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1. 发明授权

US06363728B1 System and method for controlled delivery of liquefied gases from a bulk source 有权
标题翻译：用于从大量源控制输送液化气体的系统和方法
公开(公告)号：US06363728B1
公开(公告)日：2002-04-02
申请号：US09597262
申请日：2000-06-20
申请人： Richard J. Udischas , Benjamin J. Jurcik , Hwa-Chi Wang , Robert G. Irwin
发明人： Richard J. Udischas , Benjamin J. Jurcik , Hwa-Chi Wang , Robert G. Irwin
IPC分类号： F17C704
CPC分类号： F17C7/04 , F17C9/02 , F17C2221/05 , F17C2223/013 , F17C2225/0123 , F17C2227/0369 , F17C2250/043 , F17C2250/0631 , F17C2270/0518 , Y02E60/321
摘要： Provided is a novel system and method for delivery of gas from a liquefied state. The system includes (a) a delivery vessel holding a bulk quantity of liquefied gas therein; (b) a heat exchanger disposed on the delivery vessel to provide or remove energy from the liquefied gas only; and (c) a pressure controller for monitoring and adjusting the energy delivered to the vessel. The system and method allow for controlled delivery of liquefied gas from a delivery vessel at a predetermined flow rate. Particular applicability is found in the delivery of gases to semiconductor process tools.
摘要翻译：提供了一种用于从液化状态输送气体的新型系统和方法。该系统包括（a）在其中容纳大量液化气体的输送容器; （b）设置在输送容器上以便仅提供或从液化气体中除去能量的热交换器; 和（c）压力控制器，用于监测和调节输送到船舶的能量。该系统和方法允许以预定流量从输送容器控制输送液化气体。在向半导体加工工具输送气体时发现了特殊的适用性。

2. 发明授权

US4158570A Preparing magnesium oxychloride and/or oxysulfate cements 失效
标题翻译：制备氯氧化镁和/或硫酸氢氧化物水泥
公开(公告)号：US4158570A
公开(公告)日：1979-06-19
申请号：US937297
申请日：1978-08-28
申请人： Robert G. Irwin
发明人： Robert G. Irwin
IPC分类号： C04B9/02 , C04B9/04
CPC分类号： C04B9/02 , C04B9/04
摘要： A method of preparing magnesium oxychloride and/or oxysulfate cements is described which involves the control of temperature of the magnesium chloride and/or sulfate solutions and the magnesium oxide used to prepare the cements during mixing and the controlled addition of the requisite amounts of magnesium oxide, magnesium chloride and/or sulfate required to form the cements during the mixing procedure. In mixing the requisite oxides with the sulfate and/or chloride solutions used to produce the cement mixtures, the oxide is mixed and thoroughly blended with at least 80 percent of the requisite chloride and/or sulfate solution required to provide a homogeneous mixture. After achieving the initial homogeneous mixture, the balance of the chloride and/or sulfate solution required to provide the requisite chemical constituents to form an oxychloride or oxysulfate cement is added and thoroughly blended to provide a second homogeneous mixture capable of forming a magnesium oxychloride or magnesium oxysulfate cement product upon setting.
摘要翻译：描述了制备氯氧化镁和/或硫酸氢氧化物水泥的方法，其涉及在混合期间控制氯化镁和/或硫酸盐溶液和用于制备水泥的氧化镁的温度，并且控制加入所需量的氧化镁，在混合过程中形成水泥所需的氯化镁和/或硫酸盐。在将所需的氧化物与用于生产水泥混合物的硫酸盐和/或氯化物溶液混合时，将氧化物与至少80％所需的氯化物和/或硫酸盐溶液混合并充分混合以提供均匀的混合物。在达到初始均匀混合物之后，加入提供所需化学成分以形成氯氧化物或硫酸氢氧化物粘合剂所需的氯化物和/或硫酸盐溶液的余量并充分混合以提供能够形成氯氧化镁或镁的第二均匀混合物氧硫酸盐水泥产品。

3. 发明授权

US5744676A Olefin oligomerization process 失效
标题翻译：烯烃低聚方法
公开(公告)号：US5744676A
公开(公告)日：1998-04-28
申请号：US606669
申请日：1996-02-26
申请人： Kevin J. Theriot , Robert G. Irwin
发明人： Kevin J. Theriot , Robert G. Irwin
IPC分类号： C07C2/20 , C07C2/08
CPC分类号： C07C2/20 , C07C2527/1213 , C07C2531/02
摘要： Alpha-olefin oligomers are produced by oligomerizing an alpha-olefin monomer with a catalyst system comprising boron trifluoride, a protic promoter, and a modifier which is (a) at least one 1,3-dioxolane, or (b) at least one 1,3-dioxane, or (c) a combination of (a) and (b). Use of these modifiers in the BF.sub.3 -catalyzed oligomerization makes it possible to modify the promoted catalytic reaction so that product containing as much as 50% or more of dimer can be produced at high conversions, at modest reaction temperatures, and in short reaction periods.
摘要翻译：通过用包含三氟化硼，质子促进剂和改性剂的催化剂体系使α-烯烃单体低聚来制备α-烯烃低聚物，所述改性剂是（a）至少一种1,3-二氧戊环，或（b）至少一种1 ，（c）（a）和（b）的组合。在BF 3催化的低聚反应中使用这些改性剂使得可以改进促进的催化反应，使得含有多达50％或更多二聚体的产物可在高转化率，适度的反应温度和短的反应时间内产生。

4. 发明授权

US5650548A Olefin oligomerization process 失效
标题翻译：烯烃低聚方法
公开(公告)号：US5650548A
公开(公告)日：1997-07-22
申请号：US491459
申请日：1995-06-16
申请人： Kevin J. Theriot , Robert G. Irwin
发明人： Kevin J. Theriot , Robert G. Irwin
IPC分类号： C07C2/20 , C07C2/08
CPC分类号： C07C2/20 , C07C2527/1213 , C07C2531/02
摘要： Alpha-olefin oligomer is prepared by contacting an alpha-olefin monomer which contains from about 6 to about 20 carbon atoms with a catalyst system comprising boron trifluoride, a protic promoter, and an organic sulfone, sulfoxide, carbonate, thiocarbonate, or sulfonate. Oligomer containing as much as 50% or more of dimer can be produced at high conversions, at modest reaction temperatures, and in acceptably short reaction periods.
摘要翻译：通过使含有约6至约20个碳原子的α-烯烃单体与包含三氟化硼，质子促进剂和有机砜，亚砜，碳酸酯，硫代碳酸酯或磺酸酯的催化剂体系接触来制备α-烯烃低聚物。含有多达50％或更多二聚体的低聚物可以在适度的反应温度和可接受的短的反应时间内以高转化率产生。

5. 发明授权

US5633420A Olefin oligomerization process 失效
标题翻译：烯烃低聚方法
公开(公告)号：US5633420A
公开(公告)日：1997-05-27
申请号：US532953
申请日：1995-09-22
申请人： Kevin J. Theriot , Robert G. Irwin
发明人： Kevin J. Theriot , Robert G. Irwin
IPC分类号： C07C2/20 , C07C2/08
CPC分类号： C07C2/20 , C07C2527/1213 , C07C2531/02
摘要： Alpha-olefin oligomers are prepared by a process which comprises contacting an oligomerizable olefin monomer with a catalyst system comprising a catalytic amount of boron trifluoride, a protic promoter, and an organic modifier selected from the group consisting of phosphate, thiophosphate, phosphine oxide, and phosphine sulfide. The oligomerizable olefin monomer is a C.sub.6 to C.sub.20 linear olefin comprising at least 50 mole % alpha olefin.
摘要翻译： α-烯烃低聚物通过以下方法制备，该方法包括将可低聚烯烃单体与包含催化量的三氟化硼，质子促进剂和选自磷酸酯，硫代磷酸酯，氧化膦和硫化磷。可低聚烯烃单体是包含至少50摩尔％α-烯烃的C 6至C 20直链烯烃。

6. 发明授权

US5347043A Process for preparing Michael addition products 失效
标题翻译：迈克尔加成产物的制备方法
公开(公告)号：US5347043A
公开(公告)日：1994-09-13
申请号：US169261
申请日：1993-12-20
申请人： Mahmood Sabahi , Robert G. Irwin
发明人： Mahmood Sabahi , Robert G. Irwin
IPC分类号： C07C67/343 , C07C69/34 , C07C67/00 , C07C67/465 , C07C69/38
CPC分类号： C07C67/343
摘要： Dialkyl malonate/alkyl acrylate Michael addition product mixtures having at least three acceptor moieties in a substantial number of the molecules can be consistently prepared without the need for long reaction times or the use of a large excess of the acceptor when the reaction is effected by gradually adding one molar proportion of a dialkyl malonate to at least three molar proportions of an alkyl acrylate which has been preheated to 60.degree.-80.degree. C. in admixture with an initiator and a phase transfer catalyst. In a preferred embodiment, the preheated mixture is maintained at 60.degree.-80.degree. C. for at least one hour before the dialkyl malonate is added in order to increase the percentage of product composed of the heavier components.
摘要翻译：丙二酸二烷基酯/丙烯酸烷基酯在相当数量的分子中具有至少三个受体部分的迈克尔加成产物混合物可以一致地制备，而不需要长的反应时间或当反应通过逐渐地进行反应时使用大量过量的受体将1摩尔比例的丙二酸二烷基酯加入到至少三摩尔比例的丙烯酸烷基酯中，该丙烯酸烷基酯与引发剂和相转移催化剂混合预热至60-80℃。在优选的实施方案中，将预热的混合物在加入丙二酸二烷基酯之前保持在60-80℃至少1小时以增加由较重组分组成的产物的百分比。

7. 发明授权

US5929297A Olefin oligomerization process 失效
标题翻译：烯烃低聚方法
公开(公告)号：US5929297A
公开(公告)日：1999-07-27
申请号：US936410
申请日：1997-09-25
申请人： Kevin J. Theriot , Robert G. Irwin
发明人： Kevin J. Theriot , Robert G. Irwin
IPC分类号： C07C2/20 , C07C2/04 , C07C2/02
CPC分类号： C07C2/20 , C07C2527/1213 , C07C2531/02
摘要： Alpha-olefin oligomers are produced by oligomering alpha-olefin monomer with a catalyst system comprising boron trifluoride, a protic promoter, and a special type of modifier. The modifier is a compound that satisfies the following criteria: (a) it has at least one moiety in which a carbonyl group is directly bonded to a nitrogen atom which is in turn bonded to two separate carbon atoms, (b) it is devoid of any nitrogen atom other than a nitrogen atom that is either (i) directly bonded to two separate carbon atoms and to a carbonyl group or (ii) is triply bonded to a single carbon atom, and (c) it is devoid of any protonic functional substituent. These modifiers control the oligomer product distribution and provide higher percentages of lower oligomers, especially dimers.
摘要翻译：通过用包含三氟化硼，质子促进剂和特殊类型的改性剂的催化剂体系低聚α-烯烃单体制备α-烯烃低聚物。改性剂是满足以下标准的化合物：（a）至少有一个部分，其中羰基直接键合到氮原子上，氮原子又连接到两个单独的碳原子上，（b）没有（i）直接键合到两个单独的碳原子和羰基的氮原子以外的任何氮原子或（ii）三键键合到单个碳原子上，（c）没有任何质子功能取代基。这些改性剂控制低聚物产物分布并提供较高百分比的低级低聚物，特别是二聚体。

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