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1. 发明授权

US5028478A Fiber reinforced composite materials having resin practice inter-layer zones 失效
标题翻译：具有树脂实践层间区域的纤维增强复合材料
公开(公告)号：US5028478A
公开(公告)日：1991-07-02
申请号：US137720
申请日：1987-12-24
申请人： Nobuyuki Odagiri , Shigeru Suzue , Hajime Kishi , Takeji Nakae , Akimitsu Matsusaki
发明人： Nobuyuki Odagiri , Shigeru Suzue , Hajime Kishi , Takeji Nakae , Akimitsu Matsusaki
IPC分类号： C08J5/24
CPC分类号： C08J5/24 , F17C2209/2154 , Y10S428/902 , Y10T428/24994 , Y10T428/254 , Y10T428/26 , Y10T428/31551 , Y10T428/31562 , Y10T428/31721 , Y10T428/31725 , Y10T428/31786 , Y10T442/3545
摘要： Tough laminated composite material which comprise (A) long reinforcing fibers, (B) a matrix resin mixed with the long reinforcing fibers and (C1) a resin, preferably in the form of fine resin particles, forming a phase separate from said matrix resin which is localized in inter-layer zones, wherein 90% or more of said resin (C1) is localized in inter-layer zones and/or wherein the border length factor in the inter-layer zones is 2.5 or more and prepegs used to form the composite materials.

2. 发明授权

US07208228B2 Epoxy resin for fiber reinforced composite materials 有权
标题翻译：纤维增强复合材料用环氧树脂
公开(公告)号：US07208228B2
公开(公告)日：2007-04-24
申请号：US10420776
申请日：2003-04-23
申请人： James E. Brown , Norimitsu Natsume , Nobuyuki Odagiri , Jeffrey J. Hawkey , Brian S. Hayes
发明人： James E. Brown , Norimitsu Natsume , Nobuyuki Odagiri , Jeffrey J. Hawkey , Brian S. Hayes
IPC分类号： B32B27/38 , B32B27/04 , B32B27/18 , C08L63/00
CPC分类号： C08J5/24 , C08J2363/00 , C08L63/00 , Y10T428/24994 , Y10T428/31511 , Y10T428/31525 , C08L2666/04
摘要： An epoxy resin composition for a cured material, comprising (A) an epoxy resin comprising an epoxy compound X, the epoxy compound X has an epoxy equivalent weight of at least 400, (B) a curing agent, and (C) a liquid rubber that is liquid at room temperature and comprises a reactive group; wherein the epoxy compound X has a solubility parameter value of SpX, the liquid rubber has a solubility parameter value of SpY and the ratio of SpY/SpX could be in the range of 0.7 to 1.3; and wherein the liquid rubber could form no visible domains by optical microscopy or has a maximum domain size of at most 3 microns in the cured material is described. The epoxy resin composition provides a fiber-reinforced material with higher compressive modulus and strength, toughness and better handling ability over standard epoxy resin systems. This invention is excellent for small thin walled tube structures like fishing rods or applications that require good compressive strength.
摘要翻译：一种用于固化材料的环氧树脂组合物，其包含（A）环氧树脂，其包含环氧化合物X，环氧化合物X的环氧当量为至少400，（B）固化剂，和（C）液体橡胶在室温下为液体，包含反应性基团; 其中环氧化合物X具有SpX的溶解度参数值，液体橡胶具有SpY的溶解度参数值，SpY / SpX的比例可以在0.7至1.3的范围内; 并且其中液体橡胶可以通过光学显微镜不形成可见结构域，或者在固化材料中具有至多3微米的最大结构域尺寸。环氧树脂组合物提供了比标准环氧树脂体系更高的压缩模量和强度，韧性和更好的处理能力的纤维增强材料。本发明对于诸如钓鱼杆或需要良好抗压强度的应用的小型薄壁管结构来说是非常好的。

3. 发明授权

US5543212A Prepregs comprising a reinforcing fiber layer, a knitted fabric of thermoplastic fibers and a matrix resin 失效
标题翻译：包含增强纤维层，热塑性纤维的针织物和基质树脂的预浸料
公开(公告)号：US5543212A
公开(公告)日：1996-08-06
申请号：US339599
申请日：1994-11-14
申请人： Hiroki Oosedo , Nobuyuki Odagiri
发明人： Hiroki Oosedo , Nobuyuki Odagiri
IPC分类号： B29B11/16 , B29C70/08 , B32B5/12 , B32B5/14 , B32B27/04 , C08J5/04 , C08J5/24 , D03D3/00 , B32B5/02 , B32B7/00
CPC分类号： C08J5/24 , B29C70/083 , B32B5/12 , C08J5/047 , B29K2101/10 , B29K2105/08 , B29K2105/0836 , B29K2301/12 , Y10S428/902 , Y10T442/494
摘要： The present invention relating to prepegs has the following constitution to achieve the above object. That is, a prepreg, comprising long reinforcing fibers [A], matrix resin [B] and a knitted fabric made from thermoplastic resin fibers [C], with the component [C] distributed near either or both of the surface layers. Moreover, the present invention relating to processes for production of prepregs has either of the following constitution to achieve the above object. That is, a process for preparing a prepreg, comprising the steps of impregnating long reinforcing fibers [A] with matrix resin [B], and bonding a knitted fabric made from thermoplastic resin fibers [C] onto one side or both sides of the intermediate product, or a process for preparing a prepreg, comprising the step of bonding matrix resin [B] formed as a film, a knitted fabric made from thermoplastic resin fibers [C] and long reinforcing fibers [A]. The prepregs of the present invention, therefore, are tacky and drapable, and the composite materials obtained by heating and forming the prepregs are high in heat resistance, and very high in impact resistance and inter-layer toughness. Furthermore, the prepregs are easy to produce and high in their latitude in availability of materials, this being industrially significant.
摘要翻译：涉及预制物的本发明具有以下结构以实现上述目的。也就是说，包含长增强纤维[A]，基质树脂[B]和由热塑性树脂纤维[C]制成的针织物的预浸料，其中组分[C]分布在表面层的一个或两个附近。此外，与制造预浸料坯的方法相关的本发明具有以下结构以实现上述目的。也就是说，制备预浸料的方法包括以下步骤：用基质树脂[B]浸渍长增强纤维[A]，并将由热塑性树脂纤维[C]制成的针织物粘合到中间体的一侧或两侧产品或制备预浸料的方法，包括将由热塑性树脂纤维[C]和长增强纤维[A]制成的针织物与作为膜形成的基质树脂[B]接合的步骤。因此，本发明的预浸料具有粘性和悬垂性，通过加热和形成预浸料获得的复合材料的耐热性高，耐冲击性和层间韧性非常高。此外，预浸料容易生产，在材料可用性方面的纬度高，这在工业上是显着的。

4. 发明授权

US5413847A Prepreg and composite 失效
标题翻译：预浸料和复合材料
公开(公告)号：US5413847A
公开(公告)日：1995-05-09
申请号：US38102
申请日：1993-03-30
申请人： Hajime Kishi , Atsushi Ozaki , Nobuyuki Odagiri
发明人： Hajime Kishi , Atsushi Ozaki , Nobuyuki Odagiri
IPC分类号： B29C70/02 , C08J5/24 , B32B5/16
CPC分类号： C08J5/24 , B29C70/025 , B29K2995/0089 , Y10S428/902 , Y10T428/2918 , Y10T428/30 , Y10T442/2082 , Y10T442/673
摘要： A prepreg and a composite prepared from the prepreg having high impact resistance, high interlayer toughness and high tensile strength are disclosed. The prepreg comprises the following elements [A], [B] and [C]:[A]: reinforcing fibers;[B]: a resin composition including a thermosetting resin and a thermoplastic resin which is soluble in said thermosetting resin, which resin composition being capable of forming a micro-phase separation structure; and[C]: fine particles which are insoluble in said element [B] and which do not contain an elastomer component;said element [C] being localized in a surface of said prepreg. The present invention also provides a composite prepared from this prepreg.
摘要翻译：公开了一种由具有高耐冲击性，高层间韧性和高拉伸强度的预浸料制备的预浸料和复合材料。预浸料包括以下元件[A]，[B]和[C]：[A]：增强纤维; [B]：可溶于所述热固性树脂的热固性树脂和热塑性树脂的树脂组合物，该树脂组合物能够形成微相分离结构; 和[C]：不溶于所述元素[B]并且不含弹性体组分的细颗粒; 所述元素[C]定位在所述预浸料坯的表面中。本发明还提供了由该预浸料制备的复合材料。

5. 发明授权

US06117551A Carbon fiber prepreg, and a production process thereof 有权
标题翻译：碳纤维预浸料及其制造方法
公开(公告)号：US06117551A
公开(公告)日：2000-09-12
申请号：US125124
申请日：1998-08-11
申请人： Hideo Nagata , Nobuyuki Odagiri , Takeshi Terashita , Hajime Kishi , Shoji Yamane
发明人： Hideo Nagata , Nobuyuki Odagiri , Takeshi Terashita , Hajime Kishi , Shoji Yamane
IPC分类号： B29B11/16 , B29B15/10 , C08J5/24 , C08L63/00 , B32B5/16 , B32B9/06 , B32B31/20
CPC分类号： C08J5/24 , B29B15/105 , C08L63/00 , B29K2307/00 , C08J2363/00 , C08J2477/00 , C08J2481/06 , Y10T428/24994 , Y10T428/254 , Y10T428/30 , Y10T428/31511 , Y10T428/31551
摘要： The present invention relates to a carbon fiber prepreg. The carbon fiber prepreg of the present invention is characterized in that a carbon fiber bundle comprising a plurality of continuous carbon filaments and having a hook drop value of 10 cm or more as the degree of fiber entanglement is impregnated with a base resin mainly composed of a thermosetting resin, and that particles of 150 .mu.m or less in particle size made of a thermoplastic resin account for 20 wt % or less based on the weight of the entire prepreg and distributed at a higher concentration in the surface zone than in the inside. The carbon fiber prepreg of the present invention is good in tackiness and less changing in tackiness with the lapse of time, and can form a composite with an excellent compression interlaminar shear strength (CILS) at high temperature after moisture absorption while maintaining good impact resistance. It also allows the production of a composite very higher than the conventional composite in the compressive strength (LCS) of a cross laminated panel. The carbon fiber prepreg of the present invention can be preferably used as a structural member in such areas as aerospace area, sporting area and civil engineering and architecture area.
摘要翻译： PCT No.PCT / JP97 / 04642 Sec。 371日期：1998年8月11日 102（e）日期1998年8月11日PCT 1997年12月16日PCT公布。第WO98 / 26912号公报日期：1998年6月25日本发明涉及一种碳纤维预浸料。本发明的碳纤维预浸料的特征在于，将包含多个连续碳纤丝并且具有10cm以上的钩滴值作为纤维缠结度的碳纤维束浸渍在主要由热可塑性树脂，由热塑性树脂制成的粒径为150μm以下的粒子相对于整个预浸料坯的重量为20重量％以下，分散在表面区域的浓度高于内部。本发明的碳纤维预浸料随着时间的推移粘合性和粘合性变化小，能够在保持良好的耐冲击性的同时，在高温下形成具有优异的压缩层间剪切强度（CILS）的复合体。它还允许在交叉层压板的抗压强度（LCS）中生产比常规复合材料高得多的复合材料。本发明的碳纤维预浸料可以优选用作航空航天领域，体育用地，民用建筑领域等的结构构件。

6. 发明授权

US5626916A Cloth prepreg, process for producing the same and reinforcing fabric 失效
标题翻译：布料预浸料，其生产方法和增强织物
公开(公告)号：US5626916A
公开(公告)日：1997-05-06
申请号：US594848
申请日：1996-01-31
申请人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
发明人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
IPC分类号： B29C70/08 , C08J5/04 , C08J5/24 , C08L63/00 , D03D15/00 , B05D3/02
CPC分类号： D03D15/00 , B29C70/08 , C08J5/042 , C08J5/24 , C08L63/00 , D03D15/0011 , D03D15/12 , D06C29/00 , B29K2105/0809 , C08J2363/00 , D10B2101/06 , D10B2101/12 , D10B2331/021 , D10B2401/063 , D10B2505/02 , Y10S428/902 , Y10S8/16 , Y10T428/30 , Y10T442/2008 , Y10T442/2098 , Y10T442/2951 , Y10T442/2984 , Y10T442/3065
摘要： Disclosed is a process of producing a prepreg which is suited for preparing honeycomb sandwich panels, by which the formation of pores in the interlayer zones in the cured composite can be reduced. The prepreg comprises a resin composition including an epoxy resin, a curing agent and a solid rubber, and a woven fabric made of reinforcing fibers, the meshes of the woven fabric being crushed such that said prepreg has a cover factor K.sub.p of 97-99.9%. Also disclosed is a reinforcing fabric comprising warps and woofs which are multifilament yarns made of carbon fibers, the widths W (mm) and finenesses D (d:denier) of the warp and woof satisfying the equation of:W=k.multidot.(D/.rho.).sup.5/9(wherein k represents 3.5.times.10.sup.-2 -10.0.times.10.sup.-2 (mm.multidot.d.sup.-5/9) and .rho. represents specific gravity of said carbon fibers), the woven fabric having a cover factor K.sub.c of 90.0-99.8%.
摘要翻译：公开了一种制备适于制备蜂窝夹层板的预浸料坯的方法，通过该方法可以减少固化复合材料中的夹层区域中的孔隙的形成。预浸料包括一种包括环氧树脂，固化剂和固体橡胶的树脂组合物和由增强纤维制成的机织织物，织物的网格被压碎，使得所述预浸料的覆盖系数Kp为97-99.9％。还公开了包括经纱和纬纱的增强织物，其是由碳纤维制成的复丝纱线，纬纱的宽度W（mm）和细度D（d：旦尼尔）满足以下等式：W = kx（D / rho ）+ E，fra 5/9 + EE（其中k表示3.5×10 -2 -10.0×10 -2（mm×d-+ E，fra 5/9 + EE），rho表示所述碳纤维的比重），织物覆盖系数Kcof为90.0-99.8％。

7. 发明授权

US5616405A Cloth prepreg, process for producing the same and reinforcing fabric 失效
标题翻译：布料预浸料，其生产方法和增强织物
公开(公告)号：US5616405A
公开(公告)日：1997-04-01
申请号：US368671
申请日：1995-01-04
申请人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
发明人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
IPC分类号： B29C70/08 , C08J5/04 , C08J5/24 , C08L63/00 , D03D15/00 , B32B5/16
CPC分类号： D03D15/00 , B29C70/08 , C08J5/042 , C08J5/24 , C08L63/00 , D03D15/0011 , D03D15/12 , D06C29/00 , B29K2105/0809 , C08J2363/00 , D10B2101/06 , D10B2101/12 , D10B2331/021 , D10B2401/063 , D10B2505/02 , Y10S428/902 , Y10S8/16 , Y10T428/30 , Y10T442/2008 , Y10T442/2098 , Y10T442/2951 , Y10T442/2984 , Y10T442/3065
摘要： Disclosed is a prepreg which is suited for preparing honeycomb sandwich panels, by which the formation of pores in the interlayer zones in the cured composite can be reduced. The prepreg of the present invention comprises a resin composition including an epoxy resin, a curing agent and a solid rubber, and a woven fabric made of reinforcing fibers, the meshes of the woven fabric being crushed such that said prepreg has a cover factor K.sub.p of 97-99.9%. Also disclosed is a reinforcing fabric comprising warps and woofs which are multifilament yarns made of carbon fibers, the widths W (mm) and finenesses D (d:denier) of the warp and woof satisfying the equation of:W=k.multidot.(D/.rho.).sup.5/9(wherein k represents 3.5.times.10.sup.-2 -10.0.times.10.sup.-2 (mm.multidot.d.sup.-5/9) and .rho. represents specific gravity of said carbon fibers), the woven fabric having a cover factor K.sub.c of 90.0-99.8%.
摘要翻译：公开了一种适用于制备蜂窝夹层板的预浸料，通过该预浸料坯可以减少固化的复合材料中的夹层区域中的孔隙的形成。本发明的预浸料包括含有环氧树脂，固化剂和固体橡胶的树脂组合物和由增强纤维制成的机织织物，所述织物的网格被粉碎，使得所述预浸料坯具有覆盖系数Kp 97-99.9％。还公开了包括经纱和纬纱的增强织物，其是由碳纤维制成的复丝纱线，纬纱的宽度W（mm）和细度D（d：旦尼尔）满足以下等式：W = kx（D / rho ）+ E，fra 5/9 + EE（其中k表示3.5×10 -2 -10.0×10 -2（mm×d-+ E，fra 5/9 + EE），rho表示所述碳纤维的比重），织物覆盖系数Kc为90.0-99.8％。

8. 发明授权

US5447785A Cloth prepreg, process for producing the same and reinforcing fabric 失效
标题翻译：布料预浸料，其生产方法和增强织物
公开(公告)号：US5447785A
公开(公告)日：1995-09-05
申请号：US88635
申请日：1993-07-09
申请人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
发明人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
IPC分类号： B29C70/08 , C08J5/04 , C08J5/24 , C08L63/00 , D03D15/00 , B32B5/02
CPC分类号： D03D15/00 , B29C70/08 , C08J5/042 , C08J5/24 , C08L63/00 , D03D15/0011 , D03D15/12 , D06C29/00 , B29K2105/0809 , C08J2363/00 , D10B2101/06 , D10B2101/12 , D10B2331/021 , D10B2401/063 , D10B2505/02 , Y10S428/902 , Y10S8/16 , Y10T428/30 , Y10T442/2008 , Y10T442/2098 , Y10T442/2951 , Y10T442/2984 , Y10T442/3065
摘要： Disclosed is a reinforcing fabric comprising warps and woofs which are multifilament yarns made of carbon fibers, the widths W (mm) and finenesses D (d:denier) of the warp and woof satisfying the equation of:W=k.multidot.(D/.rho.).sup.5/9(wherein k represents 3.5.times.10.sup.-2 - 10.0.times.10.sup.-2 (mm.multidot.d.sup.-5/9) and .rho. represents specific gravity of said carbon fibers), the woven fabric having a cover factor K.sub.c of 90.0-99.8%. The warps and woofs are twisted to not more than 5 turns/m.
摘要翻译：公开了一种包括经纱和纬纱的增强织物，其是由碳纤维制成的复丝纱线，经纱和纬纱的宽度W（mm）和细度D（d：旦尼尔）满足以下等式：W = kx（D / rho） 5/9（其中k表示3.5×10-2-10.0×10-2（mm×d-5/9），rho表示所述碳纤维的比重），所述机织织物的覆盖系数Kc为90.0-99.8％。经线扭曲至不超过5圈/米。

9. 发明授权

US5557831A Process for producing a woven carbon reinforcing fabric with a high cover factor 失效
标题翻译：制造具有高覆盖系数的编织碳增强织物的方法
公开(公告)号：US5557831A
公开(公告)日：1996-09-24
申请号：US368674
申请日：1995-01-04
申请人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
发明人： Hajime Kishi , Nobuyuki Odagiri , Tokuo Tazaki , Hideo Nagata , Takeshi Terashita , Akira Nishimura , Hiroyasu Kato
IPC分类号： B29C70/08 , C08J5/04 , C08J5/24 , C08L63/00 , D03D15/00 , C08G79/02
CPC分类号： D03D15/00 , B29C70/08 , C08J5/042 , C08J5/24 , C08L63/00 , D03D15/0011 , D03D15/12 , D06C29/00 , B29K2105/0809 , C08J2363/00 , D10B2101/06 , D10B2101/12 , D10B2331/021 , D10B2401/063 , D10B2505/02 , Y10S428/902 , Y10S8/16 , Y10T428/30 , Y10T442/2008 , Y10T442/2098 , Y10T442/2951 , Y10T442/2984 , Y10T442/3065
摘要： Method of making a reinforcing fabric comprising warps and woofs which are multifilament yarns made of carbon fibers. The widths W (mm) and finenesses D (d:denier) of the warps and woofs satisfy the equation:W=k.multidot.(D/.rho.).sup.5/9wherein k represents 3.5.times.10.sup.-2 to 10.0.times.10.sup.-2 (mm.multidot.d.sup.-5/9) and .rho. represents specific gravity of the carbon fibers. The woven fabric has a cover factor K.sub.c of 90.0 to 99.8%. The fabric is made by treating a precursor fabric with water jets.
摘要翻译：制造包括经纱和绒毛的增强织物的方法是由碳纤维制成的复丝纱线。经纱和纬纱的宽度W（mm）和细度D（d：旦尼尔）满足以下等式：W = kx（D / rho）+ E，fra 5/9 + EE其中k表示3.5×10 -2至10.0×10 -2（mmxd- + E，fra 5/9 + EE），rho表示碳纤维的比重。织物的覆盖系数Kc为90.0至99.8％。织物通过用水射流处理前体织物制成。

10. 发明授权

US4739075A Reactive end-capping agent, addition-curable quinoxaline resin oligomer and intermediate material for fiber-reinforced composite 失效
标题翻译：反应性封端剂，可加成固化喹喔啉树脂低聚物和纤维增强复合材料中间体
公开(公告)号：US4739075A
公开(公告)日：1988-04-19
申请号：US014925
申请日：1987-02-13
申请人： Nobuyuki Odagiri , Kuniaki Tobukuro
发明人： Nobuyuki Odagiri , Kuniaki Tobukuro
IPC分类号： C07D209/76 , C07D491/18 , C07D493/08 , C08G73/20 , C07D491/052 , C07D209/56
CPC分类号： C07D493/08 , C07D209/76 , C08G73/20
摘要： Disclosed in an alicyclic end-capping agent for a heterocyclic compound, which is represented by the formula [I]: ##STR1## wherein X is CO, O, S, CH.sub.2 or substituted CH.sub.2, Y.sub.1 -Y.sub.6 are halo, H, NO.sub.2, aryl, alkaryl, arylalkyl or alkyl ether, and Z is ##STR2## (Q.sub.1 is --NH.sub.2, --SH, --OH or ##STR3## (Q.sub.2 is H, or monovalent aliphatic or amomatic group). Also disclosed is an addition-curable quinoxaline resin oligomer having the above-mentioned alicylic end-capping agents at both terminals of oligomer. This oligomer is useful especially for an intermediate material for a fiber-reinforced composite.
摘要翻译：在由式[I]表示的杂环化合物的脂环族封端剂中公开：其中X是CO，O，S，CH 2或取代的CH 2，Y 1 -Y 6是卤素，H （NO 2，芳基，烷芳基，芳基烷基或烷基醚），Z是（Q1是-NH2，-SH，-OH或）（Q2是H或一价脂肪族或异构体）公开的是在低聚物的两末端具有上述脂环族封端剂的加成固化喹喔啉树脂低聚物，该低聚物特别适用于纤维增强复合材料的中间材料。

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