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1. 发明授权

US06992205B2 Process for the production of sulfonic esters 失效
公开(公告)号：US06992205B2
公开(公告)日：2006-01-31
申请号：US10438922
申请日：2003-05-16
申请人： Fumihiko Kano , Shigeki Kunihiro , Noritaka Yoshida , Natsuki Mori
发明人： Fumihiko Kano , Shigeki Kunihiro , Noritaka Yoshida , Natsuki Mori
IPC分类号： C07C303/26
CPC分类号： C07C303/28 , C07D207/12 , C07C309/65 , C07C309/66 , C07C309/73
摘要： Sulfonic acid ester derivatives represented by the general formula (4) or (5) are produced by reacting an amino alcohol derivative represented by the general formula (1) or (2) with an organic sulfonyl halide represented by the general formula (3), in a mixed solvent composed of an aprotic organic solvent and water in the presence of a non-water-prohibiting inorganic base. This procedure can be carried out in a simple, easy, safe and economical manner while reducing the load on the environment. Wherein n represents an integer of 0 to 5, A represents a phenyl group, which may be substituted, R represents a methanesulfonyl, ethanesulfonyl, p-toluenesulfonyl or p-nitrobenzenesulfonyl group and X represents a chloride, bromine or iodine atom.

2. 发明授权

US06864372B2 Process for the production of sulfonic esters 失效
标题翻译：制备磺酸酯的方法
公开(公告)号：US06864372B2
公开(公告)日：2005-03-08
申请号：US10438924
申请日：2003-05-16
申请人： Fumihiko Kano , Shigeki Kunihiro , Noritaka Yoshida , Natsuki Mori
发明人： Fumihiko Kano , Shigeki Kunihiro , Noritaka Yoshida , Natsuki Mori
IPC分类号： C07C303/28 , C07C309/65 , C07C309/66 , C07C309/73 , C07D207/12 , C07D207/24 , C07D211/40 , C07D223/08 , C07D211/06 , C07C303/26
CPC分类号： C07C303/28 , C07D207/12 , C07C309/65 , C07C309/66 , C07C309/73
摘要： Sulfonic acid ester derivatives represented by the general formula (4) or (5) are produced by reacting an amino alcohol derivative represented by the general formula (1) or (2) with an organic sulfonyl halide represented by the general formula (3), in a mixed solvent composed of an aprotic organic solvent and water in the presence of a non-water-prohibiting inorganic base. This procedure can be carried out in a simple, easy, safe and economical manner while reducing the load on the environment. Wherein n represents an integer of 0 to 5, A represents a phenyl group, which may be substituted, R represents a methanesulfonyl, ethanesulfonyl, p-toluenesulfonyl or p-nitrobenzenesulfonyl group and X represents a chloride, bromine or iodine atom.
摘要翻译：由通式（4）或（5）表示的磺酸酯衍生物通过使由通式（1）或（2）表示的氨基醇衍生物与通式（3）表示的有机磺酰卤反应，在由非水性阻止无机碱存在下由非质子有机溶剂和水组成的混合溶剂中。该方法可以简单，容易，安全和经济地进行，同时减少环境负荷。其中n表示0至5的整数，A表示可被取代的苯基，R表示甲磺酰基，乙磺酰基，对甲苯磺酰基或对硝基苯磺酰基，X表示氯，溴或碘原子。

3. 发明授权

US6140527A Process for producing butyric ester derivatives 失效
标题翻译：丁酸衍生物的制备方法
公开(公告)号：US6140527A
公开(公告)日：2000-10-31
申请号：US355529
申请日：1999-09-07
申请人： Shigeki Kunihiro , Fumihiko Kano , Natsuki Mori
发明人： Shigeki Kunihiro , Fumihiko Kano , Natsuki Mori
IPC分类号： C07C253/14 , C07C253/34 , C07C255/20 , C07C253/00
CPC分类号： C07C253/34 , C07C253/14
摘要： This invention has its objects to provide a process for producing a butyric acid ester derivative of the above general formula (2) which is capable of removing various impurity byproducts whose formation cannot be avoided by the prior art technology, particularly the compound of the above general formula (1), with good efficiency.This invention is related to a process for producing a butyric acid ester derivative of the general formula (2) which comprises treating a mixture containing a compound of the following general formula (1) with an addition reagent capable of adding itself to said ethylenic bond to thereby convert said compound of the general formula (1) to an addition product which can be easily separated from said butyric acid ester derivative of the general formula (2) and a process for producing a butyric acid ester derivative of the general formula (2) which comprises reacting a compound of the general formula (3) with a salt of prussic acid by a flow method.HOCH.sub.2 --CH.dbd.CH--COOR (1) ##STR1##
摘要翻译： PCT No.PCT / JP98 / 03686 Sec。 371 1999年9月7日第 102（e）1999年9月7日PCT PCT 1998年8月20日PCT公布。出版物WO99 / 31050 日期1999年6月24日本发明的目的是提供一种上述通式（2）的丁酸酯衍生物的制造方法，其能够除去现有技术中不能避免的各种杂质副产物，特别是上述通式（1）的化合物，效率高。本发明涉及一种制备通式（2）的丁酸酯衍生物的方法，该方法包括用能够将其自身加入所述烯键的加成试剂处理含有下列通式（1）的化合物的混合物从而将所述通式（1）的化合物转化为可以容易地从通式（2）的丁酸酯衍生物分离的加成产物和通式（2）的丁酸酯衍生物的制备方法，其包括通过流动法使通式（3）的化合物与氢氰酸的盐反应。 HOCH2-CH = CH- COOR（1）

4. 发明授权

US06794519B2 Process for the production of sulfonic esters 失效
标题翻译：制备磺酸酯的方法
公开(公告)号：US06794519B2
公开(公告)日：2004-09-21
申请号：US10067784
申请日：2002-02-08
申请人： Fumihiko Kano , Shigeki Kunihiro , Noritaka Yoshida , Natsuki Mori
发明人： Fumihiko Kano , Shigeki Kunihiro , Noritaka Yoshida , Natsuki Mori
IPC分类号： C07D20704
CPC分类号： C07C303/28 , C07D207/12 , C07C309/65 , C07C309/66 , C07C309/73
摘要： Sulfonic acid ester derivatives represented by the general formula (4) or (5) are produced by reacting an amino alcohol derivative represented by the general formula (1) or (2) with an organic sulfonyl halide represented by the general formula (3), in a mixed solvent composed of an aprotic organic solvent and water in the presence of a non-water-prohibiting inorganic base. This procedure can be carried out in a simple, easy, safe and economical manner while reducing the load on the environment. Wherein n represents an integer of 0 to 5, A represents a phenyl group, which may be substituted, R represents a methanesulfonyl, ethanesulfonyl, p-toluenesulfonyl or p-nitrobenzenesulfonyl group and X represents a chloride, bromine or iodine atom.
摘要翻译：由通式（4）或（5）表示的磺酸酯衍生物通过使由通式（1）或（2）表示的氨基醇衍生物与通式（3）表示的有机磺酰卤反应，在由非水性阻止无机碱存在下由非质子有机溶剂和水组成的混合溶剂中。该方法可以简单，容易，安全和经济地进行，同时减少环境负荷。其中n表示0至5的整数，A表示可被取代的苯基，R表示甲磺酰基，乙磺酰基，对甲苯磺酰基或对硝基苯磺酰基，X表示氯，溴或碘原子。

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