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1. 发明授权

US06951899B2 Blend compositions of hard and soft crosslinkable acrylate copolymers 失效
标题翻译：硬和软交联丙烯酸酯共聚物的共混组合物
公开(公告)号：US06951899B2
公开(公告)日：2005-10-04
申请号：US10384373
申请日：2003-03-10
申请人： Seiji Nakagome
发明人： Seiji Nakagome
IPC分类号： C08L33/04 , C08F220/10 , C08J3/00 , C08L33/06
CPC分类号： C08J3/005 , C08J2333/06 , C08L33/06 , C08L2201/52 , C08L2205/02 , C08L2666/04
摘要： To provide a method for producing a blend composition of an acrylic type polymer having an excellent mechanical characteristic as well as a low temperature characteristic, and to provide a blend composition of an acrylic type polymer, and also to provide a blend composition of an acrylic type polymer for sealing materials having an excellent abrasion resistance which is important for sealing materials.To prepare a blend composition of an acrylic type polymer by co-precipitation after mixing (A) an aqueous latex of a copolymer—showing about −10° C. to −65° C. of a glass transition temperature Tg—obtained by emulsion polymerization or suspension polymerization of at least one of an acrylic ester and methacrylic ester with a vinyl monomer containing crosslinking group with (B) an aqueous latex of copolymer—showing about 0° C. of a glass transition temperature Tg or a softening point—obtained by emulsion polymerization or suspension polymerization of at least one of an acrylic ester and methacrylic ester with a vinyl monomer having crosslinking group.
摘要翻译：为了提供具有优异的机械特性和低温特性的丙烯酸类聚合物的共混组合物的制造方法，提供丙烯酸类聚合物的共混组合物，还提供丙烯酸类型的共混组合物用于密封材料的聚合物具有优异的耐磨性，这对于密封材料是重要的。通过在（A）共聚物的水性胶乳（A）表现出约-10℃至-65℃的乳液聚合得到的玻璃化转变温度Tg后，通过共沉淀制备丙烯酸类聚合物的共混组合物或丙烯酸酯和甲基丙烯酸酯中的至少一种与含有交联基团的乙烯基单体的悬浮聚合与（B）共聚物的水性胶乳（约0℃）的玻璃化转变温度Tg或软化点获得的共聚物的水性胶乳丙烯酸酯和甲基丙烯酸酯中的至少一种与具有交联基团的乙烯基单体的乳液聚合或悬浮聚合。

2. 发明授权

US6093853A Phenylenediamine derivative, production method thereof and antioxidant for rubber using it as effective constituent 失效
标题翻译：苯二胺衍生物，其制备方法和使用其作为有效成分的橡胶的抗氧化剂
公开(公告)号：US6093853A
公开(公告)日：2000-07-25
申请号：US106457
申请日：1998-06-30
申请人： Seiji Nakagome , Akihiko Toda
发明人： Seiji Nakagome , Akihiko Toda
IPC分类号： C07C211/55 , C07C217/80 , C07C225/22 , C07C255/56 , C08K5/18 , C07C211/00
CPC分类号： C07C255/56 , C07C211/55 , C07C217/80 , C07C225/22 , C08K5/18
摘要： A phenylenediamine derivative represented by following formula (I) or (II): ##STR1## wherein R.sub.1 and R.sub.2 each represents a hydrogen atom, a lower alkyl group, or a lower alkoxy group; R.sub.3 represents a hydrogen atom or a methyl group; R.sub.4 represents a methyl group or an ethyl group; and n and m each is 1, 2, or 3; ##STR2## wherein R.sub.1 and R.sub.2 each represents a hydrogen atom, a lower alkyl group, a lower alkoxy group, or a cyano group; and n and m each is 1, 2, or 3, is disclosed.These phenylenediamine derivatives are effectively used as antioxidants for rubbers, which scarcely cause vanishing by evaporation or a thermal denaturation even under a high-temperature condition of 150.degree. C. or higher.
摘要翻译：由下式（I）或（II）表示的苯二胺衍生物：其中R1和R2各自表示氢原子，低级烷基或低级烷氧基; R3表示氢原子或甲基; R4表示甲基或乙基; n和m各自为1,2或3; 其中R1和R2各自表示氢原子，低级烷基，低级烷氧基或氰基; 并且n和m各自为1,2或3。这些苯二胺衍生物有效地用作橡胶的抗氧化剂，即使在150℃以上的高温条件下也几乎不会蒸发消失或热变性。

3. 发明授权

US07678427B2 Process for producing aging-resistant rubber material 失效
标题翻译：生产耐老化橡胶材料的方法
公开(公告)号：US07678427B2
公开(公告)日：2010-03-16
申请号：US10533678
申请日：2003-11-19
申请人： Seiji Nakagome , Mitsuyasu Nakajima
发明人： Seiji Nakagome , Mitsuyasu Nakajima
IPC分类号： B05D3/02
CPC分类号： C08J7/065 , C08J2321/00 , C08K5/18 , C08L21/00
摘要： An aging-resistant rubber material with an improved heat resistance without deteriorating the moldability even if a rubber layer is formed from an aqueous latex of rubber and without any cost increase, even if a surface tack prevention treatment by an antitack agent is carried out, can be produced by applying a coating liquid containing an amine-based antioxidant in solution or dispersion to the surface of a cross-linked rubber material, followed by heating to a temperature of 80° C. or higher, thereby diffusing the amine-based antioxidant into the rubber material. When a coating solution containing an antitack agent together with the amine-based antioxidant in solution or dispersion is used, the surface tack prevention treatment of the cross-linked material as a product can be made at the same time.
摘要翻译：即使进行了防粘剂的表面粘合防止处理，即使橡胶层由橡胶的水性胶乳形成并且没有任何成本增加，耐老化性橡胶材料具有改善的耐热性而不劣化成型性，通过将溶液或分散体中含有胺系抗氧化剂的涂布液涂布在交联橡胶材料的表面，然后加热至80℃以上的温度，从而将胺类抗氧化剂扩散至橡胶材料。当使用在溶液或分散体中含有抗粘连剂与胺系抗氧化剂的涂布溶液时，可以同时进行作为产品的交联材料的表面防粘附处理。

4. 发明申请

US20050159519A1 Phenylenediamine derivative, production method thereof and antioxidant for rubber using it as effective constituent 审中-公开
标题翻译：苯二胺衍生物，其制备方法和使用其作为有效成分的橡胶的抗氧化剂
公开(公告)号：US20050159519A1
公开(公告)日：2005-07-21
申请号：US10354185
申请日：2003-01-30
申请人： Seiji Nakagome , Akihiko Toda
发明人： Seiji Nakagome , Akihiko Toda
IPC分类号： C07C211/55 , C07C217/80 , C07C225/22 , C07C255/56 , C08K5/18 , C08K5/16 , C07C211/50
CPC分类号： C07C255/56 , C07C211/55 , C07C217/80 , C07C225/22 , C08K5/18 , C08L21/00
摘要： A phenylenediamine derivative represented by following formula (I) or (II): wherein R1 and R2 each represents a hydrogen atom, a lower alkyl group, or a lower alkoxy group; R3 represents a hydrogen atom or a methyl group; R4 represents a methyl group or an ethyl group; and n and m each is 1, 2, or 3; wherein R1 and R2 each represents a hydrogen atom, a lower alkyl group, a lower alkoxy group, or a cyano group; and n and m each is 1, 2, or 3, is disclosed. These phenylenediamine derivatives are effectively used as antioxidants for rubbers, which scarcely cause vanishing by evaporation or a thermal denaturation even under a high-temperature condition of 150° C. or higher.
摘要翻译：由下式（I）或（II）表示的苯二胺衍生物：其中R 1和R 2各自表示氢原子，低级烷基或低级烷氧基组; R 3表示氢原子或甲基; R 4表示甲基或乙基; n和m各自为1,2或3; 其中R 1和R 2各自表示氢原子，低级烷基，低级烷氧基或氰基; 并且n和m各自为1,2或3。这些苯二胺衍生物有效地用作橡胶的抗氧化剂，即使在150℃以上的高温条件下也几乎不会蒸发而消失或热变性。

5. 发明申请

US20060035028A1 Process for producing aging-resistant rubber material 失效
标题翻译：生产耐老化橡胶材料的方法
公开(公告)号：US20060035028A1
公开(公告)日：2006-02-16
申请号：US10533678
申请日：2003-11-19
申请人： Seiji Nakagome , Mitsuyasu Nakajima
发明人： Seiji Nakagome , Mitsuyasu Nakajima
IPC分类号： B05D3/02
CPC分类号： C08J7/065 , C08J2321/00 , C08K5/18 , C08L21/00
摘要： An aging-resistant rubber material with an improved heat resistance without deteriorating the moldability even if a rubber layer is formed from an aqueous latex of rubber and without any cost increase, even if a surface tack prevention treatment by an antitack agent is carried out, can be produced by applying a coating liquid containing an amine-based antioxidant in solution or dispersion to the surface of a cross-linked rubber material, followed by heating to a temperature of 80° C. or higher, thereby diffusing the amine-based antioxidant into the rubber material. When a coating solution containing an antitack agent together with the amine-based antioxidant in solution or dispersion is used, the surface tack prevention treatment of the cross-linked material as a product can be made at the same time.
摘要翻译：即使进行了防粘剂的表面粘合防止处理，即使橡胶层由橡胶的水性胶乳形成并且没有任何成本增加，耐老化性橡胶材料具有改善的耐热性而不劣化成型性，通过将溶液或分散体中含有胺类抗氧化剂的涂布液涂布在交联橡胶材料的表面，然后加热至80℃以上的温度，从而将胺类抗氧化剂扩散到橡胶材料。当使用在溶液或分散体中含有抗粘连剂与胺系抗氧化剂的涂布溶液时，可以同时进行作为产品的交联材料的表面防粘附处理。

6. 发明授权

US06329551B1 Phenylenediamine derivative, production method thereof and antioxidant for rubber using it as effective constituent 有权
标题翻译：苯二胺衍生物，其制备方法和使用其作为有效成分的橡胶的抗氧化剂
公开(公告)号：US06329551B1
公开(公告)日：2001-12-11
申请号：US09544208
申请日：2000-04-07
申请人： Seiji Nakagome , Akihiko Toda
发明人： Seiji Nakagome , Akihiko Toda
IPC分类号： C07C21100
CPC分类号： C07C255/56 , C07C211/55 , C07C217/80 , C07C225/22 , C08K5/18 , C08L21/00
摘要： A phenylenediamine derivative represented by following formula (I) or (II): wherein R1 and R2 each represents a hydrogen atom, a lower alkyl group, or a lower alkoxy group; R3 represents a hydrogen atom or a methyl group; R4 represents a methyl group or an ethyl group; and n and m each is 1, 2, or 3; wherein R1 and R2 each represents a hydrogen atom, a lower alkyl group, a lower alkoxy group, or a cyano group; and n and m each is 1, 2, or 3, is disclosed. These phenylenediamine derivatives are effectively used as antioxidants for rubbers, which scarcely cause vanishing by evaporation or a thermal denaturation even under a high-temperature condition of 150° C. or higher.
摘要翻译：由下式（I）或（II）表示的苯二胺衍生物：其中R1和R2各自表示氢原子，低级烷基或低级烷氧基; R3表示氢原子或甲基; R4表示甲基或乙基; n和m各自为1,2或3;其中R 1和R 2各自表示氢原子，低级烷基，低级烷氧基或氰基; 并且n和m各自为1,2或3。这些苯二胺衍生物有效地用作橡胶的抗氧化剂，即使在150℃的高温条件下也几乎不会蒸发消失或热变性，或更高。

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