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1. 发明授权

US07449238B1 LiF-coated doped and undoped yttrium oxide 有权
标题翻译： LiF涂层掺杂和未掺杂的氧化钇
公开(公告)号：US07449238B1
公开(公告)日：2008-11-11
申请号：US11861498
申请日：2007-09-26
申请人： Guillermo R. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal , Woohong Kim , Bryan Sadowski
发明人： Guillermo R. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal , Woohong Kim , Bryan Sadowski
IPC分类号： B32B5/16
CPC分类号： C04B35/505 , B82Y30/00 , C04B35/62655 , C04B35/628 , C04B35/62886 , C04B35/62897 , C04B35/645 , C04B2235/3203 , C04B2235/3217 , C04B2235/3224 , C04B2235/445 , C04B2235/528 , C04B2235/5436 , C04B2235/5445 , C04B2235/5454 , C04B2235/662 , C04B2235/721 , C04B2235/786 , C04B2235/9653 , Y10T428/2991 , Y10T428/2993 , Y10T428/2995 , Y10T428/2996 , Y10T428/2998
摘要： An embodiment of the invention includes a particle. The particle includes a first yttria core; and a fluoride salt coating on the first yttria core. The coating is sufficiently continuous to prevent a large number of sites where a second yttria core may come into contact with the first yttria core. Optionally, the particle has been heated in an oxidizing atmosphere to a temperature in the range of about 400° C. to about 750° C. Optionally, the particle is substantially free of at least one of carbon-containing species and water. Optionally, the fluoride salt is lithium fluoride. Optionally, the fluoride salt is aluminum fluoride.
摘要翻译：本发明的实施方案包括颗粒。颗粒包括第一氧化钇核; 和在第一氧化钇核上的氟化物盐涂层。涂层足够连续以防止大量的第二氧化钇芯可能与第一氧化钇芯接触的位置。任选地，颗粒已经在氧化气氛中加热至约400℃至约750℃的温度。任选地，该颗粒基本上不含含碳物质和水中的至少一种。任选地，氟化物盐是氟化锂。任选地，氟化物盐是氟化铝。

2. 发明授权

US06526782B1 Multi heating zone apparatus and process for making core/clad glass fibers 有权
标题翻译：多层加热区设备及制造核心/复合玻璃纤维的工艺
公开(公告)号：US06526782B1
公开(公告)日：2003-03-04
申请号：US09964548
申请日：2001-09-28
申请人： Reza Mossadegh , Brian Cole , Pablo Pureza , Jasbinder Sanghera , Shyam Bayya , Ishwar Aggarwal
发明人： Reza Mossadegh , Brian Cole , Pablo Pureza , Jasbinder Sanghera , Shyam Bayya , Ishwar Aggarwal
IPC分类号： C03B37022
CPC分类号： C03B37/023 , C03B2201/86 , C03C3/321 , C03C13/043
摘要： This invention pertains to apparatus and process for making core/clad glass fibers. The apparatus includes a central tube or receptacle connected at the top to a pressure controller and terminating in a reduced section; a side tube or receptacle positioned at about the level of the upper portion of the central tube; an outer tube or receptacle disposed around the bottom portion of the central tube terminating in a smaller section which is concentric with and spaced directly below the section of the central tube; a side arm connecting the side tube and the outer tube; and furnaces around the side, outer, and the reduced sections of the central and the outer tubes. The process includes the steps of disposing a solid core glass rod at a point removed from hot temperature that can cause crystallization in the core glass rod, disposing a solid clad glass rod at a point removed from the core glass rod, softening to the flowing condition the solid clad glass rod, transferring the softened clad glass to a lower point, the softened clad glass having a central void therethrough, heating the softened clad glass above its crystallization temperature, cooling the softened clad glass to a draw temperature, transferring the solid core glass rod into the central void in the softened clad glass, softening to the flowing condition the solid core glass rod with the heat from the softened and cooled clad glass, and drawing the core/clad glass fiber by allowing the clad and core glasses to flow in the form of a fiber.
摘要翻译：本发明涉及制造芯/复合玻璃纤维的装置和方法。该设备包括中央管或插座，其在顶部连接到压力控制器并终止于减小的部分; 位于中心管的上部的高度的侧管或容器; 设置在中心管的底部周围的外管或容器，其终止于与中心管的截面同心并间隔开的较小部分; 连接侧管和外管的侧臂; 并围绕中心管和外管的侧面，外部和还原部分进行熔炼。该方法包括以下步骤：将固体芯玻璃棒放置在可以在芯玻璃棒中引起结晶的热温度的点处，将固体包覆玻璃棒设置在从芯玻璃棒上移除的点上，软化成流动条件固体包覆玻璃棒，将软化的包覆玻璃转移到较低点，软化的复合玻璃具有中空空隙，将软化的包覆玻璃加热到其结晶温度以上，将软化的包覆玻璃冷却至拉伸温度，将固体核将玻璃棒插入软化的包层玻璃中的中心空隙中，使来自软化和冷却的包覆玻璃的热量将固体芯玻璃棒软化成流动状态，并且通过使包层和芯玻璃流动以纤维的形式。

3. 发明授权

US07563480B1 Method for fluoride salt coated magnesium aluminate 有权
标题翻译：氟化盐涂覆的铝酸镁的方法
公开(公告)号：US07563480B1
公开(公告)日：2009-07-21
申请号：US11532572
申请日：2006-09-18
申请人： Guillermo R. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal
发明人： Guillermo R. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal
IPC分类号： B05D7/00 , B05D1/18 , B05D3/02
CPC分类号： C04B35/443 , B82Y30/00 , C04B35/62655 , C04B35/62828 , C04B35/62886 , C04B35/62897 , C04B35/645 , C04B2235/3203 , C04B2235/3217 , C04B2235/445 , C04B2235/5436 , C04B2235/5454 , C04B2235/6562 , C04B2235/6581 , C04B2235/72 , C04B2235/721 , C04B2235/77 , C04B2235/9653 , Y10T428/2991 , Y10T428/2993
摘要： A particle having a magnesium aluminate core and a fluoride salt coating on the core. The particle has been heated in an oxidizing atmosphere to a temperature in the range of about 400° C. to about 750° C. A method of making a particle by mixing a magnesium aluminate core with a solution of a fluoride salt in a solvent to form a slurry and spraying the slurry into a drying column. The slurry enters the column as an aerosol under thermal conditions that avoid boiling the solvent. The thermal conditions in the column evaporate the solvent as the aerosol moves through the column to form a coating of the fluoride salt on the core while substantially avoiding spalling.
摘要翻译：在芯上具有铝酸镁芯和氟化物盐涂层的颗粒。将颗粒在氧化气氛中加热到约400℃至约750℃的温度。一种通过将铝酸镁芯与氟化物盐在溶剂中的溶液混合制备颗粒的方法，形成浆料并将浆料喷雾到干燥塔中。在避免沸腾溶剂的热条件下，浆料作为气溶胶进入塔中。当气溶胶移动通过柱子时，塔中的热条件蒸发溶剂，以形成核心上的氟化物盐的涂层，同时基本上避免剥落。

4. 发明申请

US20060217260A1 Magnesium aluminate transparent ceramic having low scattering and absorption loss 有权
公开(公告)号：US20060217260A1
公开(公告)日：2006-09-28
申请号：US11094545
申请日：2005-03-24
申请人： Guillermo Villalobos , Jasbinder Sanghera , Shyam Bayya , Ishwar Aggarwal
发明人： Guillermo Villalobos , Jasbinder Sanghera , Shyam Bayya , Ishwar Aggarwal
IPC分类号： C04B35/443 , C04B35/64
CPC分类号： C04B35/443 , C04B35/62655 , C04B35/62828 , C04B35/62886 , C04B35/645 , C04B2235/3203 , C04B2235/444 , C04B2235/445 , C04B2235/5436 , C04B2235/72 , C04B2235/721 , C04B2235/9653
摘要： A ceramic having at least about 90% by weight magnesium aluminate and having a bulk scattering and absorption loss of less than about 1/cm at any wavelength in a range of about 0.23 to about 5.3 microns or 0.2/cm at any wavelength in a range of about 0.27 to about 4.5 microns. A method of making a ceramic by providing a plurality of particles having a magnesium aluminate core and a fluoride salt coating; heating the particles in an oxidizing atmosphere to a temperature in the range of about 400° C. to about 750° C.; and sintering the particles to form a solid ceramic.

5. 发明申请

US20070087204A1 Low loss visible-IR transmitting glass-ceramic spinel composites and process 有权
标题翻译：低损耗可见红外透射玻璃陶瓷尖晶石复合材料及工艺
公开(公告)号：US20070087204A1
公开(公告)日：2007-04-19
申请号：US11250697
申请日：2005-10-13
申请人： Shyam Bayya , Jasbinder Sanghera , Guillermo Villalobos , Geoffrey Chin , Ishwar Aggarwal
发明人： Shyam Bayya , Jasbinder Sanghera , Guillermo Villalobos , Geoffrey Chin , Ishwar Aggarwal
IPC分类号： B32B17/06
CPC分类号： C03C3/253 , C03C17/00 , C04B35/443 , C04B35/6455 , C04B37/04 , C04B37/042 , C04B37/045 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6581 , C04B2235/662 , C04B2235/77 , C04B2235/94 , C04B2235/96 , C04B2235/9607 , C04B2235/9653 , C04B2237/10 , C04B2237/125 , C04B2237/343 , C04B2237/52 , C04B2237/70 , C04B2237/704 , C04B2237/76 , C04B2237/78
摘要： This invention pertains to a composite of Spinel and BGG glass substrates and to process for bonding Spinel to BGG glass. The composite includes a Spinel and a BGG glass bonded together and having transmission in the visible and mid-infrared wavelength region. The process includes the step of heating them together above the softening temperature of the BGG glass, the composite having excellent, i.e., typically in excess of about 80%, transmission in the 0.5-5 wavelength region.
摘要翻译：本发明涉及尖晶石和BGG玻璃基板的复合材料，并且涉及将尖晶石与BGG玻璃结合的工艺。复合材料包括粘合在一起并在可见光和中红外波长区域具有透射的尖晶石和BGG玻璃。该方法包括将它们加热到高于BGG玻璃的软化温度的步骤，该复合材料在0.5-5波长范围内具有优异的，即通常超过约80％的透射率。

6. 发明申请

US20060024436A1 Method for coating small particles 审中-公开
标题翻译：涂布小颗粒的方法
公开(公告)号：US20060024436A1
公开(公告)日：2006-02-02
申请号：US11239433
申请日：2005-09-20
申请人： Shyam Bayya , Guillermo Villalobos , Jasbinder Sanghera , Ishwar Aggarwal
发明人： Shyam Bayya , Guillermo Villalobos , Jasbinder Sanghera , Ishwar Aggarwal
IPC分类号： B05D7/00
CPC分类号： C09K11/02 , B01J2/006 , B01J2/04 , C09K11/584
摘要： The coating method includes the steps of dissolving coating precursor(s) in a solvent to form a precursor solution: adding with mixing a miscible diluent to the precursor solution to form a coating solution; admixing solid particles to the coating solution to form a coating slurry, with the particles surrounded with the coating solution; spraying the coating slurry to form droplets containing at least one particle; passing the droplets through a drying zone where the droplets are dried and form dry particles coated with a coating material formed from the coating precursor(s); heat-treating the coating material on the particles emanating from the drying zone to remove volatile matter on the coating material, to improve integrity of the coating material and/or to effect another objective; and collecting dry coated particles.
摘要翻译：涂布方法包括以下步骤：将涂覆前体溶解在溶剂中以形成前体溶液：将可混溶的稀释剂与前体溶液混合形成涂布溶液; 将固体颗粒混合到涂布溶液中以形成涂覆浆料，其中颗粒被涂布溶液包围; 喷涂涂料浆料以形成含有至少一个颗粒的液滴; 使液滴通过干燥区域，其中液滴被干燥并形成涂覆有由涂层前体形成的涂层材料的干燥颗粒; 对从干燥区发出的颗粒上的涂层材料进行热处理以除去涂层材料上的挥发物质，以改善涂层材料的完整性和/或实现另一目的; 并收集干涂层颗粒。

7. 发明申请

US20050159289A1 Optical transmission of BGG glass material 失效
标题翻译： BGG玻璃材料的透光
公开(公告)号：US20050159289A1
公开(公告)日：2005-07-21
申请号：US10758750
申请日：2004-01-15
申请人： Shyam Bayya , Jasbinder Sanghera , Ishwar Aggarwal
发明人： Shyam Bayya , Jasbinder Sanghera , Ishwar Aggarwal
IPC分类号： C03C3/23 , C03C3/253
CPC分类号： C03C3/253 , C03C3/23
摘要： This invention pertains to a BGG glass material with excellent optical and mechanical properties and to a method for its preparation characterized by the use of a halogen component. The BGG glass material is essentially devoid of water, has excellent optical transmission in the visible and mid-infrared wavelength range, and can be easily molded in small and large sizes and complex shapes at a low cost.
摘要翻译：本发明涉及具有优异的光学和机械性能的BGG玻璃材料及其制备方法，其特征在于使用卤素组分。 BGG玻璃材料基本上没有水，在可见光和中红外波长范围内具有优异的光学透射率，并且可以以低成本容易地以小尺寸和大尺寸和复杂形状模制。

8. 发明授权

US07528086B2 Magnesium aluminate transparent ceramic having low scattering and absorption loss 有权
标题翻译：铝酸铝透明陶瓷具有低散射和吸收损失
公开(公告)号：US07528086B2
公开(公告)日：2009-05-05
申请号：US11094545
申请日：2005-03-24
申请人： Guillermo E. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal
发明人： Guillermo E. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal
IPC分类号： C04B35/04 , C04B35/03
CPC分类号： C04B35/443 , C04B35/62655 , C04B35/62828 , C04B35/62886 , C04B35/645 , C04B2235/3203 , C04B2235/444 , C04B2235/445 , C04B2235/5436 , C04B2235/72 , C04B2235/721 , C04B2235/9653
摘要： A ceramic having at least about 90% by weight magnesium aluminate and having a bulk scattering and absorption loss of less than about 1/cm at any wavelength in a range of about 0.23 to about 5.3 microns or 0.2/cm at any wavelength in a range of about 0.27 to about 4.5 microns. A method of making a ceramic by providing a plurality of particles having a magnesium aluminate core and a fluoride salt coating; heating the particles in an oxidizing atmosphere to a temperature in the range of about 400° C. to about 750° C.; and sintering the particles to form a solid ceramic.
摘要翻译：一种陶瓷，其具有至少约90重量％的铝酸镁，并且在任何波长范围内，在任何波长范围内，在约0.23至约5.3微米或0.2 /厘米范围内的体积散射和吸收损失小于约1 / 为约0.27至约4.5微米。一种通过提供多个具有铝酸镁芯和氟化物盐涂层的颗粒来制造陶瓷的方法; 将氧化气氛中的颗粒加热至约400℃至约750℃的温度; 并烧结颗粒以形成固体陶瓷。

9. 发明授权

US07211325B2 Fluoride salt coated magnesium aluminate 有权
标题翻译：氟化铝包覆的铝酸镁
公开(公告)号：US07211325B2
公开(公告)日：2007-05-01
申请号：US11094544
申请日：2005-03-24
申请人： Guollermo R. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal
发明人： Guollermo R. Villalobos , Jasbinder S. Sanghera , Shyam Bayya , Ishwar D. Aggarwal
IPC分类号： B32B5/16
CPC分类号： C04B35/443 , B82Y30/00 , C04B35/62655 , C04B35/62828 , C04B35/62886 , C04B35/62897 , C04B35/645 , C04B2235/3203 , C04B2235/3217 , C04B2235/445 , C04B2235/5436 , C04B2235/5454 , C04B2235/6562 , C04B2235/6581 , C04B2235/72 , C04B2235/721 , C04B2235/77 , C04B2235/9653 , Y10T428/2991 , Y10T428/2993
摘要： A particle having a magnesium aluminate core and a fluoride salt coating on the core. The particle has been heated in an oxidizing atmosphere to a temperature in the range of about 400° C. to about 750° C. A method of making a particle by mixing a magnesium aluminate core with a solution of a fluoride salt in a solvent to form a slurry and spraying the slurry into a drying column. The slurry enters the column as an aerosol under thermal conditions that avoid boiling the solvent. The thermal conditions in the column evaporate the solvent as the aerosol moves through the column to form a coating of the fluoride salt on the core while substantially avoiding spalling.
摘要翻译：在芯上具有铝酸镁芯和氟化物盐涂层的颗粒。将颗粒在氧化气氛中加热到约400℃至约750℃的温度。一种通过将铝酸镁芯与氟化物盐在溶剂中的溶液混合制备颗粒的方法，形成浆料并将浆料喷雾到干燥塔中。在避免沸腾溶剂的热条件下，浆料作为气溶胶进入塔中。当气溶胶移动通过柱子时，塔中的热条件蒸发溶剂，以形成核心上的氟化物盐的涂层，同时基本上避免剥落。

10. 发明申请

US20070087203A1 Low loss visible-IR transmitting glass-aluminum oxynitride composites and process 有权
标题翻译：低损耗可见红外透射玻璃 - 氮氧化铝复合材料及工艺
公开(公告)号：US20070087203A1
公开(公告)日：2007-04-19
申请号：US11250696
申请日：2005-10-13
申请人： Shyam Bayya , Jasbinder Sanghera , Guillermo Villalobos , Geoffrey Chin , Ishwar Aggarwal
发明人： Shyam Bayya , Jasbinder Sanghera , Guillermo Villalobos , Geoffrey Chin , Ishwar Aggarwal
IPC分类号： B32B17/06
CPC分类号： C03C3/253 , B32B2315/02 , C03C17/00 , C04B35/581 , C04B35/6455 , C04B37/005 , C04B37/04 , C04B37/042 , C04B37/045 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6581 , C04B2235/662 , C04B2235/77 , C04B2235/94 , C04B2235/96 , C04B2235/9607 , C04B2235/9653 , C04B2237/10 , C04B2237/125 , C04B2237/366 , C04B2237/52 , C04B2237/592 , C04B2237/70 , C04B2237/704 , C04B2237/76 , C04B2237/78
摘要： This invention pertains to a composite of AlON and a germanate glass, and to a process for bonding AlON to the glass. The composite includes AlON and glass bonded together and having transmission in the visible and mid-infrared wavelength region. The process includes the step of heating them together above the softening temperature of the glass, the composite having excellent, i.e., typically in excess of about 60%, transmission in the 0.4-5 wavelength region.
摘要翻译：本发明涉及AlON和锗酸盐玻璃的复合物，以及将AlON与玻璃结合的方法。该复合材料包括AlON和玻璃结合在一起并且在可见光和中红外波长区域具有透射。该方法包括将它们一起加热到高于玻璃的软化温度的步骤，该复合材料在0.4-5波长区域具有优异的，即通常超过约60％的透射率。

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