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1. 发明专利

CA2643092C CHROMATOGRAPHIC METHODS FOR MEASURING IMPURITIES IN A GAS SAMPLE 未知
公开(公告)号：CA2643092C
公开(公告)日：2014-04-29
申请号：CA2643092
申请日：2006-02-22
申请人： SYSTEME ANALYTIQUE INC
发明人： FORTIER ANDRE , GAMACHE YVES
IPC分类号： G01N30/88 , G01N30/46
摘要： The present invention provides an improved chromatographic system and an improved chromatographic method for measuring impurities in a gas sample that advantageously allow to extract a peak of impurity masked by the sample background. The method extracts an impurities peak from the sample background and put it in a second sample loop. Then, this second sample loop volume is injected into a second separation column. In fact, the system takes a "slice" from the sample background and fills the second sample loop with it. Then, the "slice", whose width is advantageously substantially equal to the impurities peak width, is injected in the second separation column. In a further preferred embodiment, the method also advantageously allows to concentrate a predetermined impurity, thereby providing an improved precision on the results. The chromatographic method advantageously provides an improved measure of argon in oxygen, oxygen in argon and oxygen in hydrogen.

2. 发明专利

CA2577824C ROTARY VALVE AND ANALYTICAL CHROMATOGRAPHIC SYSTEM USING THE SAME 未知
公开(公告)号：CA2577824C
公开(公告)日：2012-02-07
申请号：CA2577824
申请日：2004-08-25
申请人： SYSTEME ANALYTIQUE INC
发明人： GAMACHE YVES , FORTIER ANDRE
IPC分类号： F16K11/074
摘要： There is provided a rotary valve for fluid analytical systems. The present valve provides improved characteristics such as an extended lifetime. The valve can fulfil different fluid analytical functions and can be a multi-ports and/or multi-positions valve. The valve is provided with extra recesses in the rotor and extra ports in the stator. These recesses allow to cancel the effect of any possible leaks by evacuating them. Such a valve then prevents cross-port leaks and can advantageously be used in highly critical applications. Moreover, the present valve can be used in an analytical system which is advantageously self-diagnostic.

3. 发明专利

CA2643092A1 CHROMATOGRAPHIC METHODS FOR MEASURING IMPURITIES IN A GAS SAMPLE 未知
公开(公告)号：CA2643092A1
公开(公告)日：2006-08-31
申请号：CA2643092
申请日：2006-02-22
申请人： SYSTEME ANALYTIQUE INC
发明人： FORTIER ANDRE , GAMACHE YVES
IPC分类号： G01N30/88 , G01N30/46
摘要： An improved chromatographic method for measuring impurities in a gas sample that allows extraction of a peak of impurity masked by the sample background. An impurity peak is extracted from the sample background and put in a second sample loop and the second sample loop volume is injected into a second separation column. A "slice" is taken from the sample background to fill the second sample loop and the "slice", whose width is preferably substantially equal to the impurities peak width, is injected into the second separation column. Another embodiment allows concentration of a predetermined impurity, thereby providing an improved precision on the results. The chromatographic method provides an improved measure of argon in oxygen, oxygen in argon and oxygen in hydrogen.

4. 发明申请

WO2007098586A1 SYSTEM AND METHOD OF ELIMINATING INTERFERENCE FOR IMPURITIES MEASUREMENT IN NOBLE GASES 审中-公开
标题翻译：消除噪声对干燥气体进行干扰的系统和方法
公开(公告)号：WO2007098586A1
公开(公告)日：2007-09-07
申请号：PCT/CA2007/000314
申请日：2007-02-28
申请人： SYSTEME ANALYTIQUE INC. , GAMACHE, Yves , FORTIER, André
发明人： GAMACHE, Yves , FORTIER, André
IPC分类号： G01N21/71 , B01D53/04 , G01N21/69
CPC分类号： G01N21/73 , C01B23/0036 , C01B23/0052 , C01B23/0063 , C01B2210/0034 , C01B2210/0045 , C01B2210/0046 , C01B2210/005 , C01B2210/0051 , C01B2210/0053 , C01B2210/0062 , C01B2210/0068 , C01B2210/007 , G01N21/69 , Y02C20/20
摘要： The invention provides a system and a method of eliminating interference for impurities measurement in noble gases based on emission spectroscopy which provide very stable, sensitive and interference free results. The method mainly relies on the use of a combination of particularly designed means serially connected for cancelling interferences and proper means for correcting linearity issues. The proposed method is particularly advantageous since it offers long- term stability while providing very accurate and reliable results, even at sub-ppb and up to 10,000 ppm levels, whatever the surrounding conditions and the additional impurities that could be present in the gas under analysis.
摘要翻译：本发明提供一种基于发射光谱消除惰性气体中的杂质测量的干扰的系统和方法，其提供非常稳定，灵敏和无干扰的结果。该方法主要依靠使用串行连接的特别设计的方法来消除干扰，并适用于校正线性问题的适当方法。所提出的方法是特别有利的，因为它提供长期稳定性，同时提供非常准确和可靠的结果，即使在亚ppb和高达10,000ppm的水平，无论周围条件和可能存在于待分析气体中的附加杂质。

5. 发明申请

WO2006021071A9 ROTARY VALVE AND ANALYTICAL CHROMATOGRAPHIC SYSTEM USING THE SAME 审中-公开
标题翻译：旋转阀和分析色谱系统
公开(公告)号：WO2006021071A9
公开(公告)日：2007-06-14
申请号：PCT/CA2004001560
申请日：2004-08-25
申请人： SYSTEME ANALYTIQUE INC , GAMACHE YVES , FORTIER ANDRE
发明人： GAMACHE YVES , FORTIER ANDRE
IPC分类号： F16K11/074
CPC分类号： G01N30/20 , F16K11/074 , G01N35/1097 , G01N2030/202 , Y10T137/1044 , Y10T137/1116 , Y10T137/86863
摘要： There is provided a rotary valve for fluid analytical systems. The present valve provides improved characteristics such as an extended lifetime. The valve can fulfil different fluid analytical functions and can be a multi-ports and/or multi-positions valve. The valve is provided with extra recesses in the rotor and extra ports in the stator. These recesses allow to cancel the effect of any possible leaks by evacuating them. Such a valve then prevents cross-port leaks and can advantageously be used in highly critical applications. Moreover, the present valve can be used in an analytical system which is advantageously self-diagnostic.
摘要翻译：提供了一种用于流体分析系统的旋转阀。本阀提供改进的特性，例如延长使用寿命。阀可以满足不同的流体分析功能，可以是多端口和/或多位置阀。该阀在转子中设有额外的凹槽，并在定子中设有额外的端口。这些凹槽允许通过撤离它们来消除任何可能的泄漏的影响。这样的阀门可以防止交叉口泄漏，并且可以有利地用于高度关键的应用中。而且，本发明的阀可用于有利地是自我诊断的分析系统。

6. 发明专利

CA2577824A1 ROTARY VALVE AND ANALYTICAL CHROMATOGRAPHIC SYSTEM USING THESAME 未知
公开(公告)号：CA2577824A1
公开(公告)日：2006-03-02
申请号：CA2577824
申请日：2004-08-25
申请人： SYSTEME ANALYTIQUE INC
发明人： FORTIER ANDRE , GAMACHE YVES
IPC分类号： F16K11/074
摘要： There is provided a rotary valve for fluid analytical systems. The present valve provides improved characteristics such as an extended lifetime. The valve can fulfil different fluid analytical functions and can be a multi-ports and/or multi-positions valve. The valve is provided with extra recesses in the rotor and extra ports in the stator. These recesses allow to cancel the effect of any possible leaks by evacuating them. Such a valve then prevents cross-port leaks and can advantageously be used in highly critical applications. Moreover, the present valve can be used in an analytical system which is advantageously self-diagnostic.

7. 发明申请

WO2006089412A1 CHROMATOGRAPHIC METHODS FOR MEASURING IMPURITIES IN A GAS SAMPLE 审中-公开
标题翻译：用于测量气体样品中的污染物的色谱方法
公开(公告)号：WO2006089412A1
公开(公告)日：2006-08-31
申请号：PCT/CA2006/000258
申请日：2006-02-22
申请人： SYSTEME ANALYTIQUE INC. , GAMACHE, Yves , FORTIER, André
发明人： GAMACHE, Yves , FORTIER, André
IPC分类号： G01N30/88 , G01N30/46
CPC分类号： G01N30/461 , G01N30/14 , G01N30/465 , G01N2030/025 , G01N2030/143 , G01N2030/8872
摘要： The present invention provides an improved chromatographic system and an improved chromatographic method for measuring impurities in a gas sample that advantageously allow to extract a peak of impurity masked by the sample background. The method extracts an impurities peak from the sample background and put it in a second sample loop. Then, this second sample loop volume is injected into a second separation column. In fact, the system takes a "slice" from the sample background and fills the second sample loop with it. Then, the "slice", whose width is advantageously substantially equal to the impurities peak width, is injected in the second separation column. In a further preferred embodiment, the method also advantageously allows to concentrate a predetermined impurity, thereby providing an improved precision on the results. The chromatographic method advantageously provides an improved measure of argon in oxygen, oxygen in argon and oxygen in hydrogen.
摘要翻译：本发明提供改进的色谱系统和用于测量气体样品中的杂质的改进的色谱方法，其有利地允许提取由样品背景掩蔽的杂质的峰。该方法从样本背景中提取杂质峰，并将其置于第二个样品环中。然后，将该第二样品环体积注入第二分离柱。实际上，系统从样本背景中获取“切片”，并用它填充第二个样本循环。然后，将其宽度有利地基本上等于杂质峰宽的“切片”注入第二分离柱。在另一优选实施方案中，该方法还有利地允许浓缩预定的杂质，从而提供对结果的改进的精度。色谱方法有利地提供氧气中氩气，氩气中的氧气和氢气中的氧气的改进测量。

8. 发明申请

WO2007045068A1 CHROMATOGRAPHIC SYSTEMS AND METHODS FOR ELIMINATING INTERFERENCE FROM INTERFERING AGENTS 审中-公开
标题翻译：用于消除干扰剂干扰的色谱系统和方法
公开(公告)号：WO2007045068A1
公开(公告)日：2007-04-26
申请号：PCT/CA2006/000364
申请日：2006-03-10
申请人： SYSTEME ANALYTIQUE INC. , GAMACHE, Yves , FORTIER, André
发明人： GAMACHE, Yves , FORTIER, André
IPC分类号： G01N30/88
CPC分类号： G01N30/40 , G01N30/468 , G01N2030/025
摘要： The present invention provides a chromatographic method for eliminating interference from interfering agents, coming from the gas sample itself or from the system material used to perform the impurities measurements, on impurities to be quantified in a gas sample. The method advantageously relies on the use of an additional valve and an additional sample loop particularly arranged in a G. C. system, and also on an additional supporting gas inlet operatively connected to the system through the additional sample loop for providing the system with a supporting gas comprising at least a predetermined portion of a predetermined active gas that will react with the unwanted interfering impurities, if any, or with the column material to cancel out unwanted active sites. Thus, the method of the present invention can advantageously be used in gas chromatographic systems to improve sensitivity thereof by acting on column separation material.
摘要翻译：本发明提供一种用于消除来自气体样品本身或来自用于进行杂质测量的系统材料的干扰剂对待在气体样品中定量的杂质的干扰的色谱方法。该方法有利地依赖于使用特别布置在GC系统中的另外的附加阀和另外的样品回路，以及通过另外的样品回路可操作地连接到系统的附加支撑气体入口，以向系统提供支撑气体，该支撑气体包括至少预定活性气体的预定部分，其将与不需要的干扰杂质（如果有的话）反应，或与柱材料反应以抵消不想要的活性位点。因此，本发明的方法可以有利地用于气相色谱系统中，以通过作用于柱分离材料来提高其敏感性。

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