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1. 发明授权

US07897128B2 Preparation of complex metal oxides 有权
标题翻译：复合金属氧化物的制备
公开(公告)号：US07897128B2
公开(公告)日：2011-03-01
申请号：US11737942
申请日：2007-04-20
申请人： Robert Quinn , Diwakar Garg , Frederick Carl Wilhelm , Terry Lee Slager
发明人： Robert Quinn , Diwakar Garg , Frederick Carl Wilhelm , Terry Lee Slager
IPC分类号： C01G45/00
CPC分类号： C01G49/0018 , C01B13/185 , C01B32/60 , C01G45/1221 , C01G49/0036 , C01G49/0072 , C01P2002/50 , C01P2002/72
摘要： The present invention provides a process for making a complex metal oxide comprising the formula AxByOz. The process comprises the steps of: (a) reacting in solution at a temperature of between about 75° C. to about 100° C. at least one water-soluble salt of A, at least one water-soluble salt of B and a stoichiometric amount of a carbonate salt or a bicarbonate salt required to form a mole of a carbonate precipitate represented by the formula AxBy(CO3)n, wherein the reacting is conducted in a substantial absence of carbon dioxide to form the carbonate precipitate and wherein the molar amount of carbonate salt or bicarbonate salt is at least three times the stoichiometric amount of carbonate or bicarbonate salt required to form a mole of the carbonate precipitate; and (b) reacting the carbonate precipitate with an oxygen containing fluid under conditions to form the complex metal oxide.
摘要翻译：本发明提供一种制备复合金属氧化物的方法，该复合金属氧化物包含式AxByOz。该方法包括以下步骤：（a）在约75℃至约100℃的温度下在溶液中使至少一种A的水溶性盐，至少一种B的水溶性盐和化学计量的形成式AxBy（CO3）n表示的摩尔碳酸盐沉淀所需的碳酸盐或碳酸氢盐，其中反应在基本上不存在二氧化碳的情况下进行以形成碳酸盐沉淀物，其中摩尔碳酸盐或碳酸氢盐的量至少为形成一摩尔碳酸盐沉淀物所需的碳酸盐或碳酸氢盐的化学计量量的三倍; 和（b）在条件下使碳酸盐沉淀物与含氧流体反应以形成复合金属氧化物。

2. 发明授权

US07824655B2 Regeneration of complex metal oxides for the production of hydrogen 有权
标题翻译：用于生产氢气的复合金属氧化物的再生
公开(公告)号：US07824655B2
公开(公告)日：2010-11-02
申请号：US11339060
申请日：2006-01-25
申请人： Terry Lee Slager , Diwakar Garg , Xiang-Dong Peng , Bryan Clair Hoke, Jr.
发明人： Terry Lee Slager , Diwakar Garg , Xiang-Dong Peng , Bryan Clair Hoke, Jr.
IPC分类号： C01B3/24 , C01B3/26
CPC分类号： C01B3/38 , C01B3/46 , C01B2203/0233 , C01B2203/0425 , C01B2203/0475 , Y02P20/52
摘要： In a process for producing a hydrogen-containing gas, a hydrocarbon feed gas and steam are introduced into a reaction vessel containing a complex metal oxide and steam-hydrocarbon reforming catalyst thereby forming a combustible gas mixture comprising hydrogen. A regeneration gas comprising greater than 0.1 volume % oxygen up to and including 2 volume % oxygen is introduced into the reaction vessel to displace at least a portion of the combustible gas mixture from the reaction vessel. Subsequently, additional regeneration gases may be introduced into the reaction vessel. Numerous means for providing various regeneration gases are presented.
摘要翻译：在制造含氢气体的方法中，将烃进料气体和蒸汽引入含有复合金属氧化物和蒸汽 - 烃重整催化剂的反应容器中，从而形成包含氢气的可燃气体混合物。将包括大于0.1体积％氧气的再生气体引入反应容器中以将至少一部分可燃气体混合物从反应容器中置换。随后，可以向反应容器中引入另外的再生气体。提出了许多用于提供各种再生气体的方法。

3. 发明申请

US20080260621A1 Preparation of Complex Metal Oxides 有权
标题翻译：复杂金属氧化物的制备
公开(公告)号：US20080260621A1
公开(公告)日：2008-10-23
申请号：US11737942
申请日：2007-04-20
申请人： Robert Quinn , Diwakar Garg , Frederick Carl Wilhelm , Terry Lee Slager
发明人： Robert Quinn , Diwakar Garg , Frederick Carl Wilhelm , Terry Lee Slager
IPC分类号： C01D1/02 , C01G45/12
CPC分类号： C01G49/0018 , C01B13/185 , C01B32/60 , C01G45/1221 , C01G49/0036 , C01G49/0072 , C01P2002/50 , C01P2002/72
摘要： The present invention provides a process for making a complex metal oxide comprising the formula AxByOz. The process comprises the steps of: (a) reacting in solution at a temperature of between about 75° C. to about 100° C. at least one water-soluble salt of A, at least one water-soluble salt of B and a stoichiometric amount of a carbonate salt or a bicarbonate salt required to form a mole of a carbonate precipitate represented by the formula AxBy(CO3)n, wherein the reacting is conducted in a substantial absence of carbon dioxide to form the carbonate precipitate and wherein the molar amount of carbonate salt or bicarbonate salt is at least three times the stoichiometric amount of carbonate or bicarbonate salt required to form a mole of the carbonate precipitate; and (b) reacting the carbonate precipitate with an oxygen containing fluid under conditions to form the complex metal oxide.
摘要翻译：本发明提供一种制备复合金属氧化物的方法，所述复合金属氧化物包括下式：其中R 1，R 2，R 3，该方法包括以下步骤：（a）在约75℃至约100℃的温度下在溶液中使至少一种A的水溶性盐，至少一种B的水溶性盐和化学计量量的形成一摩尔由式A表示的碳酸盐沉淀所需的碳酸盐或碳酸氢盐（CO 3/3）其中反应在基本上不存在二氧化碳的情况下进行以形成碳酸盐沉淀物，并且其中碳酸盐或碳酸氢盐的摩尔量为化学计量量的碳酸盐的至少三倍或形成一摩尔碳酸盐沉淀物所需的碳酸氢盐; 和（b）在条件下使碳酸盐沉淀物与含氧流体反应以形成复合金属氧化物。

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