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1. 发明授权

US5068327A Symmetrical dioxazine compounds and their use as fiber-reactive dyes 失效
标题翻译：对称二恶唑化合物及其作为纤维反应性染料的使用
公开(公告)号：US5068327A
公开(公告)日：1991-11-26
申请号：US448644
申请日：1989-12-11
申请人： Tetsuya Miyamoto , Miyao Takahashi , Takahiko Fujisaki , Shinei Ikeou , Takashi Omura
发明人： Tetsuya Miyamoto , Miyao Takahashi , Takahiko Fujisaki , Shinei Ikeou , Takashi Omura
IPC分类号： C09B62/44 , C09B62/503
CPC分类号： C09B62/4405 , C09B62/5033
摘要： A dioxazine compound represented by the following formula (I) in the free acid form, ##STR1## wherein V is a direct linkage or ##STR2## in which R.sub.3 is hydrogen or unsubstituted or substituted alkyl, and X is a direct linkage or an aliphatic, araliphatic or aromatic bridging group, provided that X stands for the bridging group as defined hereinabove when V is ##STR3## Y is unsubstituted or substituted phenylene, or unsubstituted or substituted naphthylene, Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.1 in which Z.sub.1 is a group capable of being split by the action of an alkali, Q is sulfo, hydroxy, halo, alkoxy, unsubstituted or substituted phenoxy or unsubstituted or substituted amino, and R.sub.1 and R.sub.2 independently of one another are each hydrogen or unsubstituted or substituted alkyl, which is useful for dyeing or printing fiber materials to give a dyed or printed product of a blue color superior in fastness properties, particularly those such as chlorine fastness, with superior build-up property.

2. 发明授权

US4780104A Reactive dye-containing aqueous liquid composition 失效
标题翻译：含活性染料的含水液体组合物
公开(公告)号：US4780104A
公开(公告)日：1988-10-25
申请号：US17054
申请日：1987-02-20
申请人： Noriaki Yamauchi , Kunihiko Imada , Shinei Ikeou
发明人： Noriaki Yamauchi , Kunihiko Imada , Shinei Ikeou
IPC分类号： C09B62/44 , C09B67/26 , D06P1/38
CPC分类号： C09B67/0073 , C09B62/4403 , D06P1/38 , Y10S8/917 , Y10S8/918 , Y10S8/919 , Y10S8/924
摘要： An aqueous liquid dye composition comprising 5 to 50% by weight of a reactive dye represented by the following formula, ##STR1## wherein D denotes a sulfo group-containing organic dye residue, R.sub.1 and R.sub.2 independently of one another denote a hydrogen atom or a C.sub.1 to C.sub.4 alkyl group unsubstituted or substituted with a halogen atom or a hydroxyl, cyano, C.sub.1 to C.sub.4 alkoxy, carboxy, carbamoyl, C.sub.1 to C.sub.4 alkoxycarbonyl, C.sub.1 to C.sub.4 alkylcarbonyloxy, sulfo or sulfamoyl group, A denotes a phenylene group unsubstituted or substituted with one or two members selected from methyl, ethyl, methoxy, ethoxy, chlorine, bromine and sulfo, or a naphthylene group unsubstituted or substituted with one sulfo group, X denotes a halogen atom, and Y is a group of --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z in which Z is a splittable group by the action of an alkali, 0.1 to 10% by weight of .epsilon.-caprolactam and the balance of water, the composition having a pH value of 3 to 7, which can be stored for a long period of time at a low temperature such as 5.degree. C. or lower without deterioration in its solution state.
摘要翻译：一种水性液体染料组合物，其包含5至50重量％的由下式表示的活性染料，其中D表示含磺基的有机染料残基，R 1和R 2彼此独立地表示氢原子或未取代或被卤素原子或羟基取代的C1至C4烷基，氰基，C1至C4烷氧基，羧基，氨基甲酰基，C1至C4烷氧基羰基，C1至C4烷基羰基氧基，磺基或氨磺酰基，A表示亚苯基未被取代或取代其中一个或两个选自甲基，乙基，甲氧基，乙氧基，氯，溴和磺基，或未被取代或被一个磺基取代的亚萘基，X表示卤素原子，Y是-SO 2 CH = CH 2或 -SO 2 CH 2 CH 2 Z，其中Z为可裂解基团，其为碱，0.1至10重量％的ε-己内酰胺，余量为水，该组合物的pH值为3至7，可长期储存一段时间在低点温度如5℃以下，其溶液状态不劣化。

3. 发明授权

US5438137A Fiber reactive asymmetric dioxazine compounds and their use as fiber reactive dyes 失效
标题翻译：纤维反应性不对称二嗪化合物及其作为纤维活性染料的用途
公开(公告)号：US5438137A
公开(公告)日：1995-08-01
申请号：US128725
申请日：1993-09-30
申请人： Tetsuya Miyamoto , Miyao Takahashi , Takahiko Fujisaki , Shinei Ikeou , Takashi Omura , Naoki Harada
发明人： Tetsuya Miyamoto , Miyao Takahashi , Takahiko Fujisaki , Shinei Ikeou , Takashi Omura , Naoki Harada
IPC分类号： C09B62/44 , C09B62/503 , C07D498/04
CPC分类号： C09B62/5033 , C09B62/4405
摘要： An asymmetric dioxazine compound of the following formula in the free acid form, ##STR1## wherein R is hydrogen, halogen, sulfo or alkoxy, R.sub.1, R.sub.2 and R.sub.3 are each hydrogen or alkyl, X.sub.1 and X.sub.2 are each hydrogen, halogen, alkyl, alkoxy or phenoxy, Y is alkylene, phenylene or naphthylene, Z is --SO.sub.2 CH.dbd.CH.sub.2, --SO.sub.2 CH.sub.2 CH.sub.2 OSO.sub.3 H or the like, V is hydrogen, alkyl, acyl or substituted triazinyl, and Q is halogen, alkoxy, amino or a group similar to that of ##STR2## provided that R is hydrogen, and Q is amino or a group similar to that of ##STR3## when V is substituted triazinyl, which is useful for dyeing or printing fiber materials to give dyed or printed products of a brilliant blue color superior in fastness properties, particularly those such as chlorine fastness with superior build-up property.
摘要翻译：游离酸形式的下式的不对称二恶嗪化合物，其中R是氢，卤素，磺基或烷氧基，R 1，R 2和R 3各自为氢或烷基，X 1和X 2各自为氢，卤素，烷基，烷氧基或苯氧基，Y是亚烷基，亚苯基或亚萘基，Z是-SO2CH = CH2，-SO2CH2CH2OSO3H等，V是氢，烷基，酰基或取代的三嗪基，Q是卤素，烷氧基，氨基或类似的基团条件是R为氢，Q为氨基或V为与IMA相似的基团，当V为取代的三嗪基时，可用于染色或印刷纤维材料以得到亮蓝色的染色或印刷产品耐牢度特性优异，特别是具有优异聚集性能的耐氯牢度。

4. 发明授权

US5077416A Benzodifuranone compounds useful for dyeing or printing hydrophobic fiber materials and process for their production 失效
标题翻译：用于染色或印刷疏水性纤维材料的苯并二酮化合物及其生产方法
公开(公告)号：US5077416A
公开(公告)日：1991-12-31
申请号：US408064
申请日：1989-09-15
申请人： Yasuyoshi Ueda , Jun Yamamoto , Takashi Omura , Hideo Hattori , Shinei Ikeou , Yosuke Yamamoto
发明人： Yasuyoshi Ueda , Jun Yamamoto , Takashi Omura , Hideo Hattori , Shinei Ikeou , Yosuke Yamamoto
IPC分类号： C07D493/04 , C09B57/00
CPC分类号： C07D493/04 , C09B57/00
摘要： A heterocyclic compound of the formula, ##STR1## wherein A and B are each hydrogen, alkyl or alkoxy, Y is hydrogen, alkyl, alkoxy or --O--R.sup.2 --X--R.sup.1, or Y and B are taken together with each other to form methylenedioxy, R.sup.1 is alkyl, phenyl or alkenyl, R.sup.2 is unsubstituted or substituted alkylene, and X is --O--, --S--, --SO--, --SO.sub.2 -- or ##STR2## in which R.sup.3 is hydrogen or alkyl, with the proviso that R.sup.1 is C.sub.3 or C.sub.4 alkyl or alkenyl, or C.sub.1 -C.sub.4 alkyl when R.sup.2 is unsubstituted ethylene or propylene, respectively, X is --O-- or --S--, and Y and B don't form methylenedioxy, which is useful for dyeing or printing hydrophobic fiber materials with superior dyeability to give a dyed or printed product of a red color excellent in fastness properties, particularly those such as washing fastness.
摘要翻译：下式的杂环化合物，其中A和B各自为氢，烷基或烷氧基，Y为氢，烷基，烷氧基或-O-R2-X-R1，或Y和B为一起彼此形成亚甲二氧基，R1是烷基，苯基或烯基，R2是未取代或取代的亚烷基，X是-O - ， - S - ， - SO-，-SO2-或者其中R3是氢或烷基，条件是当R 2为未取代的乙烯或丙烯时，R 1为C 3或C 4烷基或链烯基或C 1 -C 4烷基，X为-O-或-S-，并且Y和B不形成亚甲二氧基可用于染色或印刷具有优异染色性的疏水性纤维材料，得到耐光性优异的红色染色或印刷品，特别是耐洗牢度。

5. 发明授权

US4832698A Aqueous liquid composition of vinylsulfone type reactive dyes in lithium salt form and buffer 失效
标题翻译：乙烯砜型活性染料的锂盐形式和缓冲液的液体组合物
公开(公告)号：US4832698A
公开(公告)日：1989-05-23
申请号：US35864
申请日：1987-04-08
申请人： Shinei Ikeou , Takemi Tokieda , Noriaki Yamauchi , Kunihiko Imada , Yutaka Kayane
发明人： Shinei Ikeou , Takemi Tokieda , Noriaki Yamauchi , Kunihiko Imada , Yutaka Kayane
IPC分类号： C09B67/26
CPC分类号： C09B67/0073 , Y10S8/918 , Y10S8/937
摘要： An aqueous liquid dye composition comprising a dye represented by the following formula in a free acid form, ##STR1## wherein Y is --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 X in which X is a group splittable by the action of an alkali, and a pH buffer, the dye being in the form of a lithium salt, and the liquid dye composition having a pH value of from 3 through 7 and a dye content of from 5 through 50% by weight based on the weight of the liquid dye composition, which can be stored stably for a long period of time even at a low temperature such as 0.degree. C. or lower, and a high temperature such as 40.degree. C. or higher.
摘要翻译：一种水性液体染料组合物，其包含游离酸形式的由下式表示的染料，其中Y为-CH = CH 2或-CH 2 CH 2 X，其中X为可通过碱作用而裂解的基团，以及pH缓冲液，染料为锂盐形式，液体染料组合物的pH值为3-7，染料含量为5-50重量％，基于液体染料组合物的重量，其可以即使在0℃以下的低温以及40℃以上的高温下也能够长期稳定地保存。

6. 发明授权

US4740903A Data processing system for chromatography 失效
标题翻译：色谱数据处理系统
公开(公告)号：US4740903A
公开(公告)日：1988-04-26
申请号：US733879
申请日：1985-05-14
申请人： Kiyoharu Nakatsuka , Shinei Ikeou
发明人： Kiyoharu Nakatsuka , Shinei Ikeou
IPC分类号： G01N30/86 , G01N30/62 , G06F17/00 , G06F15/20
CPC分类号： G06K9/00543 , G01N2030/626 , G01N30/8631 , G01N30/8668
摘要： A system for processing chromatographic data which comprises an input for data representative of two chromatograms x and y, a memory for storing the inputted data of the chromatograms, and a computer operative to read out, from the memory, retention times x.sub.i and y.sub.i (i=1, . . . , n; n.gtoreq.2) of at least two principal peaks of the chromatograms, respectively, and derive one function for converting the retention times x.sub.i to y.sub.i using the chromatogram y as the reference chromatogram, which gives a minimum estimated error. The computer is further operative to calculate, on the basis of the derived function, the modified retention time x'.sub.j of all the peaks of the chromatogram x. Therefore, the system permits to eliminate errors orginated from the judgment of a skilled person and to indentify and quantitatively analyze chromatogram obtained precisely without skill.
摘要翻译：一种用于处理色谱数据的系统，其包括用于表示两个色谱图x和y的数据的输入，用于存储色谱图的输入数据的存储器，以及用于从存储器读出保留时间xi和yi（i = 1，...，n，n> / = 2），并且使用色谱图y作为参考色谱，得到一个将保留时间xi转换为yi的函数，其给出最小估计误差。计算机进一步操作以基于导出的函数计算色谱图x的所有峰的修改的保留时间x'j。因此，该系统允许消除由本领域技术人员的判断引起的错误，并且能够准确地并且定量地分析精确获得的没有技术的色谱图。

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