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1. 发明授权

US5542956A Process for dyeing or printing hydroxyl group containing fiber materials 失效
标题翻译：用于染色或印刷含羟基纤维材料的方法
公开(公告)号：US5542956A
公开(公告)日：1996-08-06
申请号：US313665
申请日：1994-09-27
申请人： David McMullan , Rudolf Schaulin , Urs Lauk
发明人： David McMullan , Rudolf Schaulin , Urs Lauk
IPC分类号： C09B67/22 , C09B31/08 , C09B31/22 , C09B35/039 , C09B43/16 , C09B45/28 , C09B56/06 , C09B62/04 , D06P3/62 , D06P3/66 , D06P3/82 , D06P3/87 , D06P1/02
CPC分类号： D06P3/8223 , C09B31/08 , C09B31/22 , C09B35/039 , C09B43/16 , C09B45/28 , C09B56/06 , C09B62/04 , D06P3/62 , D06P3/66 , D06P3/8219
摘要： The invention relates to a process for dyeing or printing hydroxyl group containing fiber materials, which comprises using at least one yellow or orange dyeing dye of formula ##STR1## wherein the substituents are as defined in claim 1, together with at least one blue dyeing dye and/or at least one red dyeing dye. Level dyeings and prints with good allround fastness properties are obtained by the process of the invention.
摘要翻译：本发明涉及一种用于染色或印刷含羟基纤维材料的方法，其包括使用至少一种式（1）+ TR图像的黄色或橙色染色染料，其中取代基如权利要求1所定义，以及至少一种蓝染色剂和/或至少一种红染色剂。通过本发明的方法获得具有良好耐环牢性的水平染色和印花。

2. 发明授权

US5320648A Process for dyeing or printing hydroxyl group containing fibre materials 失效
标题翻译：用于染色或印刷含羟基纤维材料的方法
公开(公告)号：US5320648A
公开(公告)日：1994-06-14
申请号：US991670
申请日：1992-12-16
申请人： David H. McMullan , Rudolf Schaulin , Urs Lauk
发明人： David H. McMullan , Rudolf Schaulin , Urs Lauk
IPC分类号： C09B67/22 , C09B31/08 , C09B31/22 , C09B35/039 , C09B43/16 , C09B45/28 , C09B62/04 , D06P3/62 , D06P3/66 , D06P3/82 , C09B56/00 , D06P1/06
CPC分类号： C09B31/22 , C09B31/08 , C09B35/039 , C09B43/16 , C09B45/28 , C09B62/04 , D06P3/62 , D06P3/66 , D06P3/8219 , D06P3/8223 , Y10S8/918 , Y10S8/922
摘要： The invention relates to a process for dyeing or printing hydroxyl group containing fibre materials, which comprises using at least one yellow or orange dyeing dye of formula ##STR1## wherein the substituents are as defined in claim 1, together with at least one blue dyeing dye and/or at least one red dyeing dye. Level dyeings and prints with good allround fastness properties are obtained by the process of the invention.
摘要翻译：本发明涉及一种用于染色或印刷含羟基纤维材料的方法，其包括使用至少一种式（1）的黄色或橙色染色染料，其中取代基如权利要求1所定义，连同至少一个蓝染色剂和/或至少一种红染色剂。通过本发明的方法获得具有良好耐环牢性的水平染色和印花。

3. 发明授权

US5176717A Use of sulfonated polyazo dyes for dyeing leather in brilliant fast red shades 失效
标题翻译：使用硫酸化多晶氧化皮，用于在快速红色的皮肤中染色皮革
公开(公告)号：US5176717A
公开(公告)日：1993-01-05
申请号：US732987
申请日：1991-07-19
申请人： Rudolf Schaulin , Peter Moser , Alois Puntener
发明人： Rudolf Schaulin , Peter Moser , Alois Puntener
IPC分类号： C09B33/16 , C09B33/052 , C09B43/16 , C09B62/09 , D06P3/32
CPC分类号： D06P3/3286 , C09B33/052 , C09B43/16 , C09B62/09 , D06P3/3226
摘要： The use of compounds of the formula ##STR1## in which the symbols are as defined in claim 1, for dyeing leather is described.
摘要翻译：描述了其中符号如权利要求1中定义的用于染色皮革的式“IMAGE”（1） + TR 的化合物的用途。

4. 发明授权

US4997919A Azo direct dyes containing a non-reactive triazinyl moiety 失效
标题翻译：含有非反应性三嗪基部分的偶氮直接染料
公开(公告)号：US4997919A
公开(公告)日：1991-03-05
申请号：US370203
申请日：1989-06-19
申请人： Rudolf Schaulin
发明人： Rudolf Schaulin
IPC分类号： C09B43/16 , C09B62/09 , D06P3/54 , D06P3/62
CPC分类号： C09B43/16
摘要： This invention relates to direct dyes for various substrates, in particular cellulosic fiber materials. The inventive dyes are high-temperature-resistant and highly suitable for the single bath, one step dyeing of polyester/cotton mixed fabrics with a disperse dye for the polyester fibers under the dyeing conditions for polyester fibers.The inventive dyes are of the formula ##STR1## in which A is a radical of the formula ##STR2## A' has the meaning of A or is a mono- or polyazo dye radical which is different from A, R and R', independently of one another, are hydrogen or C.sub.1 -C.sub.4 alkyl which is unsubstituted or substituted by chlorine, hydroxyl, cyano, carboxyl, sulfo, sulfato, methoxy, ethoxy, methoxycarbonyl or ethoxycarbonyl, R.sub.1 is hydroxyl, C.sub.1 -C.sub.4 alkoxy, halogen, C.sub.1 -C.sub.4 alkylthio, amino, N-mono- or N,N-di-C.sub.1 -C.sub.4 alkylamino which is unsubstituted or substituted in the alkyl moiety by hydroxyl, carboxyl or C.sub.1 -C.sub.4 alkoxy, cyclohexylamino, phenylamino or N-C.sub.1 -C.sub.4 alkyl-N-phenylamino which are unsubstituted or substituted in the phenyl moiety by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, carboxyl, sulfo or halogen, morpholino, piperidino or 3-carboxy- or 3-carboxamidopyridin-1-yl, R.sub.2 is unsubstituted or hydroxy-substituted C.sub.1 -C.sub.4 alkyl, and the phenyl radical (a) is unsubstituted or substituted by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, halogen, hydroxyl, carboxyl, sulfo, --NHCOR.sub.2 or unsubstituted or sulfo-, C.sub.1 -C.sub.4 alkoxy-, hydroxyl- or halogen-substituted phenylazo or 1-2-naphthylazo.
摘要翻译：本发明涉及用于各种基材，特别是纤维素纤维材料的直接染料。本发明的染料具有耐高温性，高度适用于单浴，在聚酯纤维染色条件下，聚酯/棉混纺织物与聚酯纤维分散染料一步染色。本发明的染料具有下式（IMAGE）（1），其中A是下式的基团：（A）A'具有A的含义，或者是不同于A的单或多偶氮染料基团， R和R'彼此独立地是氢或未被取代或被氯，羟基，氰基，羧基，磺基，硫酸根，甲氧基，乙氧基，甲氧基羰基或乙氧基羰基取代的C1-C4烷基，R1是羟基，C1-C4烷氧基，卤素，C 1 -C 4烷硫基，氨基，未被取代或在烷基部分被羟基，羧基或C 1 -C 4烷氧基，环己基氨基，苯基氨基或N-C 1 -C 4烷基 - C 1 -C 4烷基，C 1 -C 4烷氧基，羧基，磺基或卤素，吗啉代，哌啶子基或3-羧基 - 或3-甲酰胺基吡啶-1-基在苯基部分未取代或取代的N-苯基氨基，未取代或羟基 - 取代的C 1 -C 4烷基，苯基（a）未取代或被C 1 -C 4烷基，C 1 -C 4烷氧基，卤素，羟基，碳原子氧基，磺基，-NHCOR 2或未取代的或磺基，C 1 -C 4烷氧基 - ，羟基或卤素取代的苯偶氮或1-2-萘基偶氮。

5. 发明授权

US5147410A Process for the end-to-end dyeing of cellulosic fibres: desalted direct dye and migration inhibitor 失效
标题翻译：细胞纤维素终端染色的工艺：脱硫直接染色剂和转移抑制剂
公开(公告)号：US5147410A
公开(公告)日：1992-09-15
申请号：US700001
申请日：1991-05-14
申请人： Anette Heindl , Rudolf Schaulin , Thomas Stockhorst
发明人： Anette Heindl , Rudolf Schaulin , Thomas Stockhorst
IPC分类号： C09B67/26 , C09B67/54 , D06P3/62
CPC分类号： D06P3/62 , C09B67/0073 , C09B67/0096 , Y10S8/918
摘要： The invention relates to a process for the end-to-end dyeing of cellulosic fibres or cellulosic fibre blends with direct dyes by the pad dyeing process, which comprises padding said fibre materials with an aqueous liquor containing one or more deionized dyes and a migration inhibitor, then expressing the padded goods and subsequently fixing the dye thereon.The process of the invention is suitable for dyeing textile cellulosic fibres or cellulosic fibre blends end-to-end in shades of good allround fastness properties.
摘要翻译：本发明涉及通过垫染色方法对直接染料进行纤维素纤维或纤维素纤维共混物的端到端染色的方法，该方法包括用含有一种或多种去离子染料和迁移抑制剂的含水液体填充所述纤维材料，然后表达填充物品并随后将染料固定在其上。本发明的方法适用于以良好的全能牢度性质的色调将纺织纤维素纤维或纤维素纤维混合物端到端染色。

6. 发明授权

US4661292A Process for the preparation of 1,4-diamino-2,3-dicyanoanthraquinone 失效
标题翻译：制备1,4-二氨基-2,3-二氰基蒽醌的方法
公开(公告)号：US4661292A
公开(公告)日：1987-04-28
申请号：US784434
申请日：1985-10-03
申请人： Rudolf Schaulin , Maurice Grelat
发明人： Rudolf Schaulin , Maurice Grelat
IPC分类号： C07C309/53 , C07C67/00 , C07C255/58 , C07C301/00 , C07C303/22 , C07C143/665 , C07C97/24
CPC分类号： C07C255/58
摘要： The invention relates to a process for the preparation of 1,4-diamino-2,3-dicyanoanthraquinone, starting from 1,4-diaminoanthraquinones, or salts thereof, of the formula ##STR1## wherein n is 0, 1 or 2. To introduce the two cyanide radicals, the starting material is treated, in the presence of an oxidizing agent, with a compound which donates cyanide ions. The process comprises using as solvent a mixture of a carboxamide, an N-alkylated carboxamide or a lactam and water, which mixture contains more than 10% by weight of water.1,4-Diamino-2,3-dicyanoanthraquinone is an important intermediate for the synthesis of textile dyes.
摘要翻译：本发明涉及由1,4-二氨基蒽醌或其盐，其中n为0,1或2的1,4-二氨基-2,3-二氰基蒽醌的制备方法，其中n为0,1或2。引入两个氰化物基团，在氧化剂的存在下，将起始物质与提供氰化物离子的化合物进行处理。该方法包括使用甲酰胺，N-烷基化的甲酰胺或内酰胺和水的混合物，该混合物含有超过10重量％的水。 1,4-二氨基-2,3-二氰基蒽醌是织物染料合成的重要中间体。

7. 发明授权

US5324330A Dye mixtures and the use thereof 失效
标题翻译：染料混合物及其用途
公开(公告)号：US5324330A
公开(公告)日：1994-06-28
申请号：US988539
申请日：1992-12-10
申请人： Rudolf Schaulin , Urs Lauk
发明人： Rudolf Schaulin , Urs Lauk
IPC分类号： C09B67/22 , D06P3/52 , D06P3/60 , D06P3/66 , D06P3/82 , D06P1/00 , C09B56/00
CPC分类号： C09B67/0055 , Y10S8/918 , Y10S8/922
摘要： Dye mixtures comprising at least one dye of formula ##STR1## and at least one dye of formula ##STR2## wherein the substituents are as defined in claim 1, have good allround fastness properties and are suitable for dyeing cellulosic fibre materials.
摘要翻译：包含至少一种下式的染料的染料混合物，其中取代基如权利要求1所定义，其中取代基如权利要求1所定义，具有式（1）的化合物和/或图像的至少一种式适用于染色纤维素纤维材料。

8. 发明授权

US4699735A Process for the preparation of 1,4-diaminoanthraquinone-2-sulfonic acid 失效
标题翻译： 1,4-二氨基蒽醌-2-磺酸的制备方法
公开(公告)号：US4699735A
公开(公告)日：1987-10-13
申请号：US818449
申请日：1986-01-13
申请人： Maurice Grelat , Rudolf Schaulin
发明人： Maurice Grelat , Rudolf Schaulin
IPC分类号： C07B61/00 , B01J31/00 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C309/53 , C09B1/24 , C07C143/665
CPC分类号： C09B1/24
摘要： The invention relates to a process for the preparation of 1,4-diaminoanthraquinone-2-sulfonic acid by sulfonating 1,4-diaminoanthraquinone or leuco-1,4-diaminoanthraquinone, which comprises carrying out the sulfonation at elevated temperature with oleum as sulfonating agent, with or without the addition of a Lewis base. The 1,4-diaminoanthraquinone-2-sulfonic acid is used in particular for synthesizing anthraquinoid disperse dyes for dyeing hydrophobic fibre materials.
摘要翻译：本发明涉及通过磺化1,4-二氨基蒽醌或无色-1,4-二氨基蒽醌制备1,4-二氨基蒽醌-2-磺酸的方法，该方法包括在发酵油作为磺化剂的高温下进行磺化有或没有添加路易斯碱。 1,4-二氨基蒽醌-2-磺酸特别用于合成用于染色疏水性纤维材料的蒽醌分散染料。

9. 发明授权

US5328995A Azo dyes containing triazine middle components and a 1,4-phenylene-2,5-disubstituted coupling component 失效
标题翻译：含有三嗪中间组分和1,4-亚苯基-2,5-二取代偶合组分的偶氮染料
公开(公告)号：US5328995A
公开(公告)日：1994-07-12
申请号：US9427
申请日：1993-01-27
申请人： Rudolf Schaulin , Urs Lauk
发明人： Rudolf Schaulin , Urs Lauk
IPC分类号： C07D251/18 , C07C245/08 , C07D251/12 , C07D251/48 , C07D251/50 , C07D251/52 , C07D251/70 , C09B33/06 , C09B33/08 , C09B43/11 , C09B43/16 , C09B62/04 , C09B62/09 , C09D11/00 , D06P1/18 , D06P1/382 , D06P3/24 , D06P3/62 , D06P3/66 , D06P3/82 , D06P3/04
CPC分类号： C09B43/11 , C09B43/16 , C09B62/043 , C09B62/09
摘要： The compounds of the formula ##STR1## where the substituents are as defined in claim 1, are direct dyes for various substrates, in particular cellulosic fibre materials. They are high temperature resistant and therefore are particularly highly suitable for the one-bath, single-stage dyeing of polyester/cotton blend fabrics with a disperse dye for the polyester fibres under the dyeing conditions for polyester fibres.
摘要翻译：取代基如权利要求1中所定义的式（IMA）（1）的化合物是用于各种底物，特别是纤维素纤维材料的直接染料。它们耐高温，因此特别适用于在聚酯纤维的染色条件下，聚酯/棉混纺织物与聚酯纤维分散染料的单浴，单级染色。

10. 发明授权

US5059682A Water-soluble phthalocyanine compounds, process for their preparation and their use 失效
标题翻译：水溶性酚酞化合物及其制备方法及其应用
公开(公告)号：US5059682A
公开(公告)日：1991-10-22
申请号：US346689
申请日：1989-05-03
申请人： Rudolf Schaulin
发明人： Rudolf Schaulin
IPC分类号： C09B56/14 , D06P3/54 , D06P3/62 , D06P1/39
CPC分类号： C09B56/14
摘要： The compounds of the formula ##STR1## in which the substituents and indices are as defined in claim 1, are green direct dyes for various substrates, in particular cellulosic fibre materials. They are stable to high temperatures and are therefore particularly suitable for the one-bath, one-stage dyeing of polyester/cotton mixed fabrics together with a disperse dye for the polyester fibres, under the dyeing conditions for polyester fibres.
摘要翻译：取代基和指数如权利要求1所定义的式（IMAG）化合物是用于各种底物的绿色直接染料，特别是纤维素纤维材料。它们对高温稳定，因此特别适用于在聚酯纤维的染色条件下，聚酯/棉混纺织物与聚酯纤维的分散染料一步染色一步染色。

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