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1. 发明授权

US08142857B2 Compound and method for producing the same 有权
标题翻译：化合物及其制备方法
公开(公告)号：US08142857B2
公开(公告)日：2012-03-27
申请号：US12330382
申请日：2008-12-08
申请人： Chi-Fa Hsieh , Jui-Ming Yeh , Tai-Kang Liu
发明人： Chi-Fa Hsieh , Jui-Ming Yeh , Tai-Kang Liu
IPC分类号： B05D1/34
CPC分类号： C08G18/0823 , C08G18/3228 , C08G18/4277 , C08G18/6659 , C08G18/758 , C08K9/08 , C09D175/04
摘要： The invention provides a compound and method of producing the same. The method of the invention includes the following steps. First of all, Polycaprolactone (PCL), dimethylol propionic acid (DMPA), 4,4′-methylenebis (cyclohexyl isocyanate) (H12MDI), and dibutyltin dilaurate (DBT) are mixed in a solvent in the first place and a solution is formed. This solution is then mixed with triethylamine (TEA) and triethylene tetramine (TETA). After that, amino-terminated anionic waterborne polyurethane (WPU) is produced. A sol-gel process is proceeded with a mixture of amino-terminated anionic waterborne polyurethane, tetraethylorthosilicate (TEOS) without any extra catalyst, and a compound, waterborne polyurethane-silica nanocomposite materials, is eventually produced.
摘要翻译：本发明提供了一种化合物及其制备方法。本发明的方法包括以下步骤。首先将聚己内酯（PCL），二羟甲基丙酸（DMPA），4,4'-亚甲基双（环己基异氰酸酯）（H12MDI）和二月桂酸二丁基锡（DBT）首先在溶剂中混合，形成溶液。然后将该溶液与三乙胺（TEA）和三亚乙基四胺（TETA）混合。之后，生成氨基封端的阴离子水性聚氨酯（WPU）。溶胶 - 凝胶法用氨基封端的阴离子水性聚氨酯，原硅酸四乙酯（TEOS）与无任何额外催化剂的混合物进行，最终生产化合物水性聚氨酯 - 二氧化硅纳米复合材料。

2. 发明授权

US07822583B2 Method of batch falling strand devolatilizer 有权
标题翻译：批量降链脱挥器的方法
公开(公告)号：US07822583B2
公开(公告)日：2010-10-26
申请号：US11785110
申请日：2007-04-16
申请人： Tai-Kang Liu , Chi-Fa Hsieh
发明人： Tai-Kang Liu , Chi-Fa Hsieh
IPC分类号： G06F17/50
CPC分类号： B01D1/065 , B01D1/22
摘要： A design method of batch falling strand devolatilizers is disclosed. The method includes following steps. Firstly, construct a database that contains data of batch falling strand devolatilizer vs. devolatilization of at least one kind of polymer. Then data in the database is substituted into a mass balance difference equation to get a backmixing parameter. When the backmixing parameter is zero or is approaching zero, a liquid diffusion stage efficiency equation having a film equation or a pool equation is integrated with the mass balance difference equation to get a devolatilization process efficiency equation. By optimizing of a theoretical value of the backmixing parameter, a theoretical value of the process efficiency from calculation of the devolatilization process efficiency equation approaches the value of the process efficiency. Then the theoretical value of the backmixing parameter is substituted into the devolatilization process efficiency equation for performing volume design of the batch falling strand devolatilizer.
摘要翻译：公开了一种批量降链脱挥发份的设计方法。该方法包括以下步骤。首先构建一个数据库，该数据库包含批量降链脱挥发物与至少一种聚合物的脱挥发分数据。然后将数据库中的数据代入质量平衡差分方程以获得回混参数。当回混参数为零或接近零时，具有膜方程或池方程的液体扩散阶段效率方程与质量平衡差分方程整合，得到脱挥发分过程效率方程。通过优化回混参数的理论值，通过计算脱挥发分过程效率方程式的过程效率的理论值接近过程效率的值。然后将后混合参数的理论值代入进行批量降链脱挥器的体积设计的脱挥发分过程效率方程。

3. 发明申请

US20080255338A1 Method of batch falling strand devolatilizer 有权
标题翻译：批量降链脱挥器的方法
公开(公告)号：US20080255338A1
公开(公告)日：2008-10-16
申请号：US11785110
申请日：2007-04-16
申请人： Tai-Kang Liu , Chi-Fa Hsieh
发明人： Tai-Kang Liu , Chi-Fa Hsieh
IPC分类号： B01J19/18
CPC分类号： B01D1/065 , B01D1/22
摘要： A design method of batch falling strand devolatilizers is disclosed. The method includes following steps. Firstly, construct a database that contains data of batch falling strand devolatilizer vs. devolatilization of at least one kind of polymer. Then data in the database is substituted into a mass balance difference equation to get a backmixing parameter. When the backmixing parameter is zero or is approaching zero, a liquid diffusion stage efficiency equation having a film equation or a pool equation is integrated with the mass balance difference equation to get a devolatilization process efficiency equation. By means of a theoretical value of the backmixing parameter, a theoretical value of the process efficiency from calculation of the devolatilization process efficiency equation approaches the value of the process efficiency. Then the theoretical value of the backmixing parameter is substituted into the devolatilization process efficiency equation for performing volume design of the batch falling strand devolatilizer.
摘要翻译：公开了一种批量降链脱挥发份的设计方法。该方法包括以下步骤。首先构建一个数据库，该数据库包含批量降链脱挥发物与至少一种聚合物的脱挥发分数据。然后将数据库中的数据代入质量平衡差分方程以获得回混参数。当回混参数为零或接近零时，具有膜方程或池方程的液体扩散阶段效率方程与质量平衡差分方程整合，得到脱挥发分过程效率方程。通过回混参数的理论值，计算脱挥发分过程效率方程式的过程效率的理论值接近过程效率的值。然后将后混合参数的理论值代入进行批量降链脱挥器的体积设计的脱挥发分过程效率方程。

4. 发明申请

US20100311922A1 SYSTEM AND METHOD FOR MANUFACTURING ORGANOPOLYSILOXANE 有权
标题翻译：用于制造有机硅氧烷的系统和方法
公开(公告)号：US20100311922A1
公开(公告)日：2010-12-09
申请号：US12479816
申请日：2009-06-07
申请人： Tai-Kang Liu , Chi-Fa Hsieh
发明人： Tai-Kang Liu , Chi-Fa Hsieh
IPC分类号： C08F2/01 , B01J19/00
CPC分类号： C08G77/10
摘要： The invention discloses a method and a system for manufacturing organopolysiloxane. The system comprises N raw material tanks, N gauging tanks, a first reactor, a second reactor and at least one product tanks which are arranged in order from high to low. The manufacturing method comprises the following steps of: firstly, N raw materials are added into the N raw material tanks respectively. Then, a plurality of processing parameters about the organopolysiloxane are inputted to control the N gauging tanks to measure the dosage of the N raw materials according to the processing parameters, which along with a cyclic siloxane monomer are inputted into the first reactor. The first reactor is controlled to carry on ring-opening and re-distribution polymerization equilibrium reaction to the N raw materials and the cyclic siloxane monomer, so as to generate an intermediate product, and transfer the intermediate product into the second reactor. Finally, the second reactor is controlled to carry on a decomposition transient catalytic reaction to the intermediate product and a devolatilization operation to obtain the organopolysiloxane products.
摘要翻译：本发明公开了一种制造有机聚硅氧烷的方法和系统。该系统包括N个原料罐，N个测量罐，第一反应器，第二反应器和至少一个从高到低的顺序排列的产品罐。制造方法包括以下步骤：首先将N种原料分别加入N原料罐中。然后，输入关于有机聚硅氧烷的多个处理参数，以控制N个测量罐，以根据处理参数测量N种原料的用量，其中环状硅氧烷单体与第一反应器一起输入。控制第一反应器对N原料和环状硅氧烷单体进行开环和再分配聚合反应平衡反应，以产生中间产物，并将中间产物转移到第二反应器中。最后，控制第二反应器对中间产物进行分解瞬态催化反应，并进行脱挥发分操作以获得有机聚硅氧烷产物。

5. 发明申请

US20100143597A1 COMPOUND AND METHOD FOR PRODUCING THE SAME 有权
标题翻译：化合物及其制造方法
公开(公告)号：US20100143597A1
公开(公告)日：2010-06-10
申请号：US12330382
申请日：2008-12-08
申请人： CHI-FA HSIEH , JUI-MING YEH , TAI-KANG LIU
发明人： CHI-FA HSIEH , JUI-MING YEH , TAI-KANG LIU
IPC分类号： B05D3/00 , C08L75/04
CPC分类号： C08G18/0823 , C08G18/3228 , C08G18/4277 , C08G18/6659 , C08G18/758 , C08K9/08 , C09D175/04
摘要： The invention provides a compound and method of producing the same. The method of the invention includes the following steps. First of all, Polycaprolactone (PCL), dimethylol propionic acid (DMPA), 4,4′-methylenebis (cyclohexyl isocyanate) (H12MDI), and dibutyltin dilaurate (DBT) are mixed in a solvent in the first place and a solution is formed. This solution is then mixed with triethylamine (TEA) and triethylene tetramine (TETA). After that, amino-terminated anionic waterborne polyurethane (WPU) is produced. A sol-gel process is proceeded with a mixture of amino-terminated anionic waterborne polyurethane, tetraethylorthosilicate (TEOS) without any extra catalyst, and a compound, waterborne polyurethane-silica nanocomposite materials, is eventually produced.
摘要翻译：本发明提供了一种化合物及其制备方法。本发明的方法包括以下步骤。首先将聚己内酯（PCL），二羟甲基丙酸（DMPA），4,4'-亚甲基双（环己基异氰酸酯）（H12MDI）和二月桂酸二丁基锡（DBT）首先在溶剂中混合，形成溶液。然后将该溶液与三乙胺（TEA）和三亚乙基四胺（TETA）混合。之后，生成氨基封端的阴离子水性聚氨酯（WPU）。溶胶 - 凝胶法用氨基封端的阴离子水性聚氨酯，原硅酸四乙酯（TEOS）与无任何额外催化剂的混合物进行，最终生产化合物水性聚氨酯 - 二氧化硅纳米复合材料。

6. 发明申请

US20120101203A1 COMPOUND AND METHOD FOR PRODUCING THE SAME 审中-公开
标题翻译：化合物及其制造方法
公开(公告)号：US20120101203A1
公开(公告)日：2012-04-26
申请号：US13342034
申请日：2012-01-01
申请人： Chi-Fa Hsieh , Jui-Ming Yeh , Tai-Kang Liu
发明人： Chi-Fa Hsieh , Jui-Ming Yeh , Tai-Kang Liu
IPC分类号： C08K5/5415 , C08L75/04
CPC分类号： C08G18/0823 , C08G18/3228 , C08G18/4277 , C08G18/6659 , C08G18/758 , C08K9/08 , C09D175/04
摘要： The invention provides a compound and method of producing the same. The method of the invention includes the following steps. First of all, Polycaprolactone (PCL), dimethylol propionic acid (DMPA), 4,4′-methylenebis (cyclohexyl isocyanate) (H12MDI), and dibutyltin dilaurate (DBT) are mixed in a solvent in the first place and a solution is formed. This solution is then mixed with triethylamine (TEA) and triethylene tetramine (TETA). After that, amino-terminated anionic waterborne polyurethane (WPU) is produced. A sol-gel process is proceeded with a mixture of amino-terminated anionic waterborne polyurethane, tetraethylorthosilicate (TEOS) without any extra catalyst, and a compound, waterborne polyurethane-silica nanocomposite materials, is eventually produced.
摘要翻译：本发明提供了一种化合物及其制备方法。本发明的方法包括以下步骤。首先将聚己内酯（PCL），二羟甲基丙酸（DMPA），4,4'-亚甲基双（环己基异氰酸酯）（H12MDI）和二月桂酸二丁基锡（DBT）首先在溶剂中混合，形成溶液。然后将该溶液与三乙胺（TEA）和三亚乙基四胺（TETA）混合。之后，生成氨基封端的阴离子水性聚氨酯（WPU）。溶胶 - 凝胶法用氨基封端的阴离子水性聚氨酯，原硅酸四乙酯（TEOS）与无任何额外催化剂的混合物进行，最终生产化合物水性聚氨酯 - 二氧化硅纳米复合材料。

7. 发明授权

US08071032B2 System and method for manufacturing organopolysiloxane 有权
标题翻译：制造有机聚硅氧烷的体系及方法
公开(公告)号：US08071032B2
公开(公告)日：2011-12-06
申请号：US12479816
申请日：2009-06-07
申请人： Tai-Kang Liu , Chi-Fa Hsieh
发明人： Tai-Kang Liu , Chi-Fa Hsieh
IPC分类号： B01J19/00 , C08F2/01
CPC分类号： C08G77/10
摘要： The invention discloses a method and a system for manufacturing organopolysiloxane. The system comprises N raw material tanks, N gauging tanks, a first reactor, a second reactor and at least one product tanks which are arranged in order from high to low. The manufacturing method comprises the following steps of: firstly, N raw materials are added into the N raw material tanks respectively. Then, a plurality of processing parameters about the organopolysiloxane are inputted to control the N gauging tanks to measure the dosage of the N raw materials according to the processing parameters, which along with a cyclic siloxane monomer are inputted into the first reactor. The first reactor is controlled to carry on ring-opening and re-distribution polymerization equilibrium reaction to the N raw materials and the cyclic siloxane monomer, so as to generate an intermediate product, and transfer the intermediate product into the second reactor. Finally, the second reactor is controlled to carry on a decomposition transient catalytic reaction to the intermediate product and a devolatilization operation to obtain the organopolysiloxane products.
摘要翻译：本发明公开了一种制造有机聚硅氧烷的方法和系统。该系统包括N个原料罐，N个测量罐，第一反应器，第二反应器和至少一个从高到低的顺序排列的产品罐。制造方法包括以下步骤：首先将N种原料分别加入N原料罐中。然后，输入关于有机聚硅氧烷的多个处理参数，以控制N个测量罐，以根据处理参数测量N原料的用量，其中环状硅氧烷单体与第一反应器一起输入。控制第一反应器对N原料和环状硅氧烷单体进行开环和再分配聚合反应平衡反应，以产生中间产物，并将中间产物转移到第二反应器中。最后，控制第二反应器对中间产物进行分解瞬态催化反应，并进行脱挥发分操作以获得有机聚硅氧烷产物。

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