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1. 发明申请

WO1997047294A1 ANTIBACTERIAL AGENTS AND COSMETICS AND CLOTHES CONTAINING THE SAME 审中-公开
标题翻译：抗菌剂和化妆品以及含有它的衣服
公开(公告)号：WO1997047294A1
公开(公告)日：1997-12-18
申请号：PCT/JP1997001710
申请日：1997-05-21
申请人： SODA AROMATIC CO., LTD. , NOBUHIRO, Akio , KATO, Yutaka , HASEBE, Akio
发明人： SODA AROMATIC CO., LTD.
IPC分类号： A61K31/12
CPC分类号： D06M16/00 , A01N35/06 , A01N43/22 , A61K8/0208 , A61K8/35 , A61K8/4973 , A61Q5/00 , A61Q15/00 , A61Q17/005 , D06M13/005 , D06M13/12 , D06M13/228 , Y10S514/859
摘要： Safe antibacterial agents containing macrocyclic lactones and/or macrocyclic ketones of specific chemical structures and usable in various cases for inhibiting the growth of indigenous dermal bacteria. Cosmetics containing these antibacterial agents can, in particular, suppress the evolution of the body odor and are efficacious in preventing or treating pimples. When added to clothes, these antibacterial agents can achieve antibacterial and deodorizing effects.
摘要翻译：含有特定化学结构的大环内酯和/或大环酮的安全抗菌剂，可用于各种情况下用于抑制土着皮肤细菌的生长。含有这些抗菌剂的化妆品特别能抑制身体气味的发生，并且有效地预防或治疗粉刺。当添加到衣服时，这些抗菌剂可以达到抗菌和除臭效果。

2. 发明申请

WO2014007388A1 METHOD FOR IMPROVING FLAVOR OF FOOD AND BEVERAGE, AND FOOD AND BEVERAGE HAVING FLAVOR IMPROVED THEREBY 审中-公开
标题翻译：用于改善食品和饮料的方法，以及具有改善的食品和饮料的方法
公开(公告)号：WO2014007388A1
公开(公告)日：2014-01-09
申请号：PCT/JP2013/068571
申请日：2013-07-02
申请人： AJINOMOTO CO., (THAILAND) LTD. , SODA AROMATIC CO., LTD.
发明人： FUJITSUKA, Masaaki , KAWAGUCHI, Hirokazu , CHARASAI, Bonggodmas , FUKAYA, Fuyuki , ITO, Yoshihiro , NAGAI, Satoshi , HATTORI, Shoji
IPC分类号： A23F5/18 , A23F3/20 , A23L1/015
CPC分类号： A23F5/185 , A23F3/205 , A23L5/273
摘要： The object of the present invention is to provide a method for improving flavor of food and beverage, wherein causative materials of undesirable aroma and bitterness produced in heating and processing a food and beverage is specified and selectively removed, whereby the flavor of food and beverage are improved, and the food and beverage having the flavor improved thereby. The present invention provides a process for improving flavor of food and beverage which comprises bringing food and beverage containing pyridine into contact with a weakly acidic cation exchange resin to make the pyridine adsorb on the weakly acidic cation exchange resin, making components other than pyridine desorb with alkali solution therefrom and collecting, and making pyridine desorb therefrom and collecting.
摘要翻译：本发明的目的是提供一种改善食品和饮料风味的方法，其中规定了食品和饮料的加热和加工中产生的不希望的香味和苦味的原料，并且选择性地除去食品和饮料的味道改善了食品和饮料，从而改善了风味。本发明提供了一种改善食品和饮料风味的方法，其包括使含有吡啶的食品和饮料与弱酸性阳离子交换树脂接触以使吡啶吸附在弱酸性阳离子交换树脂上，使除吡啶解吸附以外的组分与碱溶液从中收集，并使吡啶脱离并收集。

3. 发明申请

WO1998003460A1 PROCESS FOR THE PREPARATION OF ALKYL CARBOXYLATES 审中-公开
标题翻译：制备羧酸烷基酯的方法
公开(公告)号：WO1998003460A1
公开(公告)日：1998-01-29
申请号：PCT/JP1997002488
申请日：1997-07-17
申请人： TORAY INDUSTRIES, INC. , SODA AROMATIC CO., LTD. , NIWA, Atsushi , IMAMURA, Shinzo , HASEBE, Akio , ITO, Nobuhiko
发明人： TORAY INDUSTRIES, INC. , SODA AROMATIC CO., LTD.
IPC分类号： C07C67/08
CPC分类号： C07C67/08 , C07C69/34
摘要： A process for preparing high-purity alkyl carboxylates efficiently by esterifying a carboxylic acid with an alcohol in the presence of an acid catalyst, characterized in that a solid acid catalyst is used as the catalyst and that the esterification is completed by conducting dehydration in the course of the esterification to remove the formed water from the reaction system and thereafter resuming the esterification. The dialkyl esters of alkanedioic acids prepared by the process can suitably be used as intermediates for the preparation of drugs, agricultural chemicals, perfumes, dyes, liquid-crystal materials, polymers and so on.
摘要翻译：一种通过在酸催化剂存在下用醇酯化羧酸而有效制备高纯度烷基羧酸盐的方法，其特征在于使用固体酸催化剂作为催化剂，通过在该过程中进行脱水来完成酯化反应的酯化反应以从反应体系中除去形成的水，然后恢复酯化。通过该方法制备的链烷二酸的二烷基酯可以适当地用作制备药物，农药，香料，染料，液晶材料，聚合物等的中间体。

4. 发明申请

WO1997006156A1 PROCESS FOR PRODUCING 2-('omega'-ALKOXYCARBONYLALKANOYL)-4-BUTANOLIDE AND LONG-CHAIN 'omega'-HYDROXY CARBOXYLIC ACID 审中-公开
标题翻译： 2-（ω-羟基碳酰氯烷基）-4-丁醇和长链ω-羟基羧酸的制备方法
公开(公告)号：WO1997006156A1
公开(公告)日：1997-02-20
申请号：PCT/JP1995001555
申请日：1995-08-04
申请人： TORAY INDUSTRIES, INC. , SODA AROMATIC CO., LTD. , KATOU, Tetsuya , HATA, Go , ETOH, Takeaki , ITO, Nobuhiko
发明人： TORAY INDUSTRIES, INC. , SODA AROMATIC CO., LTD.
IPC分类号： C07D307/32
CPC分类号： C07D307/33 , C07C51/09 , C07C51/377 , C07C59/01
摘要： A 2-( omega -alkoxycarbonylalkanoyl)-4-butanolide is produced in a high yield with a good selectivity by the condensation reaction of gamma -butyrolactone with a readily available, inexpensive dicarboxylic ester represented by the following general formula: ROOC(CH2)nCOOR (wherein n is 7 to 13; and R represents alkyl or alkenyl). A long-chain omega -hydroxy carboxylic acid is produced by hydrolyzing and decarboxylating the above butanolide and reducing the carbonyl group of the obtained product into a methylene group.
摘要翻译：通过γ-丁内酯与由以下通式表示的容易获得的廉价二羧酸酯的缩合反应，通过高选择性产生2-（ω-烷氧基羰基烷酰基）-4-丁醇酸：ROOC（CH 2）n COOR （其中n为7至13; R为烷基或链烯基）。通过水解和脱羧上述丁醇酸并将所得产物的羰基还原成亚甲基来生产长链ω-羟基羧酸。

5. 发明申请

US20020068832A1 Methods for making 2-(omega-alkoxycarbonylalkanoyl) -4-butanolide, ester of omega-hydroxy - ( omega-3 ) -ketoaliphatic acid, and derivatives thereof 有权
标题翻译：制备2-（ω-烷氧基羰基烷酰基）-4-丁醇酯，ω-羟基 - （ω-3） - 酮脂肪酸的酯及其衍生物的方法
公开(公告)号：US20020068832A1
公开(公告)日：2002-06-06
申请号：US09997140
申请日：2001-11-29
申请人： Soda Aromatic Co., Ltd.
发明人： Hideaki Takaoka , Sigeru Wada , Nobuhiko Ito , Akio Hasebe , Shinzo Imamura , Hideo Muraoka
IPC分类号： C07D37/33
CPC分类号： C07D307/33 , C07C51/43 , C07C67/32 , C07C69/716 , C07C59/215
摘要： In industrial production of null-hydroxyaliphatic acid being an important intermediate for large cyclic lactone-based perfumes, using dicarboxylate ester which is inexpensive and readily obtainable, a method, with high yield and improved selectively, for making a 2-(null-alkoxycarbonylalkanoyl)-4-butanolide and an alkaline metal salt thereof, an ester of null-hydroxy-(null-3)-ketoaliphatic acid as a novel compound and a derivative thereof, and a method for making the same are provided. Condensation reaction of null-butyrolactone with a dicarboxylate ester represented by the general formula (1) ROOC(CH2)nCOOR wherein n is an integer of 7 to 13 and R is an alkyl group forms a condensation solution containing an alkaline metal salt of 2-(null-alkoxycarbonylalkanoyl)-4-butanolide represented by the general formula (3): 1 wherein n is an integer of 7 to 13, R is an alkyl group, and M is an alkaline metal; the solution is extracted with water or an aqueous alkaline solution and subjected to hydrolysis and decarboxylation to form an alkaline metal salt of null-hydroxy-(null-3)-ketoaliphatic acid represented by the general formula (5): 2 wherein n is an integer of 7 to 13 and M is an alkaline metal; and the compound is selectively and effectively separated and recovered and then acidified to form an null-hydroxy-(null-3)-ketoaliphatic acid represented by the general formula (10): 3 wherein n is an integer of 7 to 13.
摘要翻译：在工业生产中，ω-羟基脂肪酸是大环内酯基香料的重要中间体，使用廉价且易于获得的二羧酸酯，可以制备2-（ω-烷氧羰基烷酰基） -4-丁醇酸及其碱金属盐，作为新化合物的ω-羟基 - （ω-3） - 脂肪酸的酯及其衍生物及其制备方法。 γ-丁内酯与通式（1）表示的二羧酸酯的缩合反应ROOC（CH 2）n COOR其中n为7〜13的整数，R为烷基，形成含有2- （3）表示的（ω-烷氧基羰基烷酰基）-4-丁醇酯：其中n为7〜13的整数，R为烷基，M为碱金属; 溶液用水或碱性水溶液萃取，并进行水解和脱羧，形成由通式（5）表示的ω-羟基 - （ω-3） - 酮脂肪酸的碱金属盐：其中n为整数为7〜13，M为碱金属; 选择性且有效地分离和回收化合物，然后酸化以形成由通式（10）表示的ω-羟基 - （ω-3） - 酮脂肪酸：其中n为7至13的整数。

6. 发明申请

US20020133028A1 Methods for making 2-(omega-alkoxycarbonylalkanoyl) -4-butanolide, ester of omega-Hydroxy-(omega-3) -ketoaliphatic acid, and derivatives thereof 有权
标题翻译：制备2-（ω-烷氧羰基烷酰基）-4-丁醇酯，ω-羟基 - （ω-3） - 酮脂肪酸的酯及其衍生物的方法
公开(公告)号：US20020133028A1
公开(公告)日：2002-09-19
申请号：US10047895
申请日：2002-01-14
申请人： Soda Aromatic Co., Ltd.
发明人： Hideaki Takaoka , Sigeru Wada , Nobuhiko Ito , Akio Hasebe , Shinzo Imamura , Hideo Muraoka
IPC分类号： C07D37/33
CPC分类号： C07D307/33 , C07C51/43 , C07C67/32 , C07C69/716 , C07C59/215
摘要： In industrial production of null-hydroxyaliphatic acid being an important intermediate for large cyclic lactone-based perfumes, using dicarboxylate ester which is inexpensive and readily obtainable, a method, with high yield and improved selectively, for making a 2-(null-alkoxycarbonylalkanoyl)-4-butanolide and an alkaline metal salt thereof, an ester of null-hydroxy-(null-3)-ketoaliphatic acid as a novel compound and a derivative thereof, and a method for making the same are provided. Condensation reaction of null-butyrolactone with a dicarboxylate ester represented by the general formula (1). ROOC(CH2)nCOOR wherein n is an integer of 7 to 13 and R is an alkyl group forms a condensation solution containing an alkaline metal salt of 2-(null-alkoxycarbonylalkanoyl)-4-butanolide represented by the general formula (3): 1 wherein n is an integer of 7 to 13, R is an alkyl group, and M is an alkaline metal; the solution is extracted with water or an aqueous alkaline solution and subjected to hydrolysis and decarboxylation to form an alkaline metal salt of null-hydroxy-(null-3)-ketoaliphatic acid represented by the general formula (5): 2 wherein n is an integer of 7 to 13 and M is an alkaline metal; and the compound is selectively and effectively separated and recovered and then acidified to form an null-hydroxy-(null-3)-ketoaliphatic acid represented by the general formula (10): 3 wherein n is an integer of 7 to 13.
摘要翻译：在工业生产中，ω-羟基脂肪酸是大环内酯基香料的重要中间体，使用廉价且易于获得的二羧酸酯，可以制备2-（ω-烷氧羰基烷酰基） -4-丁醇酸及其碱金属盐，作为新化合物的ω-羟基 - （ω-3） - 脂肪酸的酯及其衍生物及其制备方法。 γ-丁内酯与通式（1）表示的二羧酸酯的缩合反应。 ROOC（CH 2）n COOR其中n为7〜13的整数，R为烷基，形成含有通式（3）表示的2-（ω-烷氧羰基烷酰基）-4-丁醇的碱金属盐的缩合溶液：其中n为7〜13的整数，R为烷基，M为碱金属; 溶液用水或碱性水溶液萃取，并进行水解和脱羧，形成由通式（5）表示的ω-羟基 - （ω-3） - 酮脂肪酸的碱金属盐：其中n为整数为7〜13，M为碱金属; 选择性且有效地分离和回收化合物，然后酸化以形成由通式（10）表示的ω-羟基 - （ω-3） - 酮脂肪酸：其中n为7至13的整数。

7. 发明申请

US20010051734A1 Methods for making 2-(omega-alkoxycarbonylalkanoyl) -4-butanolide, ester of omega-hydroxy- (omega-3) - ketoaliphatic acid, and derivatives thereof 有权
标题翻译：制备2-（ω-烷氧基羰基烷酰基）-4-丁醇酯，ω-羟基 - （ω-3） - 酮脂肪酸的酯及其衍生物的方法
公开(公告)号：US20010051734A1
公开(公告)日：2001-12-13
申请号：US09894014
申请日：2001-06-28
申请人： Soda Aromatic Co., Ltd.
发明人： Hideaki Takaoka , Sigeru Wada , Nobuhiko Ito , Akio Hasebe , Shinzo Imamura , Hideo Muraoka
IPC分类号： C07D37/33
CPC分类号： C07D307/33 , C07C51/43 , C07C67/32 , C07C69/716 , C07C59/215
摘要： In industrial production of null-hydroxyaliphatic acid being an important intermediate for large cyclic lactone-based perfumes, using dicarboxylate ester which is inexpensive and readily obtainable, a method, with high yield and improved selectively, for making a 2-(null-alkoxycarbonylalkanoyl)-4-butanolide and an alkaline metal salt thereof, an ester of null-hydroxy-(null-3)-ketoaliphatic acid as a novel compound and a derivative thereof, and a method for making the same are provided. Condensation reaction of null-butyrolactone with a dicarboxylate ester represented by the general formula (1) ROOC(CH2)nCOOR wherein n is an integer of 7 to 13 and R is an alkyl group forms a condensation solution containing an alkaline metal salt of 2-(null-alkoxycarbonylalkanoyl)-4-butanolide represented by the general formula (3): 1 wherein n is an integer of 7 to 13, R is an alkyl group, and M is an alkaline metal; the solution is extracted with water or an aqueous alkaline solution and subjected to hydrolysis and decarboxylation to form an alkaline metal salt of null-hydroxy-(null-3)-ketoaliphatic acid represented by the general formula (5): 2 wherein n is an integer of 7 to 13 and M is an alkaline metal; and the compound is selectively and effectively separated and recovered and then acidified to form an null-hydroxy-(null-3)-ketoaliphatic acid represented by the general formula (10): 3 wherein n is an integer of 7 to 13.
摘要翻译：在工业生产中，ω-羟基脂肪酸是大环内酯基香料的重要中间体，使用廉价且易于获得的二羧酸酯，可以制备2-（ω-烷氧羰基烷酰基） -4-丁醇酸及其碱金属盐，作为新化合物的ω-羟基 - （ω-3） - 脂肪酸的酯及其衍生物及其制备方法。 γ-丁内酯与通式（1）表示的二羧酸酯的缩合反应ROOC（CH 2）n COOR其中n为7〜13的整数，R为烷基，形成含有2- （3）表示的（ω-烷氧基羰基烷酰基）-4-丁醇酯：其中n为7〜13的整数，R为烷基，M为碱金属; 溶液用水或碱性水溶液萃取，并进行水解和脱羧，形成由通式（5）表示的ω-羟基 - （ω-3） - 酮脂肪酸的碱金属盐：其中n为整数为7〜13，M为碱金属; 选择性且有效地分离和回收化合物，然后酸化以形成由通式（10）表示的ω-羟基 - （ω-3） - 酮脂肪酸：其中n为7至13的整数。

8. 发明申请

US20220187261A1 VOLATILE COMPONENT EVALUATION METHOD AND DEVICE USED THEREFOR 有权
公开(公告)号：US20220187261A1
公开(公告)日：2022-06-16
申请号：US17430438
申请日：2020-02-07
申请人： SODA AROMATIC CO., LTD.
发明人： Hitoshi Takagaki , Kenzo Kasai , Hanna Ochi
IPC分类号： G01N30/86 , G01N30/60 , G01N33/00
摘要： An apparatus includes a first flow channel connected to a gas release channel of a gas chromatograph that sends at least a volatile component separated by the gas chromatograph into the mouth of an evaluator; a container that stores a non-gaseous flowable specimen having fluidity; and a second flow channel that sends the flowable specimen into the mouth.

9. 发明专利

SG11202106920YA VOLATILE COMPONENT EVALUATION METHOD AND DEVICE USED THEREFOR 未知
公开(公告)号：SG11202106920YA
公开(公告)日：2021-07-29
申请号：SG11202106920Y
申请日：2020-02-07
申请人： SODA AROMATIC CO LTD
发明人： TAKAGAKI HITOSHI , KASAI KENZO , OCHI HANNA
IPC分类号： G01N1/00 , G01N30/80 , G01N30/88
摘要： The present invention addresses the problem of evaluating simply, how an aroma component influences the senses when eating and drinking. This device is characterized by comprising: a first flow path 1 connected to the exhaust flow path from a gas chromatograph, sending into the mouth a volatile component separated by the gas chromatograph; a container 2 for placing therein a fluid sample, other than a gas, having fluidity; and a second flow path 3 sending into the mouth the fluid sample that has been placed in the container 2. Using this device allows each of the volatile components separated by the gas chromatograph and fluid samples other than gas to be sent directly into the mouth and evaluated successively, thus solving the problem.

10. 发明专利

DE3028757C2 未知
公开(公告)号：DE3028757C2
公开(公告)日：1982-09-16
申请号：DE3028757
申请日：1980-07-29
申请人： OTSUKA KAGAKU YAKUHIN K.K., OSAKA, JP , SODA AROMATIC CO., LTD., TOKYO, JP
发明人： TORRI, SHIGERU , NAKANE, SHOJI, OKAYAMA, JP , SHIRAKAWA, TOSHIFUMI, KOSHIGAYA, SAITAMA, JP , AKADA, MITSUO, TOKUSHIMA, JP
IPC分类号： C07C45/00 , C07C45/28 , C07C47/542 , C07C67/00 , C25B3/23 , C25B1/00
摘要： p-tert-Butyl benzaldehyde is prepared by performing at least once the steps of (a) electrolyzing cerium (III) nitrate or ammonium cerium (III) nitrate to obtain cerium (IV) nitrate or ammonium cerium (IV) nitrate in a mixture of water and an aliphatic acid, and (b) oxidizing p-tert-butyl toluene with the Ce(IV)-containing mixture.

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