent (R) exclusively in said polymerization medium comprising VDF and optional additional monomer(s), to fluoroelastomers having low amount of chain defects and low amount of polar end groups, notably obtainable from said process, and to curable compositions therefrom.

3. 发明授权

US09534106B2 Method for polymerizng vinylidene fluoride 有权
标题翻译：聚偏氟乙烯的方法
公开(公告)号：US09534106B2
公开(公告)日：2017-01-03
申请号：US14125940
申请日：2012-06-15
申请人： Bradley Lane Kent , Valeriy Kapelyushko , Giulio Brinati , Alessandro Veneroni
发明人： Bradley Lane Kent , Valeriy Kapelyushko , Giulio Brinati , Alessandro Veneroni
IPC分类号： C08K5/42 , C08F14/22 , C08F214/22
CPC分类号： C08K5/42 , C08F14/22 , C08F214/22 , C08F2/16
摘要： A process for manufacturing a dispersion of a vinylidene fluoride (VDF) thermoplastic polymer [polymer (F)], said process comprising polymerizing VDF in an aqueous phase comprising from 0.5 to 1.5 g/l of at least one surfactant of formula F—(CF2CF2)3—CH2CH2—SO3Xa, wherein Xa is H, a alkali metal or a NRH4 group, with RH being H or a C1-C6 hydrocarbon group [surfactant (T)] and an organic oxidizing agent [agent (O)] as polymerization initiator.
摘要翻译：一种制备偏二氟乙烯（VDF）热塑性聚合物[聚合物（F）]的分散体的方法，所述方法包括在包含0.5至1.5g / l的至少一种式F-（CF 2 CF 2）的表面活性剂的水相中聚合VDF ）3-CH 2 CH 2 -SO 3 Xa，其中Xa为H，碱金属或NRH4基，RH为H或C1-C6烃基[表面活性剂（T）]和有机氧化剂[试剂（O）]为聚合发起人

4. 发明申请

US20140058052A1 METHOD FOR MANUFACTURING FLUOROELASTOMERS 审中-公开
标题翻译：制造荧光体的方法
公开(公告)号：US20140058052A1
公开(公告)日：2014-02-27
申请号：US14114799
申请日：2012-05-02
申请人： Liubov Chernysheva , Bradley Lane Kent , Giovanni Comino , Valeriy Kapelyushko
发明人： Liubov Chernysheva , Bradley Lane Kent , Giovanni Comino , Valeriy Kapelyushko
IPC分类号： C08F214/28
CPC分类号： C08F214/28 , C08F214/22 , C08F214/222 , C08F214/225
摘要： The invention pertains to a process for manufacturing a fluoroelastomer [fluoroelastomer (A)] having a heat of fusion of less than 5 J/g as measured by ASTM D-3418-08, said method comprising emulsion polymerizing vinylidene fluoride (VDF) in the presence of at least one additional fluorinated monomer, in an aqueous polymerization medium, said method comprising polymerizing VDF and said additional fluorinated monomer(s) in the presence of a redox radical initiator system comprising: —at least one organic oxidizing agent [agent (O)]; —at least one organic reducing agent [agent (R)]; wherein agent (O) is fed to said polymerization medium separately from agent (R), so that agent (O) comes in contact with agent (R) exclusively in said polymerization medium comprising VDF and optional additional monomer(s), to fluoroelastomers having low amount of chain defects and low amount of polar end groups, notably obtainable from said process, and to curable compositions therefrom.
摘要翻译：本发明涉及通过ASTM D-3418-08测定的具有小于5J / g的熔化热的含氟弹性体（含氟弹性体（A）]的制造方法，所述方法包括：将聚偏二氟乙烯在水性聚合介质中存在至少一种另外的氟化单体，所述方法包括在氧化还原自由基引发剂体系存在下聚合VDF和所述另外的氟化单体，所述方法包括： - 至少一种有机氧化剂）]; - 至少一种有机还原剂[试剂（R）]; 其中将试剂（O）与试剂（R）分开地加入到所述聚合介质中，使得试剂（O）仅在包含VDF和任选的另外的单体的所述聚合介质中与试剂（R）接触，具有含氟弹性体少量的链缺陷和少量的极性端基，特别可从所述方法获得，以及可固化组合物。

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