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1. 发明授权

US5659094A Process for co-producing 1,1,1,2-tetrafluoroethane pentafluoroethane and 1,1,1-trifluoroethane 失效
标题翻译：共1,1,1,2-四氟乙烷五氟乙烷和1,1,1-三氟乙烷共生产方法
公开(公告)号：US5659094A
公开(公告)日：1997-08-19
申请号：US591705
申请日：1996-01-25
申请人： Hoon Sik Kim , Byung Gwon Lee , Honggon Kim , Moon Jo Chung
发明人： Hoon Sik Kim , Byung Gwon Lee , Honggon Kim , Moon Jo Chung
IPC分类号： B01J23/26 , B01J27/12 , B01J27/132 , B01J27/138 , C07B61/00 , C07C17/20 , C07C17/21 , C07C17/23 , C07C19/08
CPC分类号： C07C17/21 , B01J27/132 , B01J27/138 , C07C17/206 , C07C17/23
摘要： A process for co-production of 1,1,1,2-tetrafluoroethane (HFC-134a;CF.sub.3 CH.sub.2 F), pentafluoroethane (HFC-125; CF.sub.3 CHF.sub.2) and 1,1,1 -trifluoroethane (HFC-143a; CF.sub.3 CH.sub.3) by a two-step gaseous reaction comprising the steps of a) reacting 1,1,1-trifluoro-2-chloroethane (CFCH.sub.2 Cl, HCFC-133a) with HF in a first reactor to prepare 1,1,1,2-tetrafluoroethane (HFC-134a; CF.sub.3 CH.sub.2 F), pentafluoroethane (HFC-125; CF.sub.3 CHF.sub.2) and 1,1,1-trifluoroethane (HFC-143a; CF.sub.3 CH.sub.3); b) adding trichloroethylene (TCE:CCl.sub.2 CHCl) to the reaction product of step a) in a second reactor to prepare HCFC-133a; separating HCl, HFC-134a, HFC-125 and HFC-143a from the reaction product of step b) and recycling HCFC-133a to the first reactor, and the stages being performed in the presence of fluorization catalyst obtained by calcining a reaction product which is obtained by reacting ethanol with a mixture of calcium fluoride(CaF.sub.2) with an aqueous solution of chromium trioxide, zinc chloride and ferrous chloride is provided.
摘要翻译：一种通过两个共同生产1,1,1,2-四氟乙烷（HFC-134a; CF3CH2F），五氟乙烷（HFC-125; CF3CHF2）和1,1,1-三氟乙烷（HFC-143a; CF3CH3）的方法包括以下步骤：a）在第一反应器中使1,1,1-三氟-2-氯乙烷（CFCH2Cl，HCFC-133a）与HF反应制备1,1,1,2-四氟乙烷（HFC-134a ; CF 3 CH 2 F），五氟乙烷（HFC-125; CF 3 CHF 2）和1,1,1-三氟乙烷（HFC-143a; CF 3 CH 3）; b）在第二反应器中将三氯乙烯（TCE：CCl 2 CHCl）加入到步骤a）的反应产物中以制备HCFC-133a; 从步骤b）的反应产物中分离出HCl，HFC-134a，HFC-125和HFC-143a，并将HCFC-133a再循环到第一反应器中，这些阶段在通过煅烧反应产物得到的氟化催化剂存在下进行，通过乙醇与氟化钙（CaF 2）与三氧化铬的水溶液，氯化锌和氯化亚铁的混合物反应获得。

2. 发明授权

US5571770A Catalyst for fluorination of 1,1,1,-trifluoro-2,2-dichloroethane and method for preparing the same 失效
标题翻译：用于氟化1,1,1-三氟-2,2-二氯乙烷的催化剂及其制备方法
公开(公告)号：US5571770A
公开(公告)日：1996-11-05
申请号：US490726
申请日：1995-06-15
申请人： Hoon Sik Kim , Moon Jo Chung , Byung Gwon Lee , Hyun Joo Lee
发明人： Hoon Sik Kim , Moon Jo Chung , Byung Gwon Lee , Hyun Joo Lee
IPC分类号： B01J27/138 , B01J23/26 , B01J23/86 , C07B61/00 , C07C17/20 , C07C19/08 , C07C19/12
CPC分类号： B01J23/26 , B01J23/866 , C07C17/206
摘要： There are a catalyst for fluorination production of 1,1,1-trifluoro-2,2-dichloroethane comprises chromium, one compound selected from the group consisting of Mg and Ca and at least one metal component selected from the group consisting of Zn, Ce and Ni, wherein the molar ratio of Cr to Mg or Ca ranges from 1:1 to 1:32 and the molar ratio Cr to the metal component is not more than 1:0.5, and method for preparing the same comprising the steps of; producing an admixture of a composition comprising chromium, one compound selected from the group consisting of magnesium fluoride and calcium fluoride and at least one metal compound selected from a group consisting of cerium fluoride, zinc fluoride and nickel fluoride with water and refluxing the admixture in methanol or ethanol.
摘要翻译：具有1,1,1-三氟-2,2-二氯乙烷的氟化生产催化剂包括铬，一种选自Mg和Ca的化合物和至少一种选自Zn，Ce 和Ni，其中Cr与Mg或Ca的摩尔比范围为1：1至1:32，并且金属组分的摩尔比Cr不大于1:0.5，及其制备方法包括以下步骤：制备包含铬的组合物的混合物，一种选自氟化镁和氟化钙的化合物和至少一种选自氟化铈，氟化锌和氟化镍的金属化合物与水并将该混合物在甲醇中回流或乙醇。

3. 发明授权

US06710215B2 Method of a simultaneous preparation of hexafluoropropylene and octafluorocyclobutane 失效
标题翻译：同时制备六氟丙烯和八氟环丁烷的方法
公开(公告)号：US06710215B2
公开(公告)日：2004-03-23
申请号：US10218362
申请日：2002-08-14
申请人： Dong Ju Moon , Moon Jo Chung , Young Soo Kwon , Byoung Sung Ahn
发明人： Dong Ju Moon , Moon Jo Chung , Young Soo Kwon , Byoung Sung Ahn
IPC分类号： C07C1700
CPC分类号： C07C23/06 , C07C17/269 , C07C17/281 , C07C21/185
摘要： A method of simultaneous and selective prepararation of hexafluoropropylene and octafluorocyclebutane comprising the steps of: (a) thermally decomposing difluorochloromethane to obtain tetrafluoroethylene and then supplying the resulting tetrafluoroethylene into a fluidized bed reactor equipped with a distributor for supplying steam; and (b) supplying steam into a flow of tetrafluoroethylene supplied into the fluidized bed reactor, through a distributor for supplying steam at a certain molar ratio of tetrafluoroethylene/stream, and then performing dimerization of tetrafluoroethylene in the fluidized bed reactor under an atmospheric pressure.
摘要翻译：一种同时和选择性制备六氟丙烯和八氟环丁烷的方法，包括以下步骤：（a）热分解二氟氯甲烷以获得四氟乙烯，然后将所得的四氟乙烯供给到装有用于供应蒸汽的分配器的流化床反应器中; 和（b）通过用于以一定摩尔比的四氟乙烯/料流供给蒸汽的分配器供应蒸汽供入到流化床反应器中的四氟乙烯流中，然后在大气压下在流化床反应器中进行四氟乙烯的二聚。

4. 发明授权

US06592773B2 Refrigerant mixture comprising difluromethane, pentafluroethane and 1,1,1-trifluoroethane 失效
公开(公告)号：US06592773B2
公开(公告)日：2003-07-15
申请号：US10338139
申请日：2003-01-08
申请人： Byung Gwon Lee , Jong Sung Lim , Kun You Park , Moon Jo Chung , Seong Joon Cho
发明人： Byung Gwon Lee , Jong Sung Lim , Kun You Park , Moon Jo Chung , Seong Joon Cho
IPC分类号： C09K504
CPC分类号： C09K5/045 , C09K2205/112 , C09K2205/12 , C09K2205/22 , C09K2205/43
摘要： A novel refrigerant composition useful as a substitute for HCFC-22, comprising a first constituent of difluoromethane (CH2F2, HFC-32); a second constituent of pentafluoroethane (CHF2CF3, HFC-125); a third constituent of 1,1,1-trifluoroethane (CH3CF3, HFC-143a); a fourth constituent selected from the group consisting of cyclopropane (C3H6, RC-270), 1,1,1,2,3,3,3-heptafluoropropane (CF3CHFCF3, HFC-227ea), 1,1,1,2,2-pentafluoropropane (CH3CF2CF3, HFC-245cb), isobutane (CH(CH3)2CH3, R-600a), octafluorocyclobutane (C4F8, RC-318), 1,1,1,2,3,3-hexafluoropropane (CHF2CHFCF3, HFC-236ea), butane (C4H10, R-600), bis(difluoromethyl)ether (CHF2OCHF2, HFE-134) and pentafluoroethylmethylether (CF3CF2OCH3, HFE-245).

5. 发明授权

US6075167A Method for preparing cycloaliphatic diamines from aromatic diamines 有权
标题翻译：从芳族二胺制备脂环族二胺的方法
公开(公告)号：US6075167A
公开(公告)日：2000-06-13
申请号：US160821
申请日：1998-09-25
申请人： Hoon Sik Kim , Kun Yu Park , Young Soo Kwon , Moon Jo Chung , Byung Gwon Lee
发明人： Hoon Sik Kim , Kun Yu Park , Young Soo Kwon , Moon Jo Chung , Byung Gwon Lee
IPC分类号： C07C211/18 , C07C209/72 , C07C211/36 , C07C209/00
CPC分类号： C07C209/72
摘要： This invention relates to a method for preparing cycloaliphatic diamines by hydrogenating aromatic diamines in the presence of a supported ruthenium catalyst and a metal nitrite as a catalyst promoter to increase the rate of the hydrogenation reaction and decrease the amount of higher boiler by-products.
摘要翻译：本发明涉及一种通过在负载型钌催化剂和亚硝酸金属作为催化剂促进剂的存在下将芳族二胺加氢来制备脂环族二胺的方法，以提高氢化反应速率并减少较高的锅炉副产物的量。

6. 发明授权

US5959166A Method for concurrently producing different hydrofluoro carbons 失效
标题翻译：同时生产不同氢氟碳的方法
公开(公告)号：US5959166A
公开(公告)日：1999-09-28
申请号：US966093
申请日：1997-11-07
申请人： Hoon Sik Kim , Moon Jo Chung , Kun You Park , Young Soo Kwon
发明人： Hoon Sik Kim , Moon Jo Chung , Kun You Park , Young Soo Kwon
IPC分类号： B01J23/26 , B01J27/125 , B01J27/132 , B01J27/138 , C07B61/00 , C07C17/20 , C07C17/21 , C07C19/08 , C07C19/10 , C07C17/08
CPC分类号： C07C17/206 , C07C17/21 , Y02P20/582
摘要： A method for concurrently producing different hydrofluoro carbons, comprising the reaction of halocarbon or hydrohalocarbon with hydrogen fluoride in a reaction system consisting of a series of at least two discrete reactors, in the presence of catalysts, said reactors each being provided with different reactant materials and differing in reaction conditions including the catalysts and/or reaction temperature, thereby flexibly controlling their production rates in accordance with fluctuations in their demand, and eliminating the risk of constructing large scale plants responsible for individual hydrofluorocarbons.
摘要翻译：一种同时生产不同氢氟碳的方法，包括在由一系列至少两个不连续的反应器组成的反应体系中，在催化剂存在下，卤代烃或氢卤化碳与氟化氢的反应，所述反应器各自具有不同的反应物料和包括催化剂和/或反应温度在内的反应条件不同，从而根据其需求的波动灵活地控制其生产率，并消除构建负责单个氢氟碳化物的大型设备的风险。

7. 发明授权

US5723700A Method for concurrently producing 1,1,1,2-tetrafluoroethane and pentafluoroethane 失效
标题翻译：同时生产1,1,1,2-四氟乙烷和五氟乙烷的方法
公开(公告)号：US5723700A
公开(公告)日：1998-03-03
申请号：US708466
申请日：1996-09-05
申请人： Byung Gwon Lee , Hoon Sik Kim , Honggon Kim , Sang Deuk Lee , Moon Jo Chung
发明人： Byung Gwon Lee , Hoon Sik Kim , Honggon Kim , Sang Deuk Lee , Moon Jo Chung
IPC分类号： C07C17/10 , C07C17/20 , C07C17/21 , C07C19/08 , C07C17/08
CPC分类号： C07C19/08 , C07C17/10 , C07C17/206 , C07C17/21
摘要： There is a method for concurrently producing 1,1,1,2-tetrafluoroethane and pentafluoroethane, which comprises (A) reacting 1,1,1-trifluoro-2-chloroethane, hydrogen fluoride and chlorine in a first reactor in the presence of flurorination catalyst at a temperature in the range of from 300.degree. C. to 450.degree. C.; (B) transfering the products of step (A) together with trichloroethylene to a second reactor and reacting them at a temperature in the range of from 200.degree. C. to 400.degree. C.; (C) separating 1,1,1,2-tetrafluoroethane and pentafluoroethane from the resultant products; and (D) feeding the remaining products from step (C) back to the first reactor, wherein the molar ratio of chlorine/1,1,1-trifluoro-2-chloroethanethe in step (A) is in the range of from 0.001 to 0.05
摘要翻译：有一种同时生产1,1,1,2-四氟乙烷和五氟乙烷的方法，该方法包括（A）在第一反应器中在氟化物存在下使1,1,1-三氟-2-氯乙烷，氟化氢和氯反应催化剂在300℃至450℃的温度范围内。（B）将步骤（A）的产物与三氯乙烯一起转移到第二反应器中，并在200℃至400℃的温度下反应。（C）从所得产物中分离1,1,1,2-四氟乙烷和五氟乙烷; 和（D）将来自步骤（C）的剩余产物反馈回第一反应器，其中步骤（A）中氯/ 1,1,1-三氟-2-氯乙烷的摩尔比在0.001至 0。

8. 发明授权

US06476088B1 Polyolefin foam beads having high density crust and method for manufacturing the same 失效
标题翻译：具有高密度地壳的聚烯烃泡沫珠及其制造方法
公开(公告)号：US06476088B1
公开(公告)日：2002-11-05
申请号：US09761568
申请日：2001-01-16
申请人： Moon Jo Chung , Nak Joong Kim
发明人： Moon Jo Chung , Nak Joong Kim
IPC分类号： C08J922
CPC分类号： C08J9/18 , B29C44/3461 , C08J2323/02
摘要： Polyolefin foam bead having a high-density crust and a method for manufacturing the same are disclosed. The novel polyolefin foam bead having an surface layer (crust) which is higher in density than its inner structure can be manufactured by the method comprised of impregnating a polyolefin resin with a forming agent by stirring the mixture of the polyolefin resin particles, water and the foaming agent in a pressure vessel under heat, followed by diffusing out the foaming agent from the surface layer of the resin particle to decrease the concentration of the foaming agent in the surface layer. Thereafter, the polyolefin resin is foamed by discharging the resin particles to low pressure environment.
摘要翻译：公开了具有高密度地壳的聚烯烃泡沫珠及其制造方法。具有密度高于其内部结构的表面层（外壳）的新型聚烯烃泡沫珠粒可以通过以下方法制造：将聚烯烃树脂浸渍在成形剂中，通过搅拌聚烯烃树脂颗粒，水和发泡剂在加热的压力容器中，然后从树脂颗粒的表面层扩散出发泡剂，以降低发泡剂在表面层中的浓度。此后，聚烯烃树脂通过将树脂颗粒排放到低压环境而发泡。

9. 发明授权

US06403662B2 Continuous process for manufacturing polyolefin foam beads 有权
标题翻译：制造聚烯烃泡沫珠的连续工艺
公开(公告)号：US06403662B2
公开(公告)日：2002-06-11
申请号：US09761565
申请日：2001-01-16
申请人： Moon Jo Chung , Nak Joong Kim
发明人： Moon Jo Chung , Nak Joong Kim
IPC分类号： C08J916
CPC分类号： B29C44/3453 , B29C44/206 , B29C44/3461 , C08J9/18 , C08J2323/02 , Y10S521/917
摘要： A method for manufacturing polyolefin foam beads by a continuous process is disclosed by which the polyolefin foam beads can be produced with increased efficiency and productivity. The method comprises a step of impregnating foaming agent into polyolefin resin by mixing polyolefin resin particles, water and the foaming agent in a impregnation chamber under heat and pressure, followed by a step of storing the polyolefin resin containing the foaming agent in a storing chamber under heat and pressure. Thereafter, the resin particles are subjected to a foaming step by continuously or intermittently discharging the resin particles from the storing chamber to a low pressure expansion chamber by utilizing a discharging device, in the same time period when a next batch of polyolefin resin is added and mixed in the impregnation chamber after being supplied with the resin particles from a resin supply chamber.
摘要翻译：公开了一种通过连续方法制造聚烯烃泡沫珠的方法，通过该方法可以以更高的效率和生产率生产聚烯烃泡沫珠。该方法包括通过在聚烯烃树脂中将聚烯烃树脂颗粒，水和发泡剂在加热和压力下在浸渍室中混合，然后将含有发泡剂的聚烯烃树脂储存在储存室中的步骤，将发泡剂浸渍到聚烯烃树脂中热和压力。此后，在添加下一批聚烯烃树脂的同一时间段内，通过利用排出装置将树脂颗粒从储存室连续地或间歇地排出到低压膨胀室，从而对树脂颗粒进行发泡步骤，在从树脂供给室供给树脂粒子之后，在浸渍室中混合。

10. 发明授权

US5716592A Cerous chloride-chromic oxide catalyst for producing chlorine, methods for producing the same and a method for producing chlorine 失效
标题翻译：用于生产氯的氯化铈 - 氧化铬催化剂，其制备方法和氯生产方法
公开(公告)号：US5716592A
公开(公告)日：1998-02-10
申请号：US711226
申请日：1996-09-09
申请人： Byoung Sung Ahn , Dong Ju Moon , Kun You Park , Moon Jo Chung
发明人： Byoung Sung Ahn , Dong Ju Moon , Kun You Park , Moon Jo Chung
IPC分类号： B01J23/26 , B01J27/132 , B01J27/138 , C01B7/04
CPC分类号： B01J27/132 , B01J23/26 , B01J27/138 , Y10S423/12
摘要： A process for producing chlorine by reaction of gaseous hydrogen chloride with oxygen in the presence of a catalyst prepared by reaction of chromium trioxide and cerous chloride with ethanol and calcination of the resulting reaction product, or, alternatively, prepared by reaction of chromium trioxide with ethanol, and calcination and impregnation of the resulting chromic oxide with aqueous solution of cerous chloride.
摘要翻译：在三氧化二砷和氯化铈与乙醇反应制备的催化剂存在下，通过气态氯化氢与氧反应生成氯的方法，煅烧所得反应产物，或者通过三氧化铬与乙醇的反应制备氯的方法，并用氯化铈水溶液煅烧和浸渍所得到的氧化铬。

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