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1. 发明申请

US20130313476A1 WATER-SWELLING LAYERED DOUBLE HYDROXIDE, METHOD FOR PRODUCING SAME, GEL OR SOL SUBSTANCE, DOUBLE HYDROXIDE NANOSHEET, AND METHOD FOR PRODUCING SAME 有权
标题翻译：水解层状双氢氧化物，其制造方法，凝胶或溶剂物质，双氢氧化物纳米粒子及其制造方法
公开(公告)号：US20130313476A1
公开(公告)日：2013-11-28
申请号：US13982191
申请日：2012-01-18
申请人： Nobuo Iyi , Yasuo Ebina , Takayoshi Sasaki
发明人： Nobuo Iyi , Yasuo Ebina , Takayoshi Sasaki
IPC分类号： B01J20/28
CPC分类号： B01J20/28014 , C01F7/002 , C01F7/005 , C01G5/006 , C01G51/006 , C01G53/006 , C01P2002/08 , C01P2002/22 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2004/03 , C01P2004/04 , C09C1/40
摘要： Provided is a water-swelling layered double hydroxide characterized by having an organic sulfonic acid anion (A−) between layers, and by being represented by the belowmentioned general formula (1): QZR(OH)2(Z+1)(A−)(1-y)(Xn−)y/n.mH2O . . . (1). Here, Q is a divalent metal, R is a trivalent metal, A− is an organic sulfonic acid anion, m is a real number greater than 0, and z is in the range of 1.8≦z≦4.2. Xn− is the n-valent anion remaining without A− substitution, n is 1 or 2, y represents the remaining portion of Xn−, and 0≦y
摘要翻译：本发明提供一种水溶性层状双氢氧化物，其特征在于在层间具有有机磺酸阴离子（A-），并由下述通式（1）表示：QZR（OH）2（Z + 1）（A- ）（1-y）（Xn-）y / n.mH2O。。。（1）。这里，Q是二价金属，R是三价金属，A-是有机磺酸阴离子，m是大于0的实数，z在1.8 @ z @ 4.2的范围内。 Xn-是没有A-取代的n价阴离子，n是1或2，y表示Xn-的剩余部分，0≤y<0.4。

2. 发明授权

US07651675B2 Process for producing flaky titanium oxide capable of absorbing visible light 失效
标题翻译：能够吸收可见光的片状氧化钛的制造方法
公开(公告)号：US07651675B2
公开(公告)日：2010-01-26
申请号：US11662504
申请日：2005-09-13
申请人： Taki Matsumoto , Nobuo Iyi , Yoshiro Kaneko , Kenji Kitamura
发明人： Taki Matsumoto , Nobuo Iyi , Yoshiro Kaneko , Kenji Kitamura
IPC分类号： C01G23/047 , C01G25/00
CPC分类号： C09C1/0018 , B01J21/063 , B01J27/24 , B01J35/004 , B01J37/036 , C01G23/053 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2004/03 , C09C1/3607
摘要： When titanium oxide is doped with nitrogen, the resulting titanium oxide photocatalyst can be driven with visible light, which is a main component of sunlight. However, in a known process, since a high-temperature heat treatment process necessary for nitrogen doping degrades the photocatalytic activity inherent in titanium oxide, it is difficult to produce a titanium oxide photocatalyst that can be driven with a high efficiency under sunlight.A titania/organic substance composite, which includes an organic ligand coordinated to flaky titania and forms a layered structure, is immersed in aqueous ammonia to substitute the organic ligand between layers with a hydroxyl group by a ligand exchange reaction, and at the same time, to introduce ammonium into between layers of the titania having the layered structure. The resulting composite of titania and ammonium is heated at a temperature of 400° C. or higher and in such a temperature range that does not cause rutile transition, whereby nitrogen is doped into the titania by thermal decomposition of the ammonium and, in addition, titania is crystallized to an anatase form.
摘要翻译：当氧化钛掺杂氮时，所得到的氧化钛光催化剂可以作为阳光的主要成分的可见光驱动。然而，在已知的方法中，由于氮掺杂所需的高温热处理工艺降低了氧化钛中固有的光催化活性，因此难以生产能够在阳光下以高效率驱动的氧化钛光催化剂。将包含与片状二氧化钛配位并形成层状结构的有机配体的二氧化钛/有机物复合体浸渍在氨水中，通过配体交换反应将羟基的层间的有机配体取代，以将铵引入具有层状结构的二氧化钛的层之间。将所得的二氧化钛和铵的复合物在400℃以上的温度下加热，并且在不引起金红石转变的温度范围内，通过铵的热分解将氮掺杂到二氧化钛中，另外，二氧化钛结晶成锐钛矿形式。

3. 发明授权

US09545615B2 Water-swelling layered double hydroxide, method for producing same, gel or sol substance, double hydroxide nanosheet, and method for producing same 有权
标题翻译：水溶胀层状双氢氧化物，其制造方法，凝胶或溶胶物质，双氢氧化物纳米片及其制造方法
公开(公告)号：US09545615B2
公开(公告)日：2017-01-17
申请号：US13982191
申请日：2012-01-18
申请人： Nobuo Iyi , Yasuo Ebina , Takayoshi Sasaki
发明人： Nobuo Iyi , Yasuo Ebina , Takayoshi Sasaki
IPC分类号： B01J20/28 , C01G51/00 , C01G53/00 , C01F7/00 , C01G5/00 , C09C1/40
CPC分类号： B01J20/28014 , C01F7/002 , C01F7/005 , C01G5/006 , C01G51/006 , C01G53/006 , C01P2002/08 , C01P2002/22 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2004/03 , C01P2004/04 , C09C1/40
摘要： Provided is a water-swelling layered double hydroxide characterized by having an organic sulfonic acid anion (A−) between layers, and by being represented by the below mentioned general formula (1): QZR(OH)2(Z+1)(A−)(1−y)(Xn−)y/n.mH2O . . . (1). Here, Q is a divalent metal, R is a trivalent metal, A− is an organic sulfonic acid anion, m is a real number greater than 0, and z is in the range of 1.8≦z≦4.2. Xn− is the n-valent anion remaining without A− substitution, n is 1 or 2, y represents the remaining portion of Xn−, and 0≦y
摘要翻译：提供一种水溶性层状双氢氧化物，其特征在于在层之间具有有机磺酸阴离子（A-），并由下述通式（1）表示：QZR（OH）2（Z + 1）（A - ）（1-y）（Xn-）y / n.mH2O。。。（1）。这里，Q是二价金属，R是三价金属，A-是有机磺酸阴离子，m是大于0的实数，z在1.8≤z≤4.2的范围内。 Xn-是没有A-取代的n价阴离子，n是1或2，y表示Xn-的剩余部分，0≤y<0.4。

4. 发明申请

US20080003153A1 Process for Producing Flaky Titanium Oxide Capable of Absorbing Visible Light 失效
标题翻译：生产可吸收可见光的片状氧化钛的方法
公开(公告)号：US20080003153A1
公开(公告)日：2008-01-03
申请号：US11662504
申请日：2005-09-13
申请人： Taki Matsumoto , Nobuo Iyi , Yoshiro Kaneko , Kenji Kitamura
发明人： Taki Matsumoto , Nobuo Iyi , Yoshiro Kaneko , Kenji Kitamura
IPC分类号： C01G23/04
CPC分类号： C09C1/0018 , B01J21/063 , B01J27/24 , B01J35/004 , B01J37/036 , C01G23/053 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2004/03 , C09C1/3607
摘要： When titanium oxide is doped with nitrogen, the resulting titanium oxide photocatalyst can be driven with visible light, which is a main component of sunlight. However, in a known process, since a high-temperature heat treatment process necessary for nitrogen doping degrades the photocatalytic activity inherent in titanium oxide, it is difficult to produce a titanium oxide photocatalyst that can be driven with a high efficiency under sunlight. A titania/organic substance composite, which includes an organic ligand coordinated to flaky titania and forms a layered structure, is immersed in aqueous ammonia to substitute the organic ligand between layers with a hydroxyl group by a ligand exchange reaction, and at the same time, to introduce ammonium into between layers of the titania having the layered structure. The resulting composite of titania and ammonium is heated at a temperature of 400° C. or higher and in such a temperature range that does not cause rutile transition, whereby nitrogen is doped into the titania by thermal decomposition of the ammonium and, in addition, titania is crystallized to an anatase form.
摘要翻译：当氧化钛掺杂氮时，所得到的氧化钛光催化剂可以作为阳光的主要成分的可见光驱动。然而，在已知的方法中，由于氮掺杂所需的高温热处理工艺降低了氧化钛中固有的光催化活性，因此难以生产能够在阳光下以高效率驱动的氧化钛光催化剂。将包含与片状二氧化钛配位并形成层状结构的有机配体的二氧化钛/有机物复合体浸渍在氨水中，通过配体交换反应将羟基的层间的有机配体取代，以将铵引入具有层状结构的二氧化钛的层之间。将所得的二氧化钛和铵的复合物在400℃以上的温度下加热，并且在不引起金红石转变的温度范围内，通过铵的热分解将氮掺杂到二氧化钛中，另外，二氧化钛结晶成锐钛矿形式。

5. 发明申请

US20140021404A1 METHOD FOR PRODUCING ANION-EXCHANGING LAYERED DOUBLE HYDROXIDE AND METHOD FOR SUBSTITUTING CARBONATE ION OF LAYERED DOUBLE HYDROXIDE 审中-公开
标题翻译：用于生产阴离子交换层状双氢氧化物的方法和用于取代层状双氢氧化物的碳酸盐的方法
公开(公告)号：US20140021404A1
公开(公告)日：2014-01-23
申请号：US13982153
申请日：2012-01-18
申请人： Nobuo Iyi , Hirohisa Yamada , Takayoshi Sasaki
发明人： Nobuo Iyi , Hirohisa Yamada , Takayoshi Sasaki
IPC分类号： B01J41/10
CPC分类号： B01J41/10 , C01F7/002 , C01F7/005 , C01G51/006 , C01G53/006 , C01P2002/08 , C01P2002/22 , C01P2002/72 , C01P2002/84 , C01P2004/03 , C09C1/24 , C09C1/40
摘要： A method for producing an anion-exchanging LDH using a carbonate ion-type layered double hydroxide represented by general formula QaT(OH)z(CO32−)0.5-b/2(X−)b.nH2O (where 1.8≦a≦4.2, z=2(a+1), 0≦b
摘要翻译：使用由通式QaT（OH）z（CO32-）0.5-b / 2（X-）b.nH 2 O表示的碳酸根离子型层状双氢氧化物制造阴离子交换LDH的方法（其中1.8 @ a @ 4.2 ，z = 2（a + 1），0 @ b <0.5,0≤n≤5，Q表示二价金属，T表示三价金属，X是转变成一价阴离子的元素或原子团）材料，其值b至少增加至0.5，最大值为1，其中使碳酸根离子型层状氢氧化物与包含酸性化合物（MXm）的醇溶液接触（其中m = 1,2或3;当 m = 1，M为H或NRR'R“H，其中R，R'和R”为H或有机基团;当m = 2或3时，M为金属盐，即二价或三价金属）。

6. 发明授权

US08435910B2 Preparation method for anion-exchangeable, layered double hydroxides 失效
标题翻译：阴离子交换层状双氢氧化物的制备方法
公开(公告)号：US08435910B2
公开(公告)日：2013-05-07
申请号：US12734955
申请日：2008-12-02
申请人： Nobuo Iyi , Takayoshi Sasaki
发明人： Nobuo Iyi , Takayoshi Sasaki
IPC分类号： B01J21/16
CPC分类号： C01F7/005 , B01D53/62 , B01D2251/40 , B01D2251/604 , B01D2251/606 , B01D2253/104 , B01D2253/112 , B01D2257/504 , B01J20/0277 , B01J20/041 , B01J20/043 , B01J20/06 , B01J20/08 , B01J41/10 , C01G9/006 , C01G53/006 , C01P2002/22 , C01P2002/72 , C01P2002/82 , C01P2004/03 , C02F2001/422 , Y02C10/04 , Y02P20/152
摘要： The invention has for its object to provide a preparation method for preparing an anion-exchangeable LDH by decarbonation of a carbonate ion type LDH, which makes sure de carbonation is implemented with safety in a continuous manner while crystal shape, crystal structure and crystallinity are kept intact.The invention provides a preparation method for preparing an anion-exchangeable, layered double hydroxide wherein a carbonate ion type layered double hydroxide (LDH) having a composition represented by a general formula: QxR(OH)z(CO32−)0.5-y/2(X−)y.nH2O where x is indicative of a numeral range of 1.8≦x≦4.2; z is indicative of 2(x+1); y is indicative of a minimum value of at least 0 that increases to less than 1 when anions (X−) remain or a part of anions is introduced; Q is a divalent metal ion; R is a trivalent metal ion; and n is 2±2 is used as a starting material, and y in said general formula increases to a maximum of 1 by substitution of a minus monovalent anion (X−1) at a carbonate ion site thereby implementing substitution, characterized in that the starting material is dispersed in an aqueous solution mixed with a salt containing minus monovalent anions (X−) in an amount enough for substitution at the carbonate ion site while said aqueous solution is kept at a pH (hydrogen ion exponent) of greater than 4 to less than 7.
摘要翻译：本发明的目的是提供一种通过碳酸根离子型LDH的脱碳制备可阴离子交换的LDH的制备方法，其确保以连续方式安全地进行脱碳酸化，同时保持晶体形状，晶体结构和结晶度完整。本发明提供一种制备阴离子交换性层状双氢氧化物的制备方法，其中具有由以下通式表示的组成的碳酸根离子型层状双氢氧化物（LDH）：QxR（OH）z（CO32-）0.5-y / 2 （X-）y.nH 2 O，其中x表示1.8 @ x @ 4.2的数字范围; z表示2（x + 1）; y表示当阴离子（X）保留或部分阴离子被引入时，至少为0的最小值增加到小于1; Q是二价金属离子; R是三价金属离子; 并且使用n为2±2作为起始原料，通过在碳酸根离子位置取代负一价阴离子（X-1）从而实现取代，所述通式中的y增加到最大值1，其特征在于：将原料分散在与含有负一价阴离子（X-X）的盐混合的水溶液中，其量足以在碳酸盐离子位置进行取代，同时所述水溶液保持在大于4至大约4的pH（氢离子指数）至小于7。

7. 发明申请

US20100279848A1 PREPARATION METHOD FOR ANION-EXCHANGEABLE, LAYERED DOUBLE HYDROXIDES 失效
标题翻译：用于阴离子交换的层状双羟基化合物的制备方法
公开(公告)号：US20100279848A1
公开(公告)日：2010-11-04
申请号：US12734955
申请日：2008-12-02
申请人： Nobuo Iyi , Takayoshi Sasaki
发明人： Nobuo Iyi , Takayoshi Sasaki
IPC分类号： B01J37/30
CPC分类号： C01F7/005 , B01D53/62 , B01D2251/40 , B01D2251/604 , B01D2251/606 , B01D2253/104 , B01D2253/112 , B01D2257/504 , B01J20/0277 , B01J20/041 , B01J20/043 , B01J20/06 , B01J20/08 , B01J41/10 , C01G9/006 , C01G53/006 , C01P2002/22 , C01P2002/72 , C01P2002/82 , C01P2004/03 , C02F2001/422 , Y02C10/04 , Y02P20/152
摘要： The invention has for its object to provide a preparation method for preparing an anion-exchangeable LDH by decarbonation of a carbonate ion type LDH, which makes sure de carbonation is implemented with safety in a continuous manner while crystal shape, crystal structure and crystallinity are kept intact.The invention provides a preparation method for preparing an anion-exchangeable, layered double hydroxide wherein a carbonate ion type layered double hydroxide (LDH) having a composition represented by a general formula: QxR(OH)z(CO32−)0.5-y/2(X−)y.nH2O where x is indicative of a numeral range of 1.8≦x≦4.2; z is indicative of 2(x+1); y is indicative of a minimum value of at least 0 that increases to less than 1 when anions (X−) remain or a part of anions is introduced; Q is a divalent metal ion; R is a trivalent metal ion; and n is 2±2 is used as a starting material, and y in said general formula increases to a maximum of 1 by substitution of a minus monovalent anion (X−1) at a carbonate ion site thereby implementing substitution, characterized in that the starting material is dispersed in an aqueous solution mixed with a salt containing minus monovalent anions (X−) in an amount enough for substitution at the carbonate ion site while said aqueous solution is kept at a pH (hydrogen ion exponent) of greater than 4 to less than 7.
摘要翻译：本发明的目的是提供一种通过碳酸根离子型LDH的脱碳制备可阴离子交换的LDH的制备方法，其确保以连续方式安全地进行脱碳酸化，同时保持晶体形状，晶体结构和结晶度完整。本发明提供一种制备阴离子交换性层状双氢氧化物的制备方法，其中具有由以下通式表示的组成的碳酸根离子型层状双氢氧化物（LDH）：QxR（OH）z（CO32-）0.5-y / 2 （X）y.nH 2 O其中x表示数值范围为1.8＆amp; nlE; x＆nlE; 4.2; z表示2（x + 1）; y表示当阴离子（X）保留或部分阴离子被引入时，至少为0的最小值增加到小于1; Q是二价金属离子; R是三价金属离子; 并且使用n为2±2作为起始原料，通过在碳酸根离子位置取代负一价阴离子（X-1）从而实现取代，所述通式中的y增加到最大值1，其特征在于：将原料分散在与含有负一价阴离子（X-X）的盐混合的水溶液中，其量足以在碳酸盐离子位置进行取代，同时所述水溶液保持在大于4至大约4的pH（氢离子指数）至小于7。

8. 发明申请

US20100210786A1 THERMOPLASTIC LAYERED ALKYLSILOXANE AND PRODUCTION METHOD THEREFOR 审中-公开
标题翻译：热塑性层状烷基硅氧烷及其制备方法
公开(公告)号：US20100210786A1
公开(公告)日：2010-08-19
申请号：US12772408
申请日：2010-05-03
申请人： Kazuko FUJII , Hiroshi Kodama , Nobuo Iyi , Taketoshi Fujita , Shigenobu Hayashi
发明人： Kazuko FUJII , Hiroshi Kodama , Nobuo Iyi , Taketoshi Fujita , Shigenobu Hayashi
IPC分类号： C08L83/06 , C08G77/14 , C08G77/08 , C08G77/04
CPC分类号： C08G77/04 , C09D183/04
摘要： An alkyl silane compound represented by the general formula RSi(OL)3 (here, R is an alkyl group, L is H, Si or a group capable of easily changing the OL group into the OH group in a solution or a suspension), a silicon compound represented by the general formula Si(OM)4 (here, M is H, Si or a group capable of easily changing the OM group into the OH group in a solution or a suspension), and water are reacted in a solvent or a dispersion medium. A thermoplastic layered alkyl siloxane with the composition formula represented by the general formula (RSi1+xO2+1.5x+0.5xLz)m (here, R is an alkyl group, L is H, Si or a group capable of easily changing the OL group into the OH group in a solution or a suspension, and 0.5≦x≦2, 2≦m≦200, 0≦z), which is a thermoplastic inorganic/organic layered composite having good shaping property and dispersing property, capable of transitioning at various temperatures including the vicinity of the room temperature can be provided.
摘要翻译：由通式RSi（OL）3表示的烷基硅烷化合物（这里，R为烷基，L为H，Si或能够在溶液或悬浮液中容易地将OL基变为OH基的基团），由通式Si（OM）4表示的硅化合物（这里，M为H，Si或能够在溶液或悬浮液中容易地将OM基变为OH基的基团），水在溶剂中反应或分散介质。具有由通式（RSi1 + xO2 + 1.5x + 0.5xLz）m表示的组成式的热塑性层状烷基硅氧烷（这里，R是烷基，L是H，Si或能够容易地改变OL基团的基团在溶液或悬浮液中加入OH基团，和0.5＆amp; NlE; x＆lt; 2,2; nlE; m＆nlE; 200,0＆amp; nlE; z），其是具有良好成型性和分散性的热塑性无机/有机层状复合材料，可以提供包括室温附近在内的各种温度。

9. 发明申请

US20050228158A1 Thermoplatic layered alkylsiloxane and process for production thereof 审中-公开
标题翻译：热塑性层状烷基硅氧烷及其生产方法
公开(公告)号：US20050228158A1
公开(公告)日：2005-10-13
申请号：US10526395
申请日：2003-09-18
申请人： Kazauko Fujii , Hiroshi Kodama , Nobuo Iyi , Taketoshi Fujita , Shigenobu Hayashi
发明人： Kazauko Fujii , Hiroshi Kodama , Nobuo Iyi , Taketoshi Fujita , Shigenobu Hayashi
IPC分类号： C07F7/08 , C08G77/04 , C09C3/12 , C09D183/00 , C09D183/04
CPC分类号： C08G77/04 , C09D183/04
摘要： An alkyl silane compound represented by the general formula RSi(OL)3 (here, R is an alkyl group, L is H, Si or a group capable of easily changing the OL group into the OH group in a solution or a suspension), a silicon compound represented by the general formula Si(OM)4 (here, M is H, Si or a group capable of easily changing the OM group into the OH group in a solution or a suspension), and water are reacted in a solvent or a dispersion medium. A thermoplastic layered alkyl siloxane with the composition formula represented by the general formula (RSi1+xO2+1.5x+zLz)m (here, R is an alkyl group, L is H, Si or a group capable of easily changing the OL group into the OH group in a solution or a suspension, and 0.5≦x≦2, 2≦m≦200, 0≦z), which is a thermoplastic inorganic/organic layered composite having good shaping property and dispersing property, capable of transitioning at various temperatures including the vicinity of the room temperature can be provided.
摘要翻译：由通式RSi（OL）3 N表示的烷基硅烷化合物（这里，R为烷基，L为H，Si或能够容易地将OL基变为OH基的基团溶液或悬浮液），由通式Si（OM）4 S（OM）表示的硅化合物（这里，M为H，Si或能够容易地将OM基变为OH基的基团溶液或悬浮液），水在溶剂或分散介质中反应。具有由通式（RSi 1 + x O 2 + 1.5x + z L z））表示的组成式的热塑性层状烷基硅氧烷，（这里，R是烷基，L是H，Si或能够在溶液或悬浮液中容易地将OL基变成OH基的基团，并且0.5 <= x <= 可以提供能够在包括室温附近的各种温度下转变的具有良好成型性和分散性的热塑性无机/有机层状复合材料的2，2 <= m <= 200,0 <= z）。

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