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1. 发明申请

WO2009045759A1 MONOMER SOLUTION FOR PRODUCING POLYCARBONATE 审中-公开
标题翻译：用于生产聚碳酸酯的单体解决方案
公开(公告)号：WO2009045759A1
公开(公告)日：2009-04-09
申请号：PCT/US2008/077060
申请日：2008-09-19
申请人： SABIC INNOVATIVE PLASTICS IP BV , BRACK, Hans-Peter , CAMPMAN, Maarten, Antoon, Jan , OYEVAAR, Martin Herke , PEREZ DE DIEGO, Yohana , VAN DER WEKKE, Laurus , WILLEMSE, Dennis James Patrick Maria
发明人： BRACK, Hans-Peter , CAMPMAN, Maarten, Antoon, Jan , OYEVAAR, Martin Herke , PEREZ DE DIEGO, Yohana , VAN DER WEKKE, Laurus , WILLEMSE, Dennis James Patrick Maria
IPC分类号： C08G64/30
CPC分类号： C08G64/307 , C08G64/30 , Y10T436/144444 , Y10T436/17 , Y10T436/173845
摘要： A non-reactive monomer mixture is formed from a dihydroxy component having one or more dihydroxy compounds dissolved in a melted diaryl carbonate. The dihydroxy component has one or more dihydroxy compounds with a melting point above the melting point of the diaryl carbonate. The dihydroxy component has less than 600 ppb alkali metal, an acid stabilizer, or both less than 600 ppb alkali metal and an acid stabilizer. The dihydroxy compounds of the dihydroxy component and the diaryl carbonate are present in a mole ratio of from 0.9 to 1.1. The monomer mixture is at a temperature between the saturation point of the monomer mixture and the highest melting temperature of the individual dihydroxy compounds. The non-reactive monomer mixture can be stored and transported and then polymerized to form polycarbonate upon addition of a catalyst.
摘要翻译：非反应性单体混合物由具有溶解在熔融的碳酸二芳基酯中的一种或多种二羟基化合物的二羟基组分形成。二羟基组分具有一种或多种熔点高于碳酸二芳基酯的熔点的二羟基化合物。二羟基组分具有少于600ppb的碱金属，酸稳定剂，或两者少于600ppb的碱金属和酸稳定剂。二羟基成分和碳酸二芳基酯的二羟基化合物的摩尔比为0.9-1.1。单体混合物处于单体混合物的饱和点和各个二羟基化合物的最高熔融温度之间的温度。非反应性单体混合物可以储存和运输，然后在加入催化剂时聚合形成聚碳酸酯。

2. 发明申请

WO2008140531A1 PROCESS FOR THE PRODUCTION OF POLYCARBONATE USING AN ESTER SUBSTITUTED DIARYL CARBONATE 审中-公开
标题翻译：使用酯取代的二元碳酸酯生产聚碳酸酯的方法
公开(公告)号：WO2008140531A1
公开(公告)日：2008-11-20
申请号：PCT/US2007/075271
申请日：2007-08-06
申请人： GENERAL ELECTRIC COMPANY , BELFADHEL, Hatem , BRACK, Hans-peter , FERNANDEZ, Ignacio, Vic , GARCIA AGUDO, Jorge , DE GROOTH, Joris , HIDALGO, Llinas, Gerardo , MCCLOSKEY, Patrick, Joseph , OBANDO, Louis , OYEVAAR, Martin, Herke , VAN DER WEKKE, Laurus , WILLEMSE, Dennis
发明人： BELFADHEL, Hatem , BRACK, Hans-peter , FERNANDEZ, Ignacio, Vic , GARCIA AGUDO, Jorge , DE GROOTH, Joris , HIDALGO, Llinas, Gerardo , MCCLOSKEY, Patrick, Joseph , OBANDO, Louis , OYEVAAR, Martin, Herke , VAN DER WEKKE, Laurus , WILLEMSE, Dennis
IPC分类号： C08G64/06 , C08G64/30
CPC分类号： C08G64/307
摘要： A method of preparing polycarbonate includes a steps of providing a melt reaction mixture and allowing the melt reaction mixture to react to build molecular weight, thereby preparing the polycarbonate. The melt reaction mixture has a dihydroxy compound, an ester substituted diaryl carbonate mixture, and a melt trans esterification catalyst where the ester substituted diaryl carbonate mixture may contain acidsubstituted phenol. The method also includes the step of adjusting the molar ratio of acid-substituted phenol, if present, to melt transesterification catalyst (acid-substituted phenol/catalyst) in the melt reaction mixture to an amount of less than 10.
摘要翻译：制备聚碳酸酯的方法包括提供熔融反应混合物并允许熔融反应混合物反应以构建分子量的步骤，从而制备聚碳酸酯。熔融反应混合物具有二羟基化合物，酯取代的碳酸二芳酯混合物和熔体反式酯化催化剂，其中酯取代的碳酸二芳酯混合物可含有酸取代的苯酚。所述方法还包括如下步骤：将熔融反应混合物中的酯交换催化剂（酸取代的苯酚/催化剂）熔融至少于10的量的酸取代的苯酚（如果存在的话）的摩尔比。

3. 发明申请

WO2004058673A1 PROCESS FOR MANUFACTURE OF BISPHENOLS 审中-公开
标题翻译：双酚的制备方法
公开(公告)号：WO2004058673A1
公开(公告)日：2004-07-15
申请号：PCT/US2003/040436
申请日：2003-12-17
申请人： GENERAL ELECTRIC COMPANY , OYEVAAR, Martin, Herke , PEEMANS, Rudy, Francois, Alain, Jos , SCHLARMANN, Eduard, Hendricus
发明人： OYEVAAR, Martin, Herke , PEEMANS, Rudy, Francois, Alain, Jos , SCHLARMANN, Eduard, Hendricus
IPC分类号： C07C37/20
CPC分类号： C07C37/84 , C07C37/20 , C07C39/16
摘要： A method for the manufacture of bisphenols comprises introducing a combined feed stream comprising a feed stream and a recycle stream into a reactor system comprising at least one reactor containing a catalytic proportion of an acid catalyst and wherein the combined feed stream comprises a carbonyl compound and a stoichiometric excess of phenol; removing from the reactor system a reactor effluent; splitting the reactor effluent into a crystallization feed stream and an effluent recycle stream; extracting from said crystallization feed stream a bisphenol adduct, remainder comprising a mother liquor stream; dehydrating said mother liquor stream and said effluent recycle stream in a dehydrator wherein excess water and carbonyl compound are removed; and recycling the dehydrated mother liquor and the dehydrated effluent recycle stream back to the combined feed stream to effect improved production of p,p-bisphenol, along with increased reactor selectivity and reduced promoter quantities.
摘要翻译：制备双酚的方法包括将包含进料流和再循环料流的组合进料流引入包含至少一个含有催化剂比例的酸催化剂的反应器的反应器系统中，其中组合进料流包含羰基化合物和化学计量过量的苯酚; 从反应器系统中除去反应器流出物; 将反应器流出物分解成结晶进料流和流出物再循环流; 从所述结晶进料流中提取双酚加合物，其余包含母液流; 在脱水器中脱水所述母液流和所述废水再循环流，其中除去过量的水和羰基化合物; 并将脱水的母液和脱水的废液再循环物流再循环回到组合的进料流中，以改善p，p双酚的生产，同时增加反应器的选择性和减少的助催化剂量。

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