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1. 发明授权

US3957431A Process for easy-care finishing cellulosics 失效
标题翻译：易于整理纤维素的方法
公开(公告)号：US3957431A
公开(公告)日：1976-05-18
申请号：US563179
申请日：1975-03-28
申请人： Panemangalore S. Pai , Harro Petersen , Friedrich Klippel
发明人： Panemangalore S. Pai , Harro Petersen , Friedrich Klippel
IPC分类号： D06M15/423 , D06M13/34
CPC分类号： D06M15/423
摘要： Process for the easy-care finishing of cellulosics involving low formaldehyde release, wherein the cellulosics, after having been impregnated with a solution of aminoplast-forming substances and dried, are sprayed with a solution of urea.
摘要翻译：涉及低甲醛释放的纤维素易于整理的方法，其中纤维素在用氨基塑料形成物质的溶液浸渍并干燥后，用尿素溶液喷雾。

2. 发明授权

US4207073A Textile finish and processes for its preparation and use 失效
标题翻译：纺织品的整理及其制备和使用过程
公开(公告)号：US4207073A
公开(公告)日：1980-06-10
申请号：US000815
申请日：1979-01-04
申请人： Harro Petersen , Panemangalore S. Pai , Manfred Reichert
发明人： Harro Petersen , Panemangalore S. Pai , Manfred Reichert
IPC分类号： C08L71/00 , C08L77/00 , D06M13/02 , D06M13/322 , D06M13/425 , D06M15/53 , D06M15/564 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/08 , D06M15/54
CPC分类号： D06M15/564
摘要： A process for the preparation of a textile finish, the textile finish thus obtained and its use for the easy-care finishing of textiles containing, or consisting of, cellulose. The textile finish comprises an aqueous solution, of from 30 to 70 percent strength by weight, of a mixture of the conventionally formaldehyde-methylolated carbamates I and II ##STR1## where R.sup.1 is hydrogen or alkyl of 1 to 4 carbon atoms and R.sup.2 and R.sup.3 are hydrogen, or one is hydrogen and the other is methyl, in the weight ratio I:II of from 12:1 to 1:20.The textile finish is prepared by reacting a glycol or an alkylglycol of the formulae III and IV ##STR2## where R.sup.1, R.sup.2 and R.sup.3 have the above meanings, with urea at above 100.degree. C., so as to eliminate ammonia and give carbamates, and subsequent conventional methylolation with formaldehyde, wherein, in a first stage, the glycol or alkylglycol of the formula III is reacted to the extent of at least 50% with urea, in the absence of a catalyst, at from 130.degree. to 160.degree. C., to give the carbamate I, and in a second stage, carried out either in the presence of an ion exchanger, containing nickel ions, as the catalyst, at from 130.degree. to 165.degree. C., or in the absence of a catalyst at from 150.degree. to 200.degree. C., the carbamate mixture in the weight ratio I:II of from 12:1 to 1:20, is prepared by addition of the glycol or alkylglycol of the formula IV and further urea.
摘要翻译：用于制备纺织品整理剂的方法，如此获得的纺织品整理剂及其用于容易地加工含纤维素或由纤维素组成的纺织品的用途。织物整理剂包含按重量计30％至70％的常规甲醛 - 羟甲基化氨基甲酸酯I和II II的混合物的水溶液，其中R1是氢或1-4个碳原子的烷基原子，R2和R3是氢，或者一个是氢，另一个是甲基，重量比I:II为12:1至1:20。通过使式III和IV的烷基二醇R 1（OCH 2 CH 2）9-100 OH III IV，其中R 1，R 2和R 3具有上述含义，与高于100℃的尿素反应制备纺织品整理剂。，以消除氨并产生氨基甲酸酯，以及随后与甲醛的常规羟甲基化反应，其中在第一阶段中，式III的二醇或烷基二醇与尿素的反应程度至少为50％，在不存在催化剂，在130℃至160℃下，得到氨基甲酸酯I，在第二阶段中，在含有镍离子的离子交换剂存在下，在130-165℃下进行催化剂或者在150℃至200℃下不存在催化剂时，重量比I:II的氨基甲酸酯混合物的重量比为12:1至1:20，通过加入二醇或烷基二醇式IV和另外的尿素。

3. 发明授权

US4795675A Enhanced transfer printability treatment method and composition 失效
标题翻译：增强转印可印性的处理方法和组成
公开(公告)号：US4795675A
公开(公告)日：1989-01-03
申请号：US155388
申请日：1988-02-12
申请人： Larson B. Dunn, Jr. , Kenneth B. Moser , Panemangalore S. Pai
发明人： Larson B. Dunn, Jr. , Kenneth B. Moser , Panemangalore S. Pai
IPC分类号： D06M15/03 , D06M13/16
CPC分类号： D06M15/03 , Y10T442/277
摘要： The transfer printability of fabric materials containing at least a minor proportion of cellulosic or natural proteinaceous fibers such as, for example, cotton, rayon, cellulose acetate, wool, silk, etc. is notably improved by a treatment in which said fabric material is impregnated with certain glycoside reagents. Especially preferred glycoside reagents for use in such treatment are C.sub.2 -C.sub.6 alkyl monoglucosides.
摘要翻译：含有至少少部分纤维素或天然蛋白质纤维（例如棉花，人造丝，醋酸纤维素，羊毛，丝绸等）的织物材料的转印印刷性通过其中所述织物材料浸渍的处理而显着改善与某些糖苷试剂。用于这种治疗的特别优选的糖苷试剂是C 2 -C 6烷基单葡糖苷。

4. 发明授权

US4781725A Enhanced transfer printability treatment method and composition 失效
标题翻译：增强转印可印性的处理方法和组成
公开(公告)号：US4781725A
公开(公告)日：1988-11-01
申请号：US908495
申请日：1986-09-17
申请人： Larson B. Dunn, Jr. , Kenneth B. Moser , Panemangalore S. Pai
发明人： Larson B. Dunn, Jr. , Kenneth B. Moser , Panemangalore S. Pai
IPC分类号： D06M15/03 , D06P1/00 , D06P1/16 , D06P3/14 , D06P3/62
CPC分类号： D06M15/03 , Y10S8/917 , Y10S8/918 , Y10S8/93
摘要： The transfer printability of fabric materials containing at least a minor proportion of cellulosic or natural proteinaceous fibers such as, for example, cotton, rayon, cellulose acetate, wool, silk, etc. is notably improved by a treatment in which said fabric material is impregnated with certain glycoside reagents. Especially preferred glycoside reagents for use in such treatment are C.sub.2 -C.sub.6 alkyl monoglucosides.
摘要翻译：含有至少少部分纤维素或天然蛋白质纤维（例如棉花，人造丝，醋酸纤维素，羊毛，丝绸等）的织物材料的转印印刷性通过其中所述织物材料浸渍的处理而显着改善与某些糖苷试剂。用于这种治疗的特别优选的糖苷试剂是C 2 -C 6烷基单葡糖苷。

5. 发明授权

US4295847A Finishing process for textiles 失效
标题翻译：纺织品整理流程
公开(公告)号：US4295847A
公开(公告)日：1981-10-20
申请号：US115264
申请日：1980-01-25
申请人： Harro Petersen , Panemangalore S. Pai , Manfred Reichert
发明人： Harro Petersen , Panemangalore S. Pai , Manfred Reichert
IPC分类号： D06M15/423 , D06M13/38 , D06M1/02 , D06M15/38 , D06M15/54
CPC分类号： D06M15/423
摘要： Process for finishing textiles of natural or regenerated cellulose, which have been pretreated with liquid ammonia, wherein the finishing agent used is an N-monomethylol compound or N-monoalkoxymethyl compound of 4-hydroxy- or 4-alkoxy-5,5-dimethylpropyleneurea. The process couples a high degree of finishing effect (in respect of improvement of the shrink resistance and wrinkle resistance) with only a very slight effect on the hand and especially on the tensile strength.
摘要翻译：已经用液氨预处理的天然或再生纤维素纺织品的方法，其中所用的整理剂是4-羟基或4-烷氧基-5,5-二甲基亚丙基脲的N-单羟甲基化合物或N-单烷氧基甲基化合物。该方法在手上具有非常轻微的效果，特别是拉伸强度，结合了高度的整理效果（关于提高抗收缩性和抗皱性）。

6. 发明授权

US5516338A Water-soluble titanium salt-tannin dyes and methods of use thereof 失效
标题翻译：水溶性钛盐单宁染料及其使用方法
公开(公告)号：US5516338A
公开(公告)日：1996-05-14
申请号：US377954
申请日：1995-01-25
申请人： Panemangalore S. Pai
发明人： Panemangalore S. Pai
IPC分类号： C09B57/10 , C09B61/00 , D06P1/22 , D06P1/41 , D06P1/651 , D06P1/653 , D06P1/673
CPC分类号： C09B61/00 , C09B57/10 , D06P1/65118 , D06P1/653 , D06P1/67341 , D06P1/6735 , D06P1/67358 , D06P1/228 , D06P1/41
摘要： An aqueous dye composition is based upon a mixture of a water-soluble titanium salt, preferably titanium potassium oxalate and a tannin substance, preferably Myrobalan extract. This dye composition may be used to dye either natural fibers, synthetic fibers or blends thereof. The composition is particularly advantageous for either bottom dyeing denim fabric which can then be overdyed with indigo blue dye to provide blue-green hues or as a mordant for a basic dye.
摘要翻译：水性染料组合物基于水溶性钛盐，优选草酸钛钾和单宁物质，优选麝香草提取物的混合物。该染料组合物可用于染料天然纤维，合成纤维或其混合物。该组合物对于任何底部染色牛仔布织物特别有利，然后可以用靛蓝染料将其染色以提供蓝绿色调，或作为碱性染料的媒染剂。

7. 发明授权

US4331438A Process for eliminating free formaldehyde in textile materials treated with dimethylolated carbamates 失效
标题翻译：用二羟甲基化氨基甲酸酯处理的纺织材料中消除游离甲醛的方法
公开(公告)号：US4331438A
公开(公告)日：1982-05-25
申请号：US205490
申请日：1980-11-10
申请人： Panemangalore S. Pai
发明人： Panemangalore S. Pai
IPC分类号： D06M15/423 , D06M13/40
CPC分类号： D06M15/423
摘要： A process for elimination of free formaldehyde in textile materials treated with methylolated carbamates is disclosed. Textile materials comprising natural or regenerated cellulose are impregnated in the usual way with a dimethylolated carbamate. After impregnation, drying and curing, at least one side of the treated textile material is treated with a combination of a volatile inert carrier and a formaldehyde acceptor such as urea, ethylene urea, or propylene urea.
摘要翻译：公开了用羟甲基化氨基甲酸酯处理的纺织材料中消除游离甲醛的方法。包含天然或再生纤维素的纺织材料以通常的方式用二羟甲基化氨基甲酸酯浸渍。在浸渍，干燥和固化之后，处理的纺织材料的至少一面用挥发性惰性载体和甲醛受体如脲，亚乙基脲或丙烯脲的组合进行处理。

8. 发明授权

US4314806A Textile finish and processes for its preparation and use 失效
标题翻译：纺织品的整理及其制备和使用过程
公开(公告)号：US4314806A
公开(公告)日：1982-02-09
申请号：US184814
申请日：1980-09-08
申请人： Harro Petersen , Panemangalore S. Pai , Manfred Reichert
发明人： Harro Petersen , Panemangalore S. Pai , Manfred Reichert
IPC分类号： D06M15/423 , D06M15/54
CPC分类号： D06M15/423
摘要： A process for the preparation of a textile finish, the finish thus obtained and its use for the easycare finishing of textiles containing, or consisting of, cellulose. The finish comprises an aqueous solution, of from 30 to 70 percent strength by weight, of a mixture of the conventionally methyloloated(=hydroxymethylated) carbamates I and II ##STR1## where R is hydrogen or alkyl of 1 to 4 carbon atoms, in the weight ratio I:II of from 1:1 to 1:20. The finish is prepared by reacting a glycol or an alkylglycol of the formula IIIR--(OCH.sub.2 --CH.sub.2).sub.9-100 --OH IIIwhere R has the above meanings, and isobutanol with urea at above 100.degree. C., so as to eliminate ammonia and produce carbamates, and methylolation with formaldehyde. In a first stage, the glycol or alkylglycol of the formula III is reacted to the extent of at least 50% with urea, in the absence of a catalyst, at from 130 to 160.degree. C., to give the carbamate I, and in a second stage, carried out either in the presence of an ion exchanger containing nickel ions at from 130.degree. to 165.degree. C., or in the absence of a catalyst at from 150.degree. to 200.degree. C., the carbamate mixture in the weight ratio I:II of from 1:1 to 1:20 is prepared by addition of isobutanol and further urea.
摘要翻译：用于制备纺织品整理剂的方法，由此获得的成品及其用于容纳纤维素或由纤维素组成的纺织品的易擦洗的用途。整理剂包含30-70重量％的重量比的常规甲基化（=羟甲基化）氨基甲酸酯I和II II的混合物的水溶液，其中R是氢或1-4个碳原子的烷基碳原子，重量比I:I为1:1至1:20。通过使式III R-（OCH 2 -CH 2）9-100-OHIII的二醇或烷基二醇（其中R具有上述含义）与异丁醇与脲在高于100℃下反应制备完成物，以便除去氨并产生氨基甲酸酯，并与甲醛进行羟甲基化反应。在第一阶段中，式III的二醇或烷基二醇在不存在催化剂的情况下在130-160℃下与尿素反应至少50％，得到氨基甲酸酯I，并且在第二阶段是在含有130-165℃的镍离子的离子交换剂存在下进行，或在不存在催化剂的情况下在150℃至200℃下进行，重量的氨基甲酸酯混合物通过加入异丁醇和另外的尿素制备1:1:1至1:20的比例I：II。

9. 发明授权

US4295846A Process for the production of formaldehyde-free finishing agents for cellulosic textiles and the use of such agents 失效
标题翻译：用于生产无纺织物的无甲醛整理剂的方法和这种试剂的使用
公开(公告)号：US4295846A
公开(公告)日：1981-10-20
申请号：US131409
申请日：1980-03-18
申请人： Harro Petersen , Panemangalore S. Pai , Friedrich Klippel , Friedrich Reinert
发明人： Harro Petersen , Panemangalore S. Pai , Friedrich Klippel , Friedrich Reinert
IPC分类号： C07D233/40 , D06M15/423 , D06M13/34
CPC分类号： D06M15/423 , C07D233/40
摘要： Process for the production of formaldehyde-free finishing agents for textiles containing or consisting of cellulose which is based on the reaction of urea or symmetrically disubstituted urea with glyoxal in the presence of buffer salts and alcohols at a pH of below 7, buffered mixtures of 4,5-hydroxyethyleneureas or N,N'-disubstituted 4,5-dihydroxyethyleneureas partially etherified in 4- and 5-positions being formed.
摘要翻译：用于生产含有纤维素或由纤维素组成的织物的无甲醛整理剂的方法，其基于在pH7以下的缓冲盐和醇的存在下脲或对称二取代的脲与乙二醛的反应，缓冲的4 形成5-羟基亚乙基脲或N，N'-二取代的4,5-二羟基亚乙基脲在部分醚化的4-和5-位。

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