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    • 2. 发明授权
    • Method of making lithium metal oxide cathode active material
    • 制备锂金属氧化物正极活性物质的方法
    • US5520903A
    • 1996-05-28
    • US152770
    • 1993-11-15
    • On K. ChangJoseph Lundquist
    • On K. ChangJoseph Lundquist
    • C01G31/00H01M4/131H01M4/48H01M4/485H01M10/052H01M10/36
    • H01M4/485C01G31/00H01M10/052H01M4/131Y02P70/54
    • A method of making a composition having lithium, transition metal and oxygen elements and preferably having vanadium as the transition metal with a unit structure of the nominal general formula LiV.sub.3 O.sub.8, such structure being able to accept lithium ions. The method as exemplified by the formation of Li.sub.1+x V.sub.3 O.sub.8 (0.ltoreq.x.ltoreq.0.2) comprises forming a mixture of intermingled particles of vanadium pentoxide (V.sub.2 O.sub.5) and lithium carbonate (Li.sub.2 CO.sub.3) each in an amount sufficient to provide a stoichiometric ratio of approximately 1:3 of lithium to vanadium respectively; compacting the particles by applying a compressive force to the intermingled particles; and heating the intermingled particles to an elevated temperature which is below the melting point of the LiV.sub.3 O.sub.8 product of the invention. The compacting and heating steps consolidate the particles into a densified body and cause diffusion of at least a portion of the elements across particle boundaries with release of carbon dioxide, thereby providing a lithium-vanadium-oxygen composition having a unit structure of Li.sub.1+x V.sub.3 O.sub.8.
    • 制备具有锂,过渡金属和氧元素并优选具有钒作为过渡金属的组合物的方法,其具有标称通式LiV 3 O 8的单元结构,该结构能够接受锂离子。 通过形成Li1 + xV3O8(0≤x≤0.2)例示的方法包括形成混合的五氧化二钒(V 2 O 5)和碳酸锂(Li 2 CO 3)的混合物,其量足以提供化学计量 锂的比例约为1:3; 通过向混合的颗粒施加压缩力来压实颗粒; 并将混合的颗粒加热到低于本发明的LiV 3 O 8产物的熔点的升高温度。 压实和加热步骤将颗粒固结成致密化体,并导致至少一部分元素在释放二氧化碳的情况下跨越颗粒边界扩散,从而提供具有Li1 + xV3O8单元结构的锂 - 钒 - 氧组合物。
    • 4. 发明授权
    • Method of state-of-charge indication by measuring the thickness of a
battery
    • 通过测量电池厚度的充电状态指示方法
    • US5438249A
    • 1995-08-01
    • US271247
    • 1994-07-07
    • On K. ChangCharles A. Lung
    • On K. ChangCharles A. Lung
    • H01M10/48
    • H01M10/488G01R31/3606
    • The state of charge of a cell that has flexible packaging and that expands and contracts with variations in state of charge is determined by measuring changes in thickness of the cell. The invention is particularly applicable to cells having a flat geometry. A battery having a state-of-charge indicator includes at least one battery cell free to expand and contract with variations in state of charge of the battery cell and a device for measuring expansion or contraction of the battery cell, a resulting measurement indicating the state of charge of the battery cell. By measuring expansion or contraction of the battery the state of charge of a battery may be readily detected. The measurement may be directly displayed so as to be visually observable, or a signal containing measurement information may be sent to a remote location to be displayed or used for control purposes. Expansion or contraction of the battery may be measured in various ways, including measuring physical displacement of the cell package or measuring a change in pressure exerted upon a member as a result of the expansion or contraction of the battery.
    • 通过测量电池厚度的变化来确定具有柔性包装并且随着充电状态的变化而膨胀和收缩的电池的充电状态。 本发明特别适用于具有平坦几何形状的细胞。 具有充电状态指示器的电池包括至少一个电池单元,所述至少一个电池单元随着电池单元的充电状态的变化和用于测量电池单元的膨胀或收缩的装置的变化而自由膨胀和收缩,所得的测量指示状态 的电池电量。 通过测量电池的膨胀或收缩,可以容易地检测电池的充电状态。 可以直观地显示测量以便可视地观察,或者可以将包含测量信息的信号发送到远程位置以被显示或用于控制目的。 可以以各种方式测量电池的膨胀或收缩,包括测量电池组件的物理位移或测量由于电池的膨胀或收缩而施加在构件上的压力变化。
    • 5. 发明授权
    • Device for determining mechanical properties of materials
    • 用于确定材料的机械性能的装置
    • US5357786A
    • 1994-10-25
    • US101871
    • 1993-08-04
    • Charles A. LungOn K. Chang
    • Charles A. LungOn K. Chang
    • G01N3/06G01N3/42G01N3/48
    • G01N3/42G01N2203/0676
    • There is provided a method for measuring and evaluating hardness or toughness of relatively delicate materials such as polymers, semi-solids, colloids or gels to determine the firmness thereof by inserting a stylus a specific depth into the material and then determining how the material itself reacts by measuring a resultant opposing force caused by insertion of the stylus. The device used in the method of the invention comprises a stylus (plunger) to vertically impinge on the sample when the stylus is displaced vertically downward. An actuating means controls downward movement of the stylus. The actuating means comprises a movable shaft and a stationary sleeve. The shaft has one end which is threaded and a second end which is constructed and arranged to carry the stylus. The stationary sleeve has internal threads for cooperative engagement with the external threads of the shaft, whereby adjustment by the threads causes vertical movement of the stylus.
    • 提供了一种用于测量和评估诸如聚合物,半固体,胶体或凝胶之类的相对精细材料的硬度或韧性的方法,以通过将触针插入到材料中的特定深度,然后确定材料本身如何反应来确定其硬度 通过测量由触针的插入引起的相反的力。 在本发明的方法中使用的装置包括当触针垂直向下移动时垂直地撞击样品的触针(柱塞)。 致动装置控制触笔的向下运动。 致动装置包括可动轴和静止套筒。 轴的一端是螺纹的,第二端被构造和布置成承载触针。 固定套筒具有用于与轴的外螺纹协调接合的内螺纹,由此螺纹的调节引起触针的垂直运动。