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1. 发明申请

US20090143542A1 Uretonimine-Modified Isocyanate Composition and Method of Forming the Same 有权
标题翻译：脲醛亚胺改性异氰酸酯组合物及其形成方法
公开(公告)号：US20090143542A1
公开(公告)日：2009-06-04
申请号：US12367817
申请日：2009-02-09
申请人： Thomas Savino , Sandra Bananto
发明人： Thomas Savino , Sandra Bananto
IPC分类号： C08L75/04
CPC分类号： C08G18/797
摘要： A uretonimine-modified isocyanate composition has reduced color. The uretonimine-modified isocyanate composition comprises a polyisocyanate composition having two or more isocyanate groups and comprising 4,4′-diphenylmethane diisocyanate (MDI) and a catalyst for catalyzing a reaction of the isocyanate groups to form carbodiimides available for forming uretonimines and uretonimine oligomers. A first quenching agent partially quenches the reaction of the isocyanate groups to inhibit formation of the carbodiimides thereby inhibiting additional formation of uretonimines and uretonimine oligomers and a second quenching agent different than the first quenching agent quenches the reaction of the isocyanate groups to further inhibit formation of the carbodiimides thereby further inhibiting additional formation of uretonimines and uretonimine oligomers. A method of forming the uretonimine-modified isocyanate composition is also disclosed.
摘要翻译：脲酮亚胺改性的异氰酸酯组合物具有降低的颜色。脲酮亚胺改性的异氰酸酯组合物包含具有两个或多个异氰酸酯基团并且包含4,4'-二苯基甲烷二异氰酸酯（MDI）的多异氰酸酯组合物和用于催化异氰酸酯基团反应形成可用于形成脲酮亚胺和脲酮亚胺低聚物的碳二亚胺的催化剂。第一淬火剂部分地淬灭异氰酸酯基团的反应以抑制碳二亚胺的形成，从而抑制另外形成脲酮亚胺和脲酮亚胺低聚物，并且与第一淬灭剂不同的第二淬灭剂猝灭异氰酸酯基团的反应以进一步抑制碳二亚胺从而进一步抑制脲酮亚胺和脲酮亚胺低聚物的额外形成。还公开了形成脲酮亚胺改性的异氰酸酯组合物的方法。

2. 发明申请

US20090111903A1 METHOD OF MAKING POLYURETHANE FOAM 审中-公开
标题翻译：制备聚氨酯泡沫的方法
公开(公告)号：US20090111903A1
公开(公告)日：2009-04-30
申请号：US11930852
申请日：2007-10-31
申请人： Thomas Savino , Joseph Ogonowski , Brian Hyduk , Sandra Bananto
发明人： Thomas Savino , Joseph Ogonowski , Brian Hyduk , Sandra Bananto
IPC分类号： C08G18/08
CPC分类号： C08G18/10 , C08G2101/00 , C08K5/524 , C08L75/04
摘要： An isocyanate prepolymer is made by providing an isocyanate component. A phosphite that is free of active hydrogen groups is introduced into the isocyanate component. An isocyanate-reactive component and a stoichiometric excess of the isocyanate component are reacted in the presence of the phosphite to make the isocyanate prepolymer. A polyurethane foam is made by reacting the isocyanate prepolymer and a second isocyanate-reactive component in the presence of a blowing agent. A composite article is made by forming an elastomeric layer on the outer surface of the polyurethane foam core. Due to the presence of the phosphite during reaction of the isocyanate component and the isocyanate-reactive component to make the isocyanate prepolymer, more efficient use of the phosphite is made, and the full color-reducing effect of the phosphite on the polyurethane foam is realized.
摘要翻译：通过提供异氰酸酯组分制备异氰酸酯预聚物。将不含活性氢基团的亚磷酸酯引入异氰酸酯组分中。异氰酸酯反应性组分和化学计量过量的异氰酸酯组分在亚磷酸盐存在下反应以制备异氰酸酯预聚物。通过使异氰酸酯预聚物和第二异氰酸酯反应性组分在发泡剂存在下反应制备聚氨酯泡沫。通过在聚氨酯泡沫芯的外表面上形成弹性层制成复合制品。由于在异氰酸酯组分和异氰酸酯反应性组分的反应期间存在亚磷酸酯以制备异氰酸酯预聚物，因此进一步有效地使用亚磷酸酯，并且实现了亚磷酸酯对聚氨酯泡沫的全面减色效果。

3. 发明授权

US06624280B1 OLIGOMERIC AND HIGH-MOLECULAR CONVERSION PRODUCTS OF ALLOPHANIC ACID ESTERS WITH NUCLEOPHILIC COMPOUNDS AND LOW-MOLECULAR, OLIGOMERIC AND HIGH-MOLECULAR COMPOUNDS WITH ALLOPHANATE SIDE AND/OR TERMINAL GROUPS, AND THE USE THEREOF 有权
标题翻译：具有单核酸化合物和低分子量，低分子量和高分子量化合物与异丙醇侧和/或末端基团的异戊酸酯的低分子和高分子转化产物及其用途
公开(公告)号：US06624280B1
公开(公告)日：2003-09-23
申请号：US09762121
申请日：2001-03-02
申请人： Heinz-Peter Rink , Werner Jung , Ulrike Röckrath , Thomas Savino
发明人： Heinz-Peter Rink , Werner Jung , Ulrike Röckrath , Thomas Savino
IPC分类号： C08G1810
CPC分类号： C07C275/60 , C08G12/44 , C08G18/3819 , C09D161/32 , C09K3/1021
摘要： Oligomeric and high molecular mass products of reaction of alkyl and aryl allophanates with nucleophilic compounds, and also low molecular mass, oligomeric and high molecular mass compounds containing lateral and/or terminal allophanate groups, and also the use of the reaction products and/or of the compounds in coating compositions, adhesives and sealing compounds or for producing films.
摘要翻译：烷基和芳基脲基甲酸酯与亲核化合物的反应的低分子量和高分子量产物，以及含有侧基和/或末端脲基甲酸酯基团的低分子量，低聚物和高分子量化合物，以及反应产物和/或涂料组合物，粘合剂和密封化合物中的化合物或用于生产膜。

4. 发明申请

US20080085987A1 METHOD OF PRODUCING A URETONIMINE-MODIFIED ISOCYANATE COMPOSITION 审中-公开
标题翻译：生产乌司琼改性异氰酸酯组合物的方法
公开(公告)号：US20080085987A1
公开(公告)日：2008-04-10
申请号：US11538835
申请日：2006-10-05
申请人： Thomas Savino , Sandra Bananto , Nikolay Lebedinski
发明人： Thomas Savino , Sandra Bananto , Nikolay Lebedinski
IPC分类号： C08G18/00
CPC分类号： C08G18/797 , C07D229/00 , C08G18/089 , C08G18/725 , C08G18/7671
摘要： A method produces a uretonimine-modified isocyanate composition having increased low-temperature tolerance. The method comprises providing a polyisocyanate composition comprising 4,4′-diphenylmethane diisocyanate (MDI) and reacting the polyisocyanate composition at a temperature of from about 90° C. to about 115° C. in the presence of a catalyst, and optionally a co-catalyst, such that the isocyanate groups react to form uretonimine oligomers. The reaction of the polyisocyanate composition is quenched with a quenching agent to produce an intermediate composition having an intermediate isocyanate value from about 25.5 to about 28.5. A second polyisocyanate composition is added to the intermediate composition in an amount sufficient to produce the uretonimine-modified isocyanate composition having a final isocyanate value of from about 29.0 to about 29.5.
摘要翻译：一种方法产生具有增加的低温耐受性的脲酮亚胺改性的异氰酸酯组合物。该方法包括提供包含4,4'-二苯基甲烷二异氰酸酯（MDI）的多异氰酸酯组合物，并在约90℃至约115℃的温度下，在催化剂和任选的共 - 催化剂，使得异氰酸酯基团反应形成脲酮亚胺低聚物。多异氰酸酯组合物的反应用骤冷剂淬灭以产生具有约25.5至约28.5的中间体异氰酸酯值的中间体组合物。将第二多异氰酸酯组合物以足以产生具有约29.0至约29.5的最终异氰酸酯值的脲酮亚胺改性的异氰酸酯组合物的量加入到中间体组合物中。

5. 发明授权

US07777054B2 Uretonimine-modified isocyanate composition and method of forming the same 有权
标题翻译：脲醛亚胺改性异氰酸酯组合物及其形成方法
公开(公告)号：US07777054B2
公开(公告)日：2010-08-17
申请号：US12367817
申请日：2009-02-09
申请人： Thomas Savino , Sandra Banato
发明人： Thomas Savino , Sandra Banato
IPC分类号： C07D229/00 , C07D205/00
CPC分类号： C08G18/797
摘要： A uretonimine-modified isocyanate composition has reduced color. The uretonimine-modified isocyanate composition comprises a polyisocyanate composition having two or more isocyanate groups and comprising 4,4′-diphenylmethane diisocyanate (MDI) and a catalyst for catalyzing a reaction of the isocyanate groups to form carbodiimides available for forming uretonimines and uretonimine oligomers. A first quenching agent partially quenches the reaction of the isocyanate groups to inhibit formation of the carbodiimides thereby inhibiting additional formation of uretonimines and uretonimine oligomers and a second quenching agent different than the first quenching agent quenches the reaction of the isocyanate groups to further inhibit formation of the carbodiimides thereby further inhibiting additional formation of uretonimines and uretonimine oligomers. A method of forming the uretonimine-modified isocyanate composition is also disclosed.
摘要翻译：脲酮亚胺改性的异氰酸酯组合物具有降低的颜色。脲酮亚胺改性的异氰酸酯组合物包含具有两个或多个异氰酸酯基团并且包含4,4'-二苯基甲烷二异氰酸酯（MDI）的多异氰酸酯组合物和用于催化异氰酸酯基团反应形成可用于形成脲酮亚胺和脲酮亚胺低聚物的碳二亚胺的催化剂。第一淬火剂部分地淬灭异氰酸酯基团的反应以抑制碳二亚胺的形成，从而抑制另外形成脲酮亚胺和脲酮亚胺低聚物，并且与第一淬灭剂不同的第二淬灭剂猝灭异氰酸酯基团的反应以进一步抑制碳二亚胺从而进一步抑制脲酮亚胺和脲酮亚胺低聚物的额外形成。还公开了形成脲酮亚胺改性的异氰酸酯组合物的方法。

6. 发明申请

US20080119590A1 LIGNOCELLULOSIC COMPOSITE MATERIAL AND METHOD FOR PREPARING THE SAME 审中-公开
标题翻译：合成纤维素复合材料及其制备方法
公开(公告)号：US20080119590A1
公开(公告)日：2008-05-22
申请号：US12022246
申请日：2008-01-30
申请人： Thomas Savino , Sandra Bananto
发明人： Thomas Savino , Sandra Bananto
IPC分类号： C08K5/04 , B29C43/02
CPC分类号： B27N3/002 , B27N3/083
摘要： A lignocellulosic composite material and a method for preparing the lignocellulosic composite material are disclosed. The composite material includes lignocellulosic particles and a binder resin being a mixture of a polyisocyanate component and a release agent. The release agent is formed from a first component having hydroxyl groups and a second component having isocyanate groups in excess of the hydroxyl groups. The first component is selected from at least one of i) an acid phosphate and ii) pyrophosphates represented by those derived from the acid phosphates (i) and mixtures of the acid phosphates (i). The first component is passivated by mixing it with the second component which is preferably monomeric diphenylmethane diisocyanate selected from at least one of diphenylmethane-4,4′-diisocyanate, diphenylmethane-2,4′-diisocyanate, and diphenylmethane-2,2′-diisocyanate.
摘要翻译：公开了一种木质纤维复合材料和一种木质纤维复合材料的制备方法。复合材料包括木质纤维素颗粒和作为多异氰酸酯组分和脱模剂的混合物的粘合剂树脂。脱模剂由具有羟基的第一组分和具有超过羟基的异氰酸酯基的第二组分形成。第一组分选自i）酸式磷酸盐和ii）由酸式磷酸盐（i）衍生的那些和磷酸酸盐（i）的混合物所代表的焦磷酸盐中的至少一种。通过将第一组分与第二组分混合来钝化第一组分，该组分优选是选自二苯基甲烷-4,4'-二异氰酸酯，二苯基甲烷-2,4'-二异氰酸酯和二苯基甲烷-2,2'-二异氰酸酯中的至少一种的单体二苯基甲烷二异氰酸酯，二异氰酸酯。

7. 发明申请

US20070213496A1 URETONIMINE-MODIFIED ISOCYANATE COMPOSITION AND METHOD OF FORMING THE SAME 有权
标题翻译： URETONIMINE改性的异氰酸酯组合物及其形成方法
公开(公告)号：US20070213496A1
公开(公告)日：2007-09-13
申请号：US11276702
申请日：2006-03-10
申请人： Thomas Savino , Sandra Bananto
发明人： Thomas Savino , Sandra Bananto
IPC分类号： C08G18/00
CPC分类号： C08G18/797
摘要： A uretonimine-modified isocyanate composition has reduced color. The uretonimine-modified isocyanate composition comprises a polyisocyanate composition having two or more isocyanate groups and comprising 4,4′-diphenylmethane diisocyanate (MDI) and a catalyst for catalyzing a reaction of the isocyanate groups to form carbodiimides available for forming uretonimines and uretonimine oligomers. A first quenching agent partially quenches the reaction of the isocyanate groups to inhibit formation of the carbodiimides thereby inhibiting additional formation of uretonimines and uretonimine oligomers and a second quenching agent different than the first quenching agent quenches the reaction of the isocyanate groups to further inhibit formation of the carbodiimides thereby further inhibiting additional formation of uretonimines and uretonimine oligomers. A method of forming the uretonimine-modified isocyanate composition is also disclosed.
摘要翻译：脲酮亚胺改性的异氰酸酯组合物具有降低的颜色。脲酮亚胺改性的异氰酸酯组合物包含具有两个或多个异氰酸酯基团并且包含4,4'-二苯基甲烷二异氰酸酯（MDI）的多异氰酸酯组合物和用于催化异氰酸酯基团反应形成可用于形成脲酮亚胺和脲酮亚胺低聚物的碳二亚胺的催化剂。第一淬火剂部分地淬灭异氰酸酯基团的反应以抑制碳二亚胺的形成，从而抑制另外形成脲酮亚胺和脲酮亚胺低聚物，并且与第一淬灭剂不同的第二淬灭剂猝灭异氰酸酯基团的反应以进一步抑制碳二亚胺从而进一步抑制脲酮亚胺和脲酮亚胺低聚物的额外形成。还公开了形成脲酮亚胺改性的异氰酸酯组合物的方法。

8. 发明申请

US20070213432A1 URETONIMINE-MODIFIED ISOCYANATE COMPOSITION AND METHOD OF FORMING THE SAME 有权
标题翻译： URETONIMINE改性的异氰酸酯组合物及其形成方法
公开(公告)号：US20070213432A1
公开(公告)日：2007-09-13
申请号：US11276693
申请日：2006-03-10
申请人： THOMAS SAVINO
发明人： THOMAS SAVINO
IPC分类号： C08K5/34 , C08G18/08
CPC分类号： C08K5/3442 , C08G18/095 , C08G18/7657
摘要： A uretonimine-modified isocyanate composition having reduced color and a method of forming the same is disclosed. The method of forming the uretonimine-modified isocyanate composition comprises providing a polyisocyanate composition having two or more isocyanate groups and reacting the polyisocyanate composition at a temperature in a range of from about 80° C. to about 130° C. and in the presence of a catalyst. The reaction of the polyisocyanate composition is quenched with a quenching agent and a color inhibitor having a low basicity and having at least one hindered amine group is added. The uretonimine-modified isocyanate composition has a color value corresponding to an a* value of greater than about −10 and a b* value less than about 10 as defined by CIE L*a*b* (CIELAB) Color Space Specification and undergoes a % NCO group decrease of less than about 6 %.
摘要翻译：公开了具有降低颜色的脲酮亚胺改性的异氰酸酯组合物及其形成方法。形成脲酮亚胺改性的异氰酸酯组合物的方法包括提供具有两个或更多个异氰酸酯基团的多异氰酸酯组合物，并使多异氰酸酯组合物在约80℃至约130℃的温度范围内和在催化剂多异氰酸酯组合物的反应用淬灭剂淬灭，并且添加具有低碱度并具有至少一个受阻胺基团的显色抑制剂。脲酮亚胺改性的异氰酸酯组合物具有对应于大于约-10的a *值和由CIE L * a * b *（CIELAB）颜色空间规格定义的小于约10的ab *值的颜色值，并且经历％ NCO组减少不到6％。

9. 发明申请

US20050242459A1 Lignocellulosic composite material and method for preparing the same 审中-公开
标题翻译：木质纤维素复合材料及其制备方法
公开(公告)号：US20050242459A1
公开(公告)日：2005-11-03
申请号：US10835134
申请日：2004-04-29
申请人： Thomas Savino , Sandra Bananto
发明人： Thomas Savino , Sandra Bananto
IPC分类号： B27N3/00 , B27N3/08
CPC分类号： B27N3/002 , B27N3/083
摘要： A lignocellulosic composite material and a method for preparing the lignocellulosic composite material are disclosed. The composite material includes lignocellulosic particles and a binder resin being a mixture of a polyisocyanate component and a release agent. The release agent is formed from a first component having hydroxyl groups and a second component having isocyanate groups in excess of the hydroxyl groups. The first component is selected from at least one of i) an acid phosphate and ii) pyrophosphates represented by those derived from the acid phosphates (i) and mixtures of the acid phosphates (i). The first component is passivated by mixing it with the second component which is preferably monomeric diphenylmethane diisocyanate selected from at least one of diphenylmethane-4,4′-diisocyanate, diphenylmethane-2,4′-diisocyanate, and diphenylmethane-2,2′-diisocyanate.
摘要翻译：公开了一种木质纤维复合材料和一种木质纤维复合材料的制备方法。复合材料包括木质纤维素颗粒和作为多异氰酸酯组分和脱模剂的混合物的粘合剂树脂。脱模剂由具有羟基的第一组分和具有超过羟基的异氰酸酯基的第二组分形成。第一组分选自i）酸式磷酸盐和ii）由酸式磷酸盐（i）衍生的那些和磷酸酸盐（i）的混合物所代表的焦磷酸盐中的至少一种。通过将第一组分与第二组分混合来钝化第一组分，该组分优选是选自二苯基甲烷-4,4'-二异氰酸酯，二苯基甲烷-2,4'-二异氰酸酯和二苯基甲烷-2,2'-二异氰酸酯中的至少一种的单体二苯基甲烷二异氰酸酯，二异氰酸酯。

10. 发明授权

US07541397B2 Uretonimine-modified isocyanate composition and method of forming the same 有权
标题翻译：脲醛亚胺改性异氰酸酯组合物及其形成方法
公开(公告)号：US07541397B2
公开(公告)日：2009-06-02
申请号：US11276693
申请日：2006-03-10
申请人： Thomas Savino , Sandra Bananto
发明人： Thomas Savino , Sandra Bananto
IPC分类号： C08K5/34 , C08G18/08
CPC分类号： C08K5/3442 , C08G18/095 , C08G18/7657
摘要： A uretonimine-modified isocyanate composition having reduced color and a method of forming the same is disclosed. The method of forming the uretonimine-modified isocyanate composition comprises providing a polyisocyanate composition having two or more isocyanate groups and reacting the polyisocyanate composition at a temperature in a range of from about 80° C. to about 130° C. and in the presence of a catalyst. The reaction of the polyisocyanate composition is quenched with a quenching agent and a color inhibitor having a low basicity and having at least one hindered amine group is added. The uretonimine-modified isocyanate composition has a color value corresponding to an a* value of greater than about −10 and a b* value less than about 10 as defined by CIE L*a*b* (CIELAB) Color Space Specification and undergoes a % NCO group decrease of less than about 6 %.
摘要翻译：公开了具有降低颜色的脲酮亚胺改性的异氰酸酯组合物及其形成方法。形成脲酮亚胺改性的异氰酸酯组合物的方法包括提供具有两个或多个异氰酸酯基团的多异氰酸酯组合物，并使多异氰酸酯组合物在约80℃至约130℃的温度范围内和在催化剂多异氰酸酯组合物的反应用淬灭剂淬灭，并且添加具有低碱度并具有至少一个受阻胺基团的显色抑制剂。脲酮亚胺改性的异氰酸酯组合物具有对应于大于约-10的a *值和由CIE L * a * b *（CIELAB）颜色空间规格定义的小于约10的ab *值的颜色值，并且经历％ NCO组减少不到6％。

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