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1. 发明授权

US09793564B2 Composite having ion exchange function and preparation method and use thereof 有权
公开(公告)号：US09793564B2
公开(公告)日：2017-10-17
申请号：US14555302
申请日：2014-11-26
申请人： SHANDONG HUAXIA SHENZHOU NEW MATERIAL CO., LTD.
发明人： Yongming Zhang , Junke Tang , Ping Liu , Heng Zhang , Jun Wang
IPC分类号： H01M8/10 , H01M8/1072 , B01D69/14 , B01D71/32 , C08J5/22 , C08J7/16 , H01M8/1023 , H01M8/1039 , H01M8/106 , H01M8/1018
CPC分类号： H01M8/1072 , B01D69/141 , B01D71/32 , C08J5/2275 , C08J5/2281 , C08J5/2293 , C08J7/16 , C08J2379/06 , H01M8/1023 , H01M8/1039 , H01M8/106 , H01M2008/1095 , H01M2250/20 , H01M2300/0082 , Y02E60/521 , Y02P70/56 , Y02T90/32
摘要： A preparation method of composite materials having ion exchange function is provided. The method comprises the following steps: adding a trace of strong protonic acid and/or Lewis acid as a catalyst into the material during compounding, to allow nitrile groups of at least one nitrile group-containing ion exchange resin and nitrile groups of functional monomers grafted on the porous fluoropolymer membrane to form a triazine ring crosslinked structure.

2. 发明公开

EP2583747A1 FLUORINE CONTAINING IONOMER COMPOSITE WITH ION EXCHANGE FUNCTION, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：含离子交换功能的含氟离聚物复合材料及其制备方法和用途
公开(公告)号：EP2583747A1
公开(公告)日：2013-04-24
申请号：EP10853048.6
申请日：2010-06-18
申请人： Shandong Huaxia Shenzhou New Material Co., Ltd.
发明人： ZHANG, Yongming , TANG, Junke , LIU, Ping , ZHANG, Heng , WANG, Jun
IPC分类号： B01D71/32 , B01D67/00 , H01M8/02 , C08J5/22 , C08L27/18
CPC分类号： H01M8/1041 , B01D69/10 , B01D69/141 , B01D71/32 , B01D2323/30 , B01D2325/42 , C08J5/2281 , C08J2327/18 , C08K9/04 , D06M14/28 , H01M8/1023 , H01M8/1039 , H01M8/106 , H01M8/1072 , Y02E60/521 , Y02P70/56
摘要： Provided is a composite which is comprised of one or more ion exchange resin(s) and fluorine containing polymer fiber, wherein the fiber and the film-forming resin form a triazine-ring crosslinked structure, so that the film prepared from the composite is of good airtightness and stability, as well as high ion exchange capacity and high conductivity. The preparation method of the composite, the product prepared from this composite and the use thereof are also provided.
摘要翻译：本发明提供一种由一种或多种离子交换树脂和含氟聚合物纤维构成的复合物，其中纤维和成膜树脂形成三嗪环交联结构，从而由该复合物制备的膜为良好的气密性和稳定性，以及高离子交换容量和高导电性。还提供了该复合材料的制备方法，由该复合材料制备的产品及其用途。

3. 发明公开

EP2514773A4 HIGH EXCHANGE CAPACITY PERFLUORINATED ION EXCHANGE RESIN, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：与交换容量高，方法和用途的全氟化离子交换树脂
公开(公告)号：EP2514773A4
公开(公告)日：2013-07-17
申请号：EP09852156
申请日：2009-12-15
申请人： SHANDONG HUAXIA SHENZHOU NEW MATERIAL CO LTD
发明人： ZHANG YONGMING , ZHANG HENG , QIN SHENG , GAO ZIHONG , WANG LI , LI YONG , SONG XUEZHANG
IPC分类号： C08F214/26
CPC分类号： C08F214/265 , C08F214/26 , C08F214/262 , C08F214/267 , C08J5/2243 , C08J2327/12 , H01M8/1023 , H01M8/1039 , H01M2008/1095 , Y02E60/522

4. 发明授权

EP2584627B1 COMPOSITE HAVING ION EXCHANGE FUNCTION AND PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：复合离子交换功能与方法和用途
公开(公告)号：EP2584627B1
公开(公告)日：2016-10-05
申请号：EP10853043.7
申请日：2010-06-18
申请人： Shandong Huaxia Shenzhou New Material Co., Ltd.
发明人： ZHANG, Yongming , TANG, Junke , LIU, Ping , ZHANG, Heng , WANG, Jun
IPC分类号： H01M2/16 , H01M2/14 , B01D71/32 , H01M8/10 , H01M8/02 , C08J5/18 , C08J7/12 , C08J7/18 , C08J5/22
CPC分类号： H01M8/1072 , B01D69/141 , B01D71/32 , C08J5/2275 , C08J5/2281 , C08J5/2293 , C08J7/16 , C08J2379/06 , H01M8/1023 , H01M8/1039 , H01M8/106 , H01M2008/1095 , H01M2250/20 , H01M2300/0082 , Y02E60/521 , Y02P70/56 , Y02T90/32
摘要： A composite having ion exchange function, preparation method and use thereof are provided. The composite is formed by compounding ion exchange resin with fluorine-containing polymer porous membrane, wherein the nitrile groups in the ion exchange resin react with the nitrile groups grafted on the fluorine-contained polymer porous membrane to form triazine ring crosslinked structure. The composite has excellent mechanical property and gas impermeability, high ion exchange capacity and high electroconductivity.

5. 发明公开

EP2511311A4 PERFLUORINATED ION EXCHANGE RESIN, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：全氟离子交换树脂，方法和用途
公开(公告)号：EP2511311A4
公开(公告)日：2013-05-08
申请号：EP09851961
申请日：2009-12-11
申请人： SHANDONG HUAXIA SHENZHOU NEW MATERIAL CO LTD
发明人： ZHANG YONGMING , QIN SHENG , GAO ZIHONG , ZHANG HENG , WEI MAOXIANG , LI YONG , WANG JUN
IPC分类号： C08F214/26 , B01J39/00 , C08F2/22 , C08F214/18 , C08F216/14 , C08F228/02 , C08J5/22
CPC分类号： C08F214/184 , B01J39/20 , C08F214/262 , C08F216/1466 , C08J5/2237 , C08J2327/18 , H01M8/1023 , H01M8/1072 , Y02E60/521 , Y02P70/56
摘要： The present invention provides a perfluorinated ion exchange resin, whose structural formula is shown in formula M. The present invention also provides preparation method of the perfluorinated ion exchange resin, comprising subjecting tetrafluoroethylene monomers and two kinds of sulfonyl fluoride-containing vinyl ether monomers in the presence of initiator to ternary copolymerization. The perfluorinated ion exchange resin provided in accordance with the present invention can fulfill the requirements of mechanical strength and ion exchange capacity at the same time and has good thermal stability.

6. 发明授权

EP2583746B1 FLUORINE CONTAINING IONOMER COMPOSITE WITH ION EXCHANGE FUNCTION, PREPARATION METHOD AND USE THEREOF 有权转让
公开(公告)号：EP2583746B1
公开(公告)日：2019-01-09
申请号：EP10853047.8
申请日：2010-06-18
申请人： Shandong Huaxia Shenzhou New Material Co., Ltd.
发明人： ZHANG, Yongming , TANG, Junke , LIU, Ping , ZHANG, Heng , WANG, Jun
IPC分类号： B01D71/32 , B01D67/00 , H01M8/02 , C08J5/22

7. 发明公开

EP2583746A4 FLUORINE CONTAINING IONOMER COMPOSITE WITH ION EXCHANGE FUNCTION, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：荧光离子化合物与离子交换功能，制造方法及其用途
公开(公告)号：EP2583746A4
公开(公告)日：2014-01-08
申请号：EP10853047
申请日：2010-06-18
申请人： SHANDONG HUAXIA SHENZHOU NEW MATERIAL CO LTD
发明人： ZHANG YONGMING , TANG JUNKE , LIU PING , ZHANG HENG , WANG JUN
IPC分类号： B01D71/32 , B01D67/00 , C08J5/22 , H01M8/02
CPC分类号： H01M8/1048 , B01D69/10 , B01D69/141 , B01D71/32 , B01D71/82 , B01D2323/30 , B01D2325/42 , C08J5/2281 , C08J5/2293 , C08J2327/18 , H01M8/1023 , H01M8/1039 , H01M8/1044 , H01M8/106 , H01M8/1072 , H01M2008/1095 , H01M2300/0082 , Y02E60/523 , Y02P70/56
摘要： Provided is a composite which is comprised of one or more ion exchange resin(s) and a porous fluorine containing polymer membrane (2), wherein the porous membrane and the resin form a carbon-chain crosslinked structure, so that the film prepared from the composite is of good airtightness and stability, as well as high ion exchange capacity and high conductivity. The preparation method of the composite, the product prepared from this composite and the application thereof are also provided.

8. 发明授权

EP2511311B1 PERFLUORINATED ION EXCHANGE RESIN, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：全氟离子交换树脂，其制备方法和用途
公开(公告)号：EP2511311B1
公开(公告)日：2013-11-27
申请号：EP09851961.4
申请日：2009-12-11
申请人： Shandong Huaxia Shenzhou New Material Co., Ltd.
发明人： ZHANG, Yongming , QIN, Sheng , GAO, Zihong , ZHANG, Heng , WEI, Maoxiang , LI, Yong , WANG, Jun
IPC分类号： C08F214/26 , C08F214/18 , C08F228/02 , C08F2/22 , B01J39/00 , C08F216/14 , C08J5/22 , B01J39/20 , H01M8/10
CPC分类号： C08F214/184 , B01J39/20 , C08F214/262 , C08F216/1466 , C08J5/2237 , C08J2327/18 , H01M8/1023 , H01M8/1072 , Y02E60/521 , Y02P70/56
摘要： The present invention provides a perfluorinated ion exchange resin, whose structural formula is shown in formula M. The present invention also provides preparation method of the perfluorinated ion exchange resin, comprising subjecting tetrafluoroethylene monomers and two kinds of sulfonyl fluoride-containing vinyl ether monomers in the presence of initiator to ternary copolymerization. The perfluorinated ion exchange resin provided in accordance with the present invention can fulfill the requirements of mechanical strength and ion exchange capacity at the same time and has good thermal stability.
摘要翻译：本发明提供了一种全氟离子交换树脂，其结构式如式M所示。本发明还提供了全氟离子交换树脂的制备方法，包括将四氟乙烯单体和两种含磺酰氟的乙烯基醚单体在三元共聚引发剂的存在。本发明提供的全氟离子交换树脂可以同时满足机械强度和离子交换能力的要求，具有良好的热稳定性。

9. 发明公开

EP2514773A1 HIGH EXCHANGE CAPACITY PERFLUORINATED ION EXCHANGE RESIN, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：与交换容量高，方法和用途的全氟化离子交换树脂
公开(公告)号：EP2514773A1
公开(公告)日：2012-10-24
申请号：EP09852156.0
申请日：2009-12-15
申请人： Shandong Huaxia Shenzhou New Material Co., Ltd.
发明人： ZHANG, Yongming , ZHANG, Heng , QIN, Sheng , GAO, Zihong , WANG, Li , LI, Yong , SONG, Xuezhang
IPC分类号： C08F214/26
CPC分类号： C08F214/265 , C08F214/26 , C08F214/262 , C08F214/267 , C08J5/2243 , C08J2327/12 , H01M8/1023 , H01M8/1039 , H01M2008/1095 , Y02E60/522
摘要： The present invention provides a high exchange capacity perfluorinated resin comprising two kinds of sulfonyl fluoride-containing short pendant groups of different structures, which is prepared by copolymerizing tetrafluoroethylene, vinyl ether monomers comprising two kinds of sulfonyl fluoride-containing short pendant groups of different structures, and vinyl ether monomer comprising bromine-containing pendant group, wherein based on all monomer units in the copolymer, the mol % of tetrafluoroethylene monomer is 50-85%, the mol % of vinyl ether monomers comprising two kinds of sulfonyl fluoride-containing short pendant groups of different structures is 5-49% and the mol % of vinyl ether monomer comprising bromine-containing pendant group is 1-10%. Perfluorinated ion exchanges membrane prepared from such perfluorinated resin have resistance to various chemical media, high ion exchange capacity, high conductivity, high mechanical strength, high size stability, low membrane electrical resistance and long service life, and may be applied in fuel cells or high-temperature fuel cells.
摘要翻译：本发明提供一交换容量高的全氟化树脂，其包含2种不同结构的磺酰含氟化物的短侧基，所有这些制备通过共聚四氟乙烯，乙烯基醚单体包括2种不同结构的磺酰含氟化物的短侧基，和worin基于共聚物的全部单体单元的乙烯基醚单体，其包含含溴的侧基，四氟乙烯单体的摩尔％是50-85％时，摩尔％乙烯基醚单体包括2种磺酰氟化含短侧链不同结构的基团是5-49％和乙烯基醚单体的摩尔％的包含含溴的侧基是1-10％。全氟化的离子交换膜与求的全氟化树脂具有各种化学介质，高离子交换容量，高导电性，高机械强度，高尺寸稳定性，低的膜电阻和长使用寿命性制备，并且可以在燃料电池或高被应用 - 温度的燃料电池。

10. 发明公开

EP2511311A1 PERFLUORINATED ION EXCHANGE RESIN, PREPARATION METHOD AND USE THEREOF 有权转让
标题翻译：全球知识产权保护协会（IONENAUSTAUSCHHARZ），HERSTELLUNGSVERFAHREN UND VERWENDUNG
公开(公告)号：EP2511311A1
公开(公告)日：2012-10-17
申请号：EP09851961.4
申请日：2009-12-11
申请人： Shandong Huaxia Shenzhou New Material Co., Ltd.
发明人： ZHANG, Yongming , QIN, Sheng , GAO, Zihong , ZHANG, Heng , WEI, Maoxiang , LI, Yong , WANG, Jun
IPC分类号： C08F214/26 , C08F214/18 , C08F228/02 , C08F2/22 , B01J39/00
CPC分类号： C08F214/184 , B01J39/20 , C08F214/262 , C08F216/1466 , C08J5/2237 , C08J2327/18 , H01M8/1023 , H01M8/1072 , Y02E60/521 , Y02P70/56
摘要： The present invention provides a perfluorinated ion exchange resin, whose structural formula is shown in formula M. The present invention also provides preparation method of the perfluorinated ion exchange resin, comprising subjecting tetrafluoroethylene monomers and two kinds of sulfonyl fluoride-containing vinyl ether monomers in the presence of initiator to ternary copolymerization. The perfluorinated ion exchange resin provided in accordance with the present invention can fulfill the requirements of mechanical strength and ion exchange capacity at the same time and has good thermal stability.
摘要翻译：本发明提供一种全氟化离子交换树脂，其结构式如式M所示。本发明还提供了全氟化离子交换树脂的制备方法，包括在四氟乙烯单体和两种含磺酰氟的乙烯基醚单体中引发剂存在三元共聚。根据本发明提供的全氟化离子交换树脂可以同时满足机械强度和离子交换容量的要求，并具有良好的热稳定性。

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